Selective Encapsulation and Separation of Dihalobenzene Isomers with Discrete Heterometallic Macrocages

A series of metallosupramolecular architectures have been prepared, including rectangles, prisms and cages, that feature half‐sandwich rhodium(III) fragments at the vertices. Remarkably, a stable cage‐like heteropolymetallic complex possessing eight rhodium(III) and two silver(I) metal ions (3) has...

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