Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples

An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and...

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Veröffentlicht in:Bulletin of environmental contamination and toxicology 2009-11, Vol.83 (5), p.626-629
Hauptverfasser: Tang, Jianshe, Zhang, Min, Cheng, Guohua, Lu, Yitong
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Zhang, Min
Cheng, Guohua
Lu, Yitong
description An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%-95.95% of the diazinon from water and soil with CVs of 5.08%-8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%-81.58%); however, it effectively clean up the soil samples.
doi_str_mv 10.1007/s00128-009-9823-4
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subjects Aquatic Pollution
Calibration
Chemical compounds
Chromatography
Chromatography, Affinity - instrumentation
Chromatography, Affinity - methods
Chromatography, High Pressure Liquid - methods
Diazinon - analysis
Earth and Environmental Science
Ecotoxicology
Environment
Environmental Chemistry
Environmental Health
Fungicides
Insecticides
Limit of Detection
Liquid chromatography
Pesticides
Pesticides - analysis
Pollution
Pretreatment of water
Soil contamination
Soil Pollutants - analysis
Soil Science & Conservation
Soils
Waste Water Technology
Water Management
Water Pollutants, Chemical - analysis
Water pollution
Water Pollution Control
title Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples
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