Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples
An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and...
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Veröffentlicht in: | Bulletin of environmental contamination and toxicology 2009-11, Vol.83 (5), p.626-629 |
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description | An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%-95.95% of the diazinon from water and soil with CVs of 5.08%-8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%-81.58%); however, it effectively clean up the soil samples. |
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In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%-95.95% of the diazinon from water and soil with CVs of 5.08%-8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%-81.58%); however, it effectively clean up the soil samples.</description><identifier>ISSN: 0007-4861</identifier><identifier>EISSN: 1432-0800</identifier><identifier>DOI: 10.1007/s00128-009-9823-4</identifier><identifier>PMID: 19590806</identifier><language>eng</language><publisher>New York: New York : Springer-Verlag</publisher><subject>Aquatic Pollution ; Calibration ; Chemical compounds ; Chromatography ; Chromatography, Affinity - instrumentation ; Chromatography, Affinity - methods ; Chromatography, High Pressure Liquid - methods ; Diazinon - analysis ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Fungicides ; Insecticides ; Limit of Detection ; Liquid chromatography ; Pesticides ; Pesticides - analysis ; Pollution ; Pretreatment of water ; Soil contamination ; Soil Pollutants - analysis ; Soil Science & Conservation ; Soils ; Waste Water Technology ; Water Management ; Water Pollutants, Chemical - analysis ; Water pollution ; Water Pollution Control</subject><ispartof>Bulletin of environmental contamination and toxicology, 2009-11, Vol.83 (5), p.626-629</ispartof><rights>Springer Science+Business Media, LLC 2009</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a448t-ecbb8b6acaa099d896683e8c8b8838708228e3caed1acd494876fc671efbfcaa3</citedby><cites>FETCH-LOGICAL-a448t-ecbb8b6acaa099d896683e8c8b8838708228e3caed1acd494876fc671efbfcaa3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00128-009-9823-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00128-009-9823-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27929,27930,41493,42562,51324</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/19590806$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Tang, Jianshe</creatorcontrib><creatorcontrib>Zhang, Min</creatorcontrib><creatorcontrib>Cheng, Guohua</creatorcontrib><creatorcontrib>Lu, Yitong</creatorcontrib><title>Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples</title><title>Bulletin of environmental contamination and toxicology</title><addtitle>Bull Environ Contam Toxicol</addtitle><addtitle>Bull Environ Contam Toxicol</addtitle><description>An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%-95.95% of the diazinon from water and soil with CVs of 5.08%-8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%-81.58%); however, it effectively clean up the soil samples.</description><subject>Aquatic Pollution</subject><subject>Calibration</subject><subject>Chemical compounds</subject><subject>Chromatography</subject><subject>Chromatography, Affinity - instrumentation</subject><subject>Chromatography, Affinity - methods</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Diazinon - analysis</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Fungicides</subject><subject>Insecticides</subject><subject>Limit of Detection</subject><subject>Liquid chromatography</subject><subject>Pesticides</subject><subject>Pesticides - analysis</subject><subject>Pollution</subject><subject>Pretreatment of water</subject><subject>Soil contamination</subject><subject>Soil Pollutants - analysis</subject><subject>Soil Science & Conservation</subject><subject>Soils</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollutants, Chemical - analysis</subject><subject>Water pollution</subject><subject>Water Pollution Control</subject><issn>0007-4861</issn><issn>1432-0800</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kUGP0zAQhSMEYsvCD-AC1h64BezYTR1uq-zCVqpgpVI4WpNk0noV213bESp_jL-HuylaiQMny3rfezOal2WvGX3PKF18CJSyQuaUVnklC56LJ9mMCV7kVFL6NJvRBOVCluwsexHCXaLnsiieZ2esmleJKWfZ7ysNv7R1llxhRG-0hajTbxO03ZIbvd2RW_S98wZsi2Sl70fdkXrnnYHoth72u8NHcklqZ_bgdUhW15O4Q3L95fsyr8E3SRtGY8lPHXcPytKY0Troe211PPyV04wH9dZj9AjRoI3HrB-Q9iJgO7J2eiBrMPsBw8vsWQ9DwFen9zzbfLr-Vt_kq6-fl_XlKgchZMyxbRrZlNAC0KrqZFWWkqNsZSMllwuaziGRt4Adg7YTlZCLsm_LBcO-6ZOJn2fvpty9d_cjhqiMDi0OA1h0Y1AFY7JgFU3gxT_gnRu9TbupgnMmxYKXCWIT1HoXgsde7b024A-KUXWsVE2VqlSpOlaqRPK8OQWPjcHu0XHqMAHFBIQk2S36x8n_S307mXpwCrapObVZF5RxykpZUTHnfwDz4bh5</recordid><startdate>20091101</startdate><enddate>20091101</enddate><creator>Tang, Jianshe</creator><creator>Zhang, Min</creator><creator>Cheng, Guohua</creator><creator>Lu, Yitong</creator><general>New York : Springer-Verlag</general><general>Springer-Verlag</general><general>Springer Nature B.V</general><scope>FBQ</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7T7</scope><scope>7TK</scope><scope>7TV</scope><scope>7U7</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>88I</scope><scope>8C1</scope><scope>8FD</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>M0S</scope><scope>M1P</scope><scope>M2P</scope><scope>P64</scope><scope>PATMY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PYCSY</scope><scope>Q9U</scope><scope>7QH</scope><scope>7ST</scope><scope>7UA</scope><scope>SOI</scope></search><sort><creationdate>20091101</creationdate><title>Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples</title><author>Tang, Jianshe ; Zhang, Min ; Cheng, Guohua ; Lu, Yitong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a448t-ecbb8b6acaa099d896683e8c8b8838708228e3caed1acd494876fc671efbfcaa3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Aquatic Pollution</topic><topic>Calibration</topic><topic>Chemical compounds</topic><topic>Chromatography</topic><topic>Chromatography, Affinity - 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In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%-95.95% of the diazinon from water and soil with CVs of 5.08%-8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%-81.58%); however, it effectively clean up the soil samples.</abstract><cop>New York</cop><pub>New York : Springer-Verlag</pub><pmid>19590806</pmid><doi>10.1007/s00128-009-9823-4</doi><tpages>4</tpages></addata></record> |
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subjects | Aquatic Pollution Calibration Chemical compounds Chromatography Chromatography, Affinity - instrumentation Chromatography, Affinity - methods Chromatography, High Pressure Liquid - methods Diazinon - analysis Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Fungicides Insecticides Limit of Detection Liquid chromatography Pesticides Pesticides - analysis Pollution Pretreatment of water Soil contamination Soil Pollutants - analysis Soil Science & Conservation Soils Waste Water Technology Water Management Water Pollutants, Chemical - analysis Water pollution Water Pollution Control |
title | Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples |
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