Determination of Antimony in Soil Samples by Flow-Through Stripping Chronopotentiometry with a Microporous Mercury-Film Electrode
Antimony in soil samples using flow-through stripping chronopotentiometry with a microporous mercury film electrode is determined. The soil samples namely, Cambisols and Orthic Luvisols are obtained from the monitoring localities in Slovakia and Geological Institute of UK Bratislava, Slovakia from a...
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| Veröffentlicht in: | Polish journal of environmental studies 2007-01, Vol.16 (4), p.607-607 |
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| creator | Manova, A Strelec, M Beinrohr, E |
| description | Antimony in soil samples using flow-through stripping chronopotentiometry with a microporous mercury film electrode is determined. The soil samples namely, Cambisols and Orthic Luvisols are obtained from the monitoring localities in Slovakia and Geological Institute of UK Bratislava, Slovakia from a depth of 50-100 cm. The samples are detected by graphite furnace atomic absorption spectrometry. The limit of detection (LOD) and limit of quantification (LOQ) are found to be 0.6 mu dm super(-3) and 1.7 mu g dm super(-3), respectively. The efficiency of the deposition of antimony on electrode depends on the deposition potential. The highest recoveries are observed in the region of -900 to -1100 mV and deposition efficiency increases with increase in the concentration of hydrochloric acid (HCl). A linear response is observed in the concentration range of 1 to 200 mu g dm super(-3). |
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The soil samples namely, Cambisols and Orthic Luvisols are obtained from the monitoring localities in Slovakia and Geological Institute of UK Bratislava, Slovakia from a depth of 50-100 cm. The samples are detected by graphite furnace atomic absorption spectrometry. The limit of detection (LOD) and limit of quantification (LOQ) are found to be 0.6 mu dm super(-3) and 1.7 mu g dm super(-3), respectively. The efficiency of the deposition of antimony on electrode depends on the deposition potential. The highest recoveries are observed in the region of -900 to -1100 mV and deposition efficiency increases with increase in the concentration of hydrochloric acid (HCl). 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The soil samples namely, Cambisols and Orthic Luvisols are obtained from the monitoring localities in Slovakia and Geological Institute of UK Bratislava, Slovakia from a depth of 50-100 cm. The samples are detected by graphite furnace atomic absorption spectrometry. The limit of detection (LOD) and limit of quantification (LOQ) are found to be 0.6 mu dm super(-3) and 1.7 mu g dm super(-3), respectively. The efficiency of the deposition of antimony on electrode depends on the deposition potential. The highest recoveries are observed in the region of -900 to -1100 mV and deposition efficiency increases with increase in the concentration of hydrochloric acid (HCl). A linear response is observed in the concentration range of 1 to 200 mu g dm super(-3).</description><subject>Absorption</subject><subject>Antimony</subject><subject>Electrodes</subject><subject>Mercury</subject><subject>Q1</subject><subject>Soil</subject><subject>Spectrometry</subject><issn>1230-1485</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqFULtOwzAUzQASpfAPd2KL5EcTJ2NVWkBqxdAyV4573Rg5drBdVRn5cyzBznSk89LRuSlmlHFS0kVT3RX3MX4SQhtS17Pi-xkThsE4mYx34DUsXTKDdxMYB3tvLOzlMFqM0E2wsf5aHvrgL-ce9imYcTTuDKvMOD_6hDnrB0xhgqtJPUjYGRWykhMRdhjUJUzlxtgB1hZVCv6ED8Wtljbi4x_Oi4_N-rB6LbfvL2-r5bYcGRWpRNHJU0cVZ6xWRAnktWxoVXHeImpRdS1ZaFKpRhOKJySZowvSMaYrzRUVfF48_faOwX9dMKbjYKJCa6XDvO7ISCM4rdt_jflFRkTD-Q8-ZGyO</recordid><startdate>20070101</startdate><enddate>20070101</enddate><creator>Manova, A</creator><creator>Strelec, M</creator><creator>Beinrohr, E</creator><scope>7ST</scope><scope>C1K</scope><scope>SOI</scope></search><sort><creationdate>20070101</creationdate><title>Determination of Antimony in Soil Samples by Flow-Through Stripping Chronopotentiometry with a Microporous Mercury-Film Electrode</title><author>Manova, A ; Strelec, M ; Beinrohr, E</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p217t-e7badb1c3226c0c7e36a8155339eef75b904f05c8f01ede0ef7140b22f5f3c173</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Absorption</topic><topic>Antimony</topic><topic>Electrodes</topic><topic>Mercury</topic><topic>Q1</topic><topic>Soil</topic><topic>Spectrometry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Manova, A</creatorcontrib><creatorcontrib>Strelec, M</creatorcontrib><creatorcontrib>Beinrohr, E</creatorcontrib><collection>Environment Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Environment Abstracts</collection><jtitle>Polish journal of environmental studies</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Manova, A</au><au>Strelec, M</au><au>Beinrohr, E</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of Antimony in Soil Samples by Flow-Through Stripping Chronopotentiometry with a Microporous Mercury-Film Electrode</atitle><jtitle>Polish journal of environmental studies</jtitle><date>2007-01-01</date><risdate>2007</risdate><volume>16</volume><issue>4</issue><spage>607</spage><epage>607</epage><pages>607-607</pages><issn>1230-1485</issn><abstract>Antimony in soil samples using flow-through stripping chronopotentiometry with a microporous mercury film electrode is determined. The soil samples namely, Cambisols and Orthic Luvisols are obtained from the monitoring localities in Slovakia and Geological Institute of UK Bratislava, Slovakia from a depth of 50-100 cm. The samples are detected by graphite furnace atomic absorption spectrometry. The limit of detection (LOD) and limit of quantification (LOQ) are found to be 0.6 mu dm super(-3) and 1.7 mu g dm super(-3), respectively. The efficiency of the deposition of antimony on electrode depends on the deposition potential. The highest recoveries are observed in the region of -900 to -1100 mV and deposition efficiency increases with increase in the concentration of hydrochloric acid (HCl). A linear response is observed in the concentration range of 1 to 200 mu g dm super(-3).</abstract><tpages>1</tpages></addata></record> |
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| subjects | Absorption Antimony Electrodes Mercury Q1 Soil Spectrometry |
| title | Determination of Antimony in Soil Samples by Flow-Through Stripping Chronopotentiometry with a Microporous Mercury-Film Electrode |
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