One-step method for quantitative and qualitative analysis of fatty acids in marine animal samples
In the one-step method, fatty acid methyl esters (FAMEs) have been prepared without prior lipid extraction. Each oyster, clam, and squid sample was esterified with 14% boron-trifluoride (BF 3) in methanol at 100 °C for 120 min, and hexane was used to help dissolve the lipids. This method gave a high...
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| Veröffentlicht in: | Journal of experimental marine biology and ecology 2008-01, Vol.354 (1), p.1-8 |
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| container_title | Journal of experimental marine biology and ecology |
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| creator | Abdulkadir, Sakdullah Tsuchiya, Makoto |
| description | In the one-step method, fatty acid methyl esters (FAMEs) have been prepared without prior lipid extraction. Each oyster, clam, and squid sample was esterified with 14% boron-trifluoride (BF
3) in methanol at 100 °C for 120 min, and hexane was used to help dissolve the lipids. This method gave a higher recovery of fatty acids as compared to the conventional method. Using an internal standard, the fatty acid content of the sample can be determined quantitatively and qualitatively. Due to its simplicity, speed, and reduced organic solvent usage, the one-step method should be useful for the determination of fatty acid composition in marine biological samples. |
| doi_str_mv | 10.1016/j.jembe.2007.08.024 |
| format | Article |
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| ispartof | Journal of experimental marine biology and ecology, 2008-01, Vol.354 (1), p.1-8 |
| issn | 0022-0981 1879-1697 |
| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Animal and plant ecology Animal, plant and microbial ecology Biological and medical sciences Clam Fatty acids Fundamental and applied biological sciences. Psychology Gas chromatography Invertebrates Marine Mollusca One-step method Oyster Sea water ecosystems Squid Synecology |
| title | One-step method for quantitative and qualitative analysis of fatty acids in marine animal samples |
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