Analysis of cyanobacterial-derived saxitoxins using high-performance ion exchange chromatography with chemical oxidation/fluorescence detection

A single run HPLC method utilizing ion exchange as the separation mode with a novel mobile phase system coupled to chemical postcolumn oxidation and fluorescence detection has been developed and demonstrated to be applicable to the quantitative analysis of paralytic shellfish poisons (PSPs) produced...

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Veröffentlicht in:	Environmental toxicology 2005-12, Vol.20 (6), p.549-559
Hauptverfasser:	Papageorgiou, J, Nicholson, B.C, Linke, T.A, Kapralos, C
Format:	Artikel
Sprache:	eng
Schlagworte:	Anabaena - chemistry Anabaena circinalis Animal, plant and microbial ecology Applied ecology Australia Bacterial Toxins - analysis Bacterial Toxins - chemistry Bacterial Toxins - isolation & purification Biological and medical sciences carbamate toxins chemical oxidation chemical structure Chromatography, High Pressure Liquid - methods Chromatography, Ion Exchange - methods Cyanobacteria cyanobacterial paralytic shellfish poisons (PSPs) Cylindrospermopsis - chemistry decarbamoyl toxins Ecotoxicology, biological effects of pollution fluorescence fluorescence detection Fresh Water - chemistry Fundamental and applied biological sciences. Psychology General aspects high performance liquid chromatography high-performance ion exchange chromatography (HPIC) ion exchange chromatography Marine Toxins - analysis Marine Toxins - chemistry Marine Toxins - isolation & purification Microcystins n-sulfocarbamoys toxins oxidation Oxidation-Reduction paralytic shellfish poisoning reservoir water reservoirs Saxitoxin - analysis Saxitoxin - chemistry Saxitoxin - isolation & purification saxitoxins Spectrometry, Fluorescence Water Pollutants, Chemical - analysis Water Pollutants, Chemical - isolation & purification water quality
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