Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment
Objectives The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite. Materials and methods Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, V...
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| creator | Strasser, Thomas Preis, Verena Behr, Michael Rosentritt, Martin |
| description | Objectives
The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite.
Materials and methods
Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, Vita, D; E.max CAD, Ivoclar-Vivadent, FL; E.max ZirCAD, Ivoclar-Vivadent, FL; Vita Enamic, Vita, D; Cerasmart, GC, B; LAVA Ultimate, 3M, D; SHOFU Block HC, SHOFU, US; Grandio Blocs, VOCO, D; BRILLIANT Crios, Coltene, CH) and pretreated to represent clinical procedures (Hf 20 s/5%; phosphoric acid 20 s/37%; Monobond etch and prime (Ivoclar-Vivadent, FL); water-cooled diamond bur (80 μm; 4 μm); Al
2
O
3
-blasting (50 μm/1 bar, 50 μm/2 bar, 120 μm/1 bar, 120 μm/2 bar); untreated; manufacturer’s instructions). SEM-analysis (Phenom, FEI, NL) of the surfaces was performed (magnifications ≤ 10,000×). Roughness values
R
a
,
R
z
(KJ 3D, Keyence, J), and surface energy SE (OCA15 plus, SCA20, DataPhysics, D) were determined (statistics: non-parametric Mann-Whitney
U
test/Kruskal-Wallis test for independent specimen,
α
= 0.05).
Results
Kruskal-Wallis revealed significant (
p
|
| doi_str_mv | 10.1007/s00784-018-2365-6 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1995155410</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1995155410</sourcerecordid><originalsourceid>FETCH-LOGICAL-c438t-521dbfab835a4e6b4ef63c7e421d373fec6ffc2a3274b58dbbd9daa1dec970543</originalsourceid><addsrcrecordid>eNp1kF1LwzAUhoMobn78AG-k4I0Xq8tX0_Zy1E-YCKLXIU1O6sbazqS92L83s3OI4E1yOOc5b8KD0AXBNwTjdOrDkfEYkyymTCSxOEBjwpmIWZqSw--axiLPyAideL_EmHCRsmM0ojnHPCN4jORr21cfDXg_iXzvrNIQQQOu2kwi1ZjQW4OzC71Qq8ioWlXgo9ZGxex2Wsyeo1p14MLMR8qGah_ROVBdDU13ho5sGMP57j5F7_d3b8VjPH95eCpm81hzlnVxQokprSozligOouRgBdMp8NBnKbOghbWaKkZTXiaZKUuTG6WIAZ2nOOHsFF0PuWvXfvbgO1kvvIbVSjXQ9l6SPE9IknCCA3r1B122vWvC77YUpzgPkgJFBkq71nsHVq7dolZuIwmWW_tysC-Dfbm1L0XYudwl92UNZr_xozsAdAB8GDUVuF9P_5v6BYcyj7g</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1994209673</pqid></control><display><type>article</type><title>Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment</title><source>MEDLINE</source><source>SpringerNature Journals</source><creator>Strasser, Thomas ; Preis, Verena ; Behr, Michael ; Rosentritt, Martin</creator><creatorcontrib>Strasser, Thomas ; Preis, Verena ; Behr, Michael ; Rosentritt, Martin</creatorcontrib><description>Objectives
The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite.
Materials and methods
Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, Vita, D; E.max CAD, Ivoclar-Vivadent, FL; E.max ZirCAD, Ivoclar-Vivadent, FL; Vita Enamic, Vita, D; Cerasmart, GC, B; LAVA Ultimate, 3M, D; SHOFU Block HC, SHOFU, US; Grandio Blocs, VOCO, D; BRILLIANT Crios, Coltene, CH) and pretreated to represent clinical procedures (Hf 20 s/5%; phosphoric acid 20 s/37%; Monobond etch and prime (Ivoclar-Vivadent, FL); water-cooled diamond bur (80 μm; 4 μm); Al
2
O
3
-blasting (50 μm/1 bar, 50 μm/2 bar, 120 μm/1 bar, 120 μm/2 bar); untreated; manufacturer’s instructions). SEM-analysis (Phenom, FEI, NL) of the surfaces was performed (magnifications ≤ 10,000×). Roughness values
R
a
,
R
z
(KJ 3D, Keyence, J), and surface energy SE (OCA15 plus, SCA20, DataPhysics, D) were determined (statistics: non-parametric Mann-Whitney
U
test/Kruskal-Wallis test for independent specimen,
α
= 0.05).
Results
Kruskal-Wallis revealed significant (
p
< 0.001) differences for all materials with different surface treatments. Roughness ranged from
R
a
= 0.05 μm (VS; D4)/
R
z
= 0.41 μm (VS; D4) to
R
a
= 1.82 μm (EMA; SB120/2)/
R
z
= 12.05 μm (CS; SB 120/2), SE from 22.7 mN/m (VE; M) to 52.8 mN/m (CD; M). SEM analysis showed material-dependent damages after pre-treatment.
Conclusion
Different CAD/CAM materials require individual pre-treatment for optimized and protective surface activation.
Clinical relevance
Cementation is a key factor for clinical success. Given the variety of available CAD/CAM materials, specific procedures are needed.</description><identifier>ISSN: 1432-6981</identifier><identifier>EISSN: 1436-3771</identifier><identifier>DOI: 10.1007/s00784-018-2365-6</identifier><identifier>PMID: 29404810</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Acid Etching, Dental ; Aluminum oxide ; Ceramics - chemistry ; Composite Resins - chemistry ; Computer-Aided Design ; Dental Materials - chemistry ; Dental Porcelain - chemistry ; Dentistry ; Materials Testing ; Medicine ; Microscopy, Electron, Scanning ; Original Article ; Phosphoric acid ; Statistical analysis ; Surface Properties ; Zirconia ; Zirconium - chemistry</subject><ispartof>Clinical oral investigations, 2018-11, Vol.22 (8), p.2787-2797</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2018</rights><rights>Clinical Oral Investigations is a copyright of Springer, (2018). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c438t-521dbfab835a4e6b4ef63c7e421d373fec6ffc2a3274b58dbbd9daa1dec970543</citedby><cites>FETCH-LOGICAL-c438t-521dbfab835a4e6b4ef63c7e421d373fec6ffc2a3274b58dbbd9daa1dec970543</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00784-018-2365-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00784-018-2365-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,782,786,27933,27934,41497,42566,51328</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/29404810$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Strasser, Thomas</creatorcontrib><creatorcontrib>Preis, Verena</creatorcontrib><creatorcontrib>Behr, Michael</creatorcontrib><creatorcontrib>Rosentritt, Martin</creatorcontrib><title>Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment</title><title>Clinical oral investigations</title><addtitle>Clin Oral Invest</addtitle><addtitle>Clin Oral Investig</addtitle><description>Objectives
The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite.
Materials and methods
Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, Vita, D; E.max CAD, Ivoclar-Vivadent, FL; E.max ZirCAD, Ivoclar-Vivadent, FL; Vita Enamic, Vita, D; Cerasmart, GC, B; LAVA Ultimate, 3M, D; SHOFU Block HC, SHOFU, US; Grandio Blocs, VOCO, D; BRILLIANT Crios, Coltene, CH) and pretreated to represent clinical procedures (Hf 20 s/5%; phosphoric acid 20 s/37%; Monobond etch and prime (Ivoclar-Vivadent, FL); water-cooled diamond bur (80 μm; 4 μm); Al
2
O
3
-blasting (50 μm/1 bar, 50 μm/2 bar, 120 μm/1 bar, 120 μm/2 bar); untreated; manufacturer’s instructions). SEM-analysis (Phenom, FEI, NL) of the surfaces was performed (magnifications ≤ 10,000×). Roughness values
R
a
,
R
z
(KJ 3D, Keyence, J), and surface energy SE (OCA15 plus, SCA20, DataPhysics, D) were determined (statistics: non-parametric Mann-Whitney
U
test/Kruskal-Wallis test for independent specimen,
α
= 0.05).
Results
Kruskal-Wallis revealed significant (
p
< 0.001) differences for all materials with different surface treatments. Roughness ranged from
R
a
= 0.05 μm (VS; D4)/
R
z
= 0.41 μm (VS; D4) to
R
a
= 1.82 μm (EMA; SB120/2)/
R
z
= 12.05 μm (CS; SB 120/2), SE from 22.7 mN/m (VE; M) to 52.8 mN/m (CD; M). SEM analysis showed material-dependent damages after pre-treatment.
Conclusion
Different CAD/CAM materials require individual pre-treatment for optimized and protective surface activation.
Clinical relevance
Cementation is a key factor for clinical success. Given the variety of available CAD/CAM materials, specific procedures are needed.</description><subject>Acid Etching, Dental</subject><subject>Aluminum oxide</subject><subject>Ceramics - chemistry</subject><subject>Composite Resins - chemistry</subject><subject>Computer-Aided Design</subject><subject>Dental Materials - chemistry</subject><subject>Dental Porcelain - chemistry</subject><subject>Dentistry</subject><subject>Materials Testing</subject><subject>Medicine</subject><subject>Microscopy, Electron, Scanning</subject><subject>Original Article</subject><subject>Phosphoric acid</subject><subject>Statistical analysis</subject><subject>Surface Properties</subject><subject>Zirconia</subject><subject>Zirconium - chemistry</subject><issn>1432-6981</issn><issn>1436-3771</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp1kF1LwzAUhoMobn78AG-k4I0Xq8tX0_Zy1E-YCKLXIU1O6sbazqS92L83s3OI4E1yOOc5b8KD0AXBNwTjdOrDkfEYkyymTCSxOEBjwpmIWZqSw--axiLPyAideL_EmHCRsmM0ojnHPCN4jORr21cfDXg_iXzvrNIQQQOu2kwi1ZjQW4OzC71Qq8ioWlXgo9ZGxex2Wsyeo1p14MLMR8qGah_ROVBdDU13ho5sGMP57j5F7_d3b8VjPH95eCpm81hzlnVxQokprSozligOouRgBdMp8NBnKbOghbWaKkZTXiaZKUuTG6WIAZ2nOOHsFF0PuWvXfvbgO1kvvIbVSjXQ9l6SPE9IknCCA3r1B122vWvC77YUpzgPkgJFBkq71nsHVq7dolZuIwmWW_tysC-Dfbm1L0XYudwl92UNZr_xozsAdAB8GDUVuF9P_5v6BYcyj7g</recordid><startdate>20181101</startdate><enddate>20181101</enddate><creator>Strasser, Thomas</creator><creator>Preis, Verena</creator><creator>Behr, Michael</creator><creator>Rosentritt, Martin</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>8AO</scope><scope>8C1</scope><scope>8FE</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>LK8</scope><scope>M0S</scope><scope>M1P</scope><scope>M7P</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope></search><sort><creationdate>20181101</creationdate><title>Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment</title><author>Strasser, Thomas ; Preis, Verena ; Behr, Michael ; Rosentritt, Martin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c438t-521dbfab835a4e6b4ef63c7e421d373fec6ffc2a3274b58dbbd9daa1dec970543</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Acid Etching, Dental</topic><topic>Aluminum oxide</topic><topic>Ceramics - chemistry</topic><topic>Composite Resins - chemistry</topic><topic>Computer-Aided Design</topic><topic>Dental Materials - chemistry</topic><topic>Dental Porcelain - chemistry</topic><topic>Dentistry</topic><topic>Materials Testing</topic><topic>Medicine</topic><topic>Microscopy, Electron, Scanning</topic><topic>Original Article</topic><topic>Phosphoric acid</topic><topic>Statistical analysis</topic><topic>Surface Properties</topic><topic>Zirconia</topic><topic>Zirconium - chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Strasser, Thomas</creatorcontrib><creatorcontrib>Preis, Verena</creatorcontrib><creatorcontrib>Behr, Michael</creatorcontrib><creatorcontrib>Rosentritt, Martin</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Medical Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>Public Health Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>ProQuest Biological Science Collection</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Biological Science Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><jtitle>Clinical oral investigations</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Strasser, Thomas</au><au>Preis, Verena</au><au>Behr, Michael</au><au>Rosentritt, Martin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment</atitle><jtitle>Clinical oral investigations</jtitle><stitle>Clin Oral Invest</stitle><addtitle>Clin Oral Investig</addtitle><date>2018-11-01</date><risdate>2018</risdate><volume>22</volume><issue>8</issue><spage>2787</spage><epage>2797</epage><pages>2787-2797</pages><issn>1432-6981</issn><eissn>1436-3771</eissn><abstract>Objectives
The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite.
Materials and methods
Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, Vita, D; E.max CAD, Ivoclar-Vivadent, FL; E.max ZirCAD, Ivoclar-Vivadent, FL; Vita Enamic, Vita, D; Cerasmart, GC, B; LAVA Ultimate, 3M, D; SHOFU Block HC, SHOFU, US; Grandio Blocs, VOCO, D; BRILLIANT Crios, Coltene, CH) and pretreated to represent clinical procedures (Hf 20 s/5%; phosphoric acid 20 s/37%; Monobond etch and prime (Ivoclar-Vivadent, FL); water-cooled diamond bur (80 μm; 4 μm); Al
2
O
3
-blasting (50 μm/1 bar, 50 μm/2 bar, 120 μm/1 bar, 120 μm/2 bar); untreated; manufacturer’s instructions). SEM-analysis (Phenom, FEI, NL) of the surfaces was performed (magnifications ≤ 10,000×). Roughness values
R
a
,
R
z
(KJ 3D, Keyence, J), and surface energy SE (OCA15 plus, SCA20, DataPhysics, D) were determined (statistics: non-parametric Mann-Whitney
U
test/Kruskal-Wallis test for independent specimen,
α
= 0.05).
Results
Kruskal-Wallis revealed significant (
p
< 0.001) differences for all materials with different surface treatments. Roughness ranged from
R
a
= 0.05 μm (VS; D4)/
R
z
= 0.41 μm (VS; D4) to
R
a
= 1.82 μm (EMA; SB120/2)/
R
z
= 12.05 μm (CS; SB 120/2), SE from 22.7 mN/m (VE; M) to 52.8 mN/m (CD; M). SEM analysis showed material-dependent damages after pre-treatment.
Conclusion
Different CAD/CAM materials require individual pre-treatment for optimized and protective surface activation.
Clinical relevance
Cementation is a key factor for clinical success. Given the variety of available CAD/CAM materials, specific procedures are needed.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>29404810</pmid><doi>10.1007/s00784-018-2365-6</doi><tpages>11</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1432-6981 |
| ispartof | Clinical oral investigations, 2018-11, Vol.22 (8), p.2787-2797 |
| issn | 1432-6981 1436-3771 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1995155410 |
| source | MEDLINE; SpringerNature Journals |
| subjects | Acid Etching, Dental Aluminum oxide Ceramics - chemistry Composite Resins - chemistry Computer-Aided Design Dental Materials - chemistry Dental Porcelain - chemistry Dentistry Materials Testing Medicine Microscopy, Electron, Scanning Original Article Phosphoric acid Statistical analysis Surface Properties Zirconia Zirconium - chemistry |
| title | Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment |
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