Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples
Sodium dodecyl sulfate coated amino‐functionalized magnetic iron oxide nanoparticles were used as an efficient adsorbent for rapid removal and preconcentration of three important organophosphorus pesticides, chlorpyrifos, diazinon and phosalone, by ultrasound‐assisted dispersive magnetic solid‐phase...
Gespeichert in:
| Veröffentlicht in: | Journal of separation science 2018-05, Vol.41 (9), p.2037-2045 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 2045 |
|---|---|
| container_issue | 9 |
| container_start_page | 2037 |
| container_title | Journal of separation science |
| container_volume | 41 |
| creator | Hamedi, Raheleh B.G. Aghaie, Ali Hadjmohammadi, Mohammad Reza |
| description | Sodium dodecyl sulfate coated amino‐functionalized magnetic iron oxide nanoparticles were used as an efficient adsorbent for rapid removal and preconcentration of three important organophosphorus pesticides, chlorpyrifos, diazinon and phosalone, by ultrasound‐assisted dispersive magnetic solid‐phase microextraction. Fabrication of amino‐functionalized magnetic nanoparticles was certified by characteristic analyses, including Fourier transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy, and transmission electron microscopy. Affecting parameters on the removal efficiency were investigated and optimized through half‐fractional factorial design and Doehlert design, respectively. The analysis of analytes was performed by high‐performance liquid chromatography with ultraviolet detection. Under the optimum conditions, extraction recoveries for 20 ng/mL of organophosphorus pesticides were in the range of 84–97% with preconcentration factors in the range of 134–155. Replicating the experiment in above condition for five times gave the relative standard deviations |
| doi_str_mv | 10.1002/jssc.201701090 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1993013278</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2047436564</sourcerecordid><originalsourceid>FETCH-LOGICAL-c4050-118d7de9bbdfc7c943567a712216c5f04842ef9071a2c890055b1ae31b3eca913</originalsourceid><addsrcrecordid>eNqFkU1v1DAQhi1ERUvhyhFZ4sJlt_5KHB_Rik-14lA4W44zbr1K4mAnW-3_4Ycyy5Y9cKlke0bWM--M5iXkDWdrzpi42pbi14JxzTgz7Bm54DWvVkZy9fyUs_qcvCxlyxBrDHtBzoWRWteiuSC_b9zdCHP01KcMdIge-h4KdXjo6MZUUm5hnGlImc73QCGE6OPhJ8OQdq6nbuww92kHeU9TQCoD0JTvsHq6TwVvXgqdoGCb2KF4yGnAZ4kz3S7Y8a8EjLuY0zigNIo-uBkyLW6YcJpX5Cy4vsDrx3hJfn76-GPzZXX9_fPXzYfrlVesYivOm053YNq2C157o2RVa6e5ELz2VWCqUQKCYZo74XERrKpa7kDyVoJ3hstL8v6oO-X0a8F57RDLYSFuhLQUyw0uk0uhG0Tf_Ydu05JHnM4KprSSdVUrpNZHyudUSoZgpxwHl_eWM3vwzx78syf_sODto-zSDtCd8H-GIaCOwEPsYf-EnP12e7upjGDyD6t5qcs</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2047436564</pqid></control><display><type>article</type><title>Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples</title><source>Wiley Online Library All Journals</source><creator>Hamedi, Raheleh ; B.G. Aghaie, Ali ; Hadjmohammadi, Mohammad Reza</creator><creatorcontrib>Hamedi, Raheleh ; B.G. Aghaie, Ali ; Hadjmohammadi, Mohammad Reza</creatorcontrib><description>Sodium dodecyl sulfate coated amino‐functionalized magnetic iron oxide nanoparticles were used as an efficient adsorbent for rapid removal and preconcentration of three important organophosphorus pesticides, chlorpyrifos, diazinon and phosalone, by ultrasound‐assisted dispersive magnetic solid‐phase microextraction. Fabrication of amino‐functionalized magnetic nanoparticles was certified by characteristic analyses, including Fourier transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy, and transmission electron microscopy. Affecting parameters on the removal efficiency were investigated and optimized through half‐fractional factorial design and Doehlert design, respectively. The analysis of analytes was performed by high‐performance liquid chromatography with ultraviolet detection. Under the optimum conditions, extraction recoveries for 20 ng/mL of organophosphorus pesticides were in the range of 84–97% with preconcentration factors in the range of 134–155. Replicating the experiment in above condition for five times gave the relative standard deviations <6%. The calibration curves showed high linearity in the range of 0.2–700 ng/mL and the limits of detection were in the range of 0.08–0.13 ng/mL. The proposed method was successfully applied for both removal and trace determination of these three organophosphorus pesticides in environmental water and fruit juice samples.</description><identifier>ISSN: 1615-9306</identifier><identifier>EISSN: 1615-9314</identifier><identifier>DOI: 10.1002/jssc.201701090</identifier><identifier>PMID: 29377628</identifier><language>eng</language><publisher>Germany: Wiley Subscription Services, Inc</publisher><subject>Chlorpyrifos ; Design analysis ; Design optimization ; Doehlert design ; Fourier transforms ; Fractional factorial design ; Infrared analysis ; Iron oxides ; Linearity ; Liquid chromatography ; magnetic core micelle ; magnetic solid‐phase microextraction ; Microscopy ; Nanoparticles ; organophosphorus pesticides ; Pesticides ; Replicating ; Scanning electron microscopy ; Sodium dodecyl sulfate ; Thermogravimetric analysis ; Transmission electron microscopy</subject><ispartof>Journal of separation science, 2018-05, Vol.41 (9), p.2037-2045</ispartof><rights>2018 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim</rights><rights>2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4050-118d7de9bbdfc7c943567a712216c5f04842ef9071a2c890055b1ae31b3eca913</citedby><cites>FETCH-LOGICAL-c4050-118d7de9bbdfc7c943567a712216c5f04842ef9071a2c890055b1ae31b3eca913</cites><orcidid>0000-0003-2558-6426</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fjssc.201701090$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fjssc.201701090$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/29377628$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hamedi, Raheleh</creatorcontrib><creatorcontrib>B.G. Aghaie, Ali</creatorcontrib><creatorcontrib>Hadjmohammadi, Mohammad Reza</creatorcontrib><title>Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples</title><title>Journal of separation science</title><addtitle>J Sep Sci</addtitle><description>Sodium dodecyl sulfate coated amino‐functionalized magnetic iron oxide nanoparticles were used as an efficient adsorbent for rapid removal and preconcentration of three important organophosphorus pesticides, chlorpyrifos, diazinon and phosalone, by ultrasound‐assisted dispersive magnetic solid‐phase microextraction. Fabrication of amino‐functionalized magnetic nanoparticles was certified by characteristic analyses, including Fourier transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy, and transmission electron microscopy. Affecting parameters on the removal efficiency were investigated and optimized through half‐fractional factorial design and Doehlert design, respectively. The analysis of analytes was performed by high‐performance liquid chromatography with ultraviolet detection. Under the optimum conditions, extraction recoveries for 20 ng/mL of organophosphorus pesticides were in the range of 84–97% with preconcentration factors in the range of 134–155. Replicating the experiment in above condition for five times gave the relative standard deviations <6%. The calibration curves showed high linearity in the range of 0.2–700 ng/mL and the limits of detection were in the range of 0.08–0.13 ng/mL. The proposed method was successfully applied for both removal and trace determination of these three organophosphorus pesticides in environmental water and fruit juice samples.</description><subject>Chlorpyrifos</subject><subject>Design analysis</subject><subject>Design optimization</subject><subject>Doehlert design</subject><subject>Fourier transforms</subject><subject>Fractional factorial design</subject><subject>Infrared analysis</subject><subject>Iron oxides</subject><subject>Linearity</subject><subject>Liquid chromatography</subject><subject>magnetic core micelle</subject><subject>magnetic solid‐phase microextraction</subject><subject>Microscopy</subject><subject>Nanoparticles</subject><subject>organophosphorus pesticides</subject><subject>Pesticides</subject><subject>Replicating</subject><subject>Scanning electron microscopy</subject><subject>Sodium dodecyl sulfate</subject><subject>Thermogravimetric analysis</subject><subject>Transmission electron microscopy</subject><issn>1615-9306</issn><issn>1615-9314</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNqFkU1v1DAQhi1ERUvhyhFZ4sJlt_5KHB_Rik-14lA4W44zbr1K4mAnW-3_4Ycyy5Y9cKlke0bWM--M5iXkDWdrzpi42pbi14JxzTgz7Bm54DWvVkZy9fyUs_qcvCxlyxBrDHtBzoWRWteiuSC_b9zdCHP01KcMdIge-h4KdXjo6MZUUm5hnGlImc73QCGE6OPhJ8OQdq6nbuww92kHeU9TQCoD0JTvsHq6TwVvXgqdoGCb2KF4yGnAZ4kz3S7Y8a8EjLuY0zigNIo-uBkyLW6YcJpX5Cy4vsDrx3hJfn76-GPzZXX9_fPXzYfrlVesYivOm053YNq2C157o2RVa6e5ELz2VWCqUQKCYZo74XERrKpa7kDyVoJ3hstL8v6oO-X0a8F57RDLYSFuhLQUyw0uk0uhG0Tf_Ydu05JHnM4KprSSdVUrpNZHyudUSoZgpxwHl_eWM3vwzx78syf_sODto-zSDtCd8H-GIaCOwEPsYf-EnP12e7upjGDyD6t5qcs</recordid><startdate>201805</startdate><enddate>201805</enddate><creator>Hamedi, Raheleh</creator><creator>B.G. Aghaie, Ali</creator><creator>Hadjmohammadi, Mohammad Reza</creator><general>Wiley Subscription Services, Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0003-2558-6426</orcidid></search><sort><creationdate>201805</creationdate><title>Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples</title><author>Hamedi, Raheleh ; B.G. Aghaie, Ali ; Hadjmohammadi, Mohammad Reza</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4050-118d7de9bbdfc7c943567a712216c5f04842ef9071a2c890055b1ae31b3eca913</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Chlorpyrifos</topic><topic>Design analysis</topic><topic>Design optimization</topic><topic>Doehlert design</topic><topic>Fourier transforms</topic><topic>Fractional factorial design</topic><topic>Infrared analysis</topic><topic>Iron oxides</topic><topic>Linearity</topic><topic>Liquid chromatography</topic><topic>magnetic core micelle</topic><topic>magnetic solid‐phase microextraction</topic><topic>Microscopy</topic><topic>Nanoparticles</topic><topic>organophosphorus pesticides</topic><topic>Pesticides</topic><topic>Replicating</topic><topic>Scanning electron microscopy</topic><topic>Sodium dodecyl sulfate</topic><topic>Thermogravimetric analysis</topic><topic>Transmission electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hamedi, Raheleh</creatorcontrib><creatorcontrib>B.G. Aghaie, Ali</creatorcontrib><creatorcontrib>Hadjmohammadi, Mohammad Reza</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of separation science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hamedi, Raheleh</au><au>B.G. Aghaie, Ali</au><au>Hadjmohammadi, Mohammad Reza</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples</atitle><jtitle>Journal of separation science</jtitle><addtitle>J Sep Sci</addtitle><date>2018-05</date><risdate>2018</risdate><volume>41</volume><issue>9</issue><spage>2037</spage><epage>2045</epage><pages>2037-2045</pages><issn>1615-9306</issn><eissn>1615-9314</eissn><abstract>Sodium dodecyl sulfate coated amino‐functionalized magnetic iron oxide nanoparticles were used as an efficient adsorbent for rapid removal and preconcentration of three important organophosphorus pesticides, chlorpyrifos, diazinon and phosalone, by ultrasound‐assisted dispersive magnetic solid‐phase microextraction. Fabrication of amino‐functionalized magnetic nanoparticles was certified by characteristic analyses, including Fourier transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy, and transmission electron microscopy. Affecting parameters on the removal efficiency were investigated and optimized through half‐fractional factorial design and Doehlert design, respectively. The analysis of analytes was performed by high‐performance liquid chromatography with ultraviolet detection. Under the optimum conditions, extraction recoveries for 20 ng/mL of organophosphorus pesticides were in the range of 84–97% with preconcentration factors in the range of 134–155. Replicating the experiment in above condition for five times gave the relative standard deviations <6%. The calibration curves showed high linearity in the range of 0.2–700 ng/mL and the limits of detection were in the range of 0.08–0.13 ng/mL. The proposed method was successfully applied for both removal and trace determination of these three organophosphorus pesticides in environmental water and fruit juice samples.</abstract><cop>Germany</cop><pub>Wiley Subscription Services, Inc</pub><pmid>29377628</pmid><doi>10.1002/jssc.201701090</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0003-2558-6426</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1615-9306 |
| ispartof | Journal of separation science, 2018-05, Vol.41 (9), p.2037-2045 |
| issn | 1615-9306 1615-9314 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1993013278 |
| source | Wiley Online Library All Journals |
| subjects | Chlorpyrifos Design analysis Design optimization Doehlert design Fourier transforms Fractional factorial design Infrared analysis Iron oxides Linearity Liquid chromatography magnetic core micelle magnetic solid‐phase microextraction Microscopy Nanoparticles organophosphorus pesticides Pesticides Replicating Scanning electron microscopy Sodium dodecyl sulfate Thermogravimetric analysis Transmission electron microscopy |
| title | Magnetic core micelles as a nanosorbent for the efficient removal and recovery of three organophosphorus pesticides from fruit juice and environmental water samples |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-01T08%3A01%3A08IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Magnetic%20core%20micelles%20as%20a%20nanosorbent%20for%20the%20efficient%20removal%20and%20recovery%20of%20three%20organophosphorus%20pesticides%20from%20fruit%20juice%20and%20environmental%20water%20samples&rft.jtitle=Journal%20of%20separation%20science&rft.au=Hamedi,%20Raheleh&rft.date=2018-05&rft.volume=41&rft.issue=9&rft.spage=2037&rft.epage=2045&rft.pages=2037-2045&rft.issn=1615-9306&rft.eissn=1615-9314&rft_id=info:doi/10.1002/jssc.201701090&rft_dat=%3Cproquest_cross%3E2047436564%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2047436564&rft_id=info:pmid/29377628&rfr_iscdi=true |