Structural characterization of the new synthetic cannabinoids CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA and CUMYL-4CN-B7AICA
•Five new synthetic cannabinoids containing a cumyl moiety are characterized.•Constitutional isomers 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA are differentiated.•Constitutional isomers CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are differentiated. Synthetic cannabinoids are a group of new psychoactive compoun...
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| Veröffentlicht in: | Forensic science international 2017-12, Vol.281, p.98-105 |
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| creator | Bovens, Michael Bissig, Christian Staeheli, Sandra N. Poetzsch, Michael Pfeiffer, Bernhard Kraemer, Thomas |
| description | •Five new synthetic cannabinoids containing a cumyl moiety are characterized.•Constitutional isomers 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA are differentiated.•Constitutional isomers CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are differentiated.
Synthetic cannabinoids are a group of new psychoactive compounds (NPS) that act as agonists at the cannabinoid receptor. First reported in 2008, they currently represent one of the largest groups of NPS that are monitored by the European Monitoring Centre for Drugs and Drug Addiction (EMCDDA). Five samples (4 from the European RESPONSE project and one from daily casework) containing different synthetic cannabinoids were analyzed by a complex of analytical methods including gas chromatography–electron ionization mass spectrometry (GC–EI-MS), liquid chromatography–high resolution mass spectrometry (LC–HRMS), infrared spectroscopy (IR) and nuclear magnetic resonance spectroscopy (NMR). Five new synthetic cannabinoids containing a cumyl moiety as a linked group were identified: CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA, CUMYL-4CN-B7AICA. 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA as well as CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are constitutional isomers and only differ in the position of a nitrogen atom. The article contains all analytical data for a proper identification and differentiation of the five cumyl compounds. |
| doi_str_mv | 10.1016/j.forsciint.2017.10.020 |
| format | Article |
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Synthetic cannabinoids are a group of new psychoactive compounds (NPS) that act as agonists at the cannabinoid receptor. First reported in 2008, they currently represent one of the largest groups of NPS that are monitored by the European Monitoring Centre for Drugs and Drug Addiction (EMCDDA). Five samples (4 from the European RESPONSE project and one from daily casework) containing different synthetic cannabinoids were analyzed by a complex of analytical methods including gas chromatography–electron ionization mass spectrometry (GC–EI-MS), liquid chromatography–high resolution mass spectrometry (LC–HRMS), infrared spectroscopy (IR) and nuclear magnetic resonance spectroscopy (NMR). Five new synthetic cannabinoids containing a cumyl moiety as a linked group were identified: CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA, CUMYL-4CN-B7AICA. 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA as well as CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are constitutional isomers and only differ in the position of a nitrogen atom. The article contains all analytical data for a proper identification and differentiation of the five cumyl compounds.</description><identifier>ISSN: 0379-0738</identifier><identifier>EISSN: 1872-6283</identifier><identifier>DOI: 10.1016/j.forsciint.2017.10.020</identifier><identifier>PMID: 29125990</identifier><language>eng</language><publisher>Ireland: Elsevier B.V</publisher><subject>5F-CUMYL-P7AICA ; 5F-CUMYL-PINACA ; Analytical methods ; Cannabinoid receptors ; Cannabinoids ; CUMYL-4CN-B7AICA ; CUMYL-4CN-BINACA ; CUMYL-PINACA ; Data processing ; Drug abuse ; Drug addiction ; Drug testing ; Drugs ; Forensic sciences ; Gas chromatography ; Identification ; Infrared spectroscopy ; Ionization ; Isomers ; Laboratories ; Liquid chromatography ; Magnetic resonance spectroscopy ; Mass spectrometry ; Mass spectroscopy ; Metabolism ; Metabolites ; Names ; NMR ; Nuclear magnetic resonance ; Spectroscopy ; Structural analysis ; Synthetic cannabinoids ; Trends ; Urine</subject><ispartof>Forensic science international, 2017-12, Vol.281, p.98-105</ispartof><rights>2017 Elsevier B.V.</rights><rights>Copyright © 2017 Elsevier B.V. All rights reserved.</rights><rights>Copyright Elsevier Limited Dec 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c399t-61c6b406c9e26a5e376c65543a17cad77b6ad601ee08c5295c3768823d437fe03</citedby><cites>FETCH-LOGICAL-c399t-61c6b406c9e26a5e376c65543a17cad77b6ad601ee08c5295c3768823d437fe03</cites><orcidid>0000-0002-3283-606X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.proquest.com/docview/1973105863?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993,64383,64385,64387,72239</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/29125990$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Bovens, Michael</creatorcontrib><creatorcontrib>Bissig, Christian</creatorcontrib><creatorcontrib>Staeheli, Sandra N.</creatorcontrib><creatorcontrib>Poetzsch, Michael</creatorcontrib><creatorcontrib>Pfeiffer, Bernhard</creatorcontrib><creatorcontrib>Kraemer, Thomas</creatorcontrib><title>Structural characterization of the new synthetic cannabinoids CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA and CUMYL-4CN-B7AICA</title><title>Forensic science international</title><addtitle>Forensic Sci Int</addtitle><description>•Five new synthetic cannabinoids containing a cumyl moiety are characterized.•Constitutional isomers 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA are differentiated.•Constitutional isomers CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are differentiated.
Synthetic cannabinoids are a group of new psychoactive compounds (NPS) that act as agonists at the cannabinoid receptor. First reported in 2008, they currently represent one of the largest groups of NPS that are monitored by the European Monitoring Centre for Drugs and Drug Addiction (EMCDDA). Five samples (4 from the European RESPONSE project and one from daily casework) containing different synthetic cannabinoids were analyzed by a complex of analytical methods including gas chromatography–electron ionization mass spectrometry (GC–EI-MS), liquid chromatography–high resolution mass spectrometry (LC–HRMS), infrared spectroscopy (IR) and nuclear magnetic resonance spectroscopy (NMR). Five new synthetic cannabinoids containing a cumyl moiety as a linked group were identified: CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA, CUMYL-4CN-B7AICA. 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA as well as CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are constitutional isomers and only differ in the position of a nitrogen atom. The article contains all analytical data for a proper identification and differentiation of the five cumyl compounds.</description><subject>5F-CUMYL-P7AICA</subject><subject>5F-CUMYL-PINACA</subject><subject>Analytical methods</subject><subject>Cannabinoid receptors</subject><subject>Cannabinoids</subject><subject>CUMYL-4CN-B7AICA</subject><subject>CUMYL-4CN-BINACA</subject><subject>CUMYL-PINACA</subject><subject>Data processing</subject><subject>Drug abuse</subject><subject>Drug addiction</subject><subject>Drug testing</subject><subject>Drugs</subject><subject>Forensic sciences</subject><subject>Gas chromatography</subject><subject>Identification</subject><subject>Infrared spectroscopy</subject><subject>Ionization</subject><subject>Isomers</subject><subject>Laboratories</subject><subject>Liquid chromatography</subject><subject>Magnetic resonance spectroscopy</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Metabolism</subject><subject>Metabolites</subject><subject>Names</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Spectroscopy</subject><subject>Structural analysis</subject><subject>Synthetic 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characterization of the new synthetic cannabinoids CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA and CUMYL-4CN-B7AICA</title><author>Bovens, Michael ; Bissig, Christian ; Staeheli, Sandra N. ; Poetzsch, Michael ; Pfeiffer, Bernhard ; Kraemer, Thomas</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c399t-61c6b406c9e26a5e376c65543a17cad77b6ad601ee08c5295c3768823d437fe03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>5F-CUMYL-P7AICA</topic><topic>5F-CUMYL-PINACA</topic><topic>Analytical methods</topic><topic>Cannabinoid receptors</topic><topic>Cannabinoids</topic><topic>CUMYL-4CN-B7AICA</topic><topic>CUMYL-4CN-BINACA</topic><topic>CUMYL-PINACA</topic><topic>Data processing</topic><topic>Drug abuse</topic><topic>Drug addiction</topic><topic>Drug testing</topic><topic>Drugs</topic><topic>Forensic sciences</topic><topic>Gas chromatography</topic><topic>Identification</topic><topic>Infrared spectroscopy</topic><topic>Ionization</topic><topic>Isomers</topic><topic>Laboratories</topic><topic>Liquid chromatography</topic><topic>Magnetic resonance spectroscopy</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Metabolism</topic><topic>Metabolites</topic><topic>Names</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Spectroscopy</topic><topic>Structural analysis</topic><topic>Synthetic cannabinoids</topic><topic>Trends</topic><topic>Urine</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bovens, Michael</creatorcontrib><creatorcontrib>Bissig, Christian</creatorcontrib><creatorcontrib>Staeheli, Sandra N.</creatorcontrib><creatorcontrib>Poetzsch, Michael</creatorcontrib><creatorcontrib>Pfeiffer, Bernhard</creatorcontrib><creatorcontrib>Kraemer, 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CUMYL-4CN-B7AICA</atitle><jtitle>Forensic science international</jtitle><addtitle>Forensic Sci Int</addtitle><date>2017-12</date><risdate>2017</risdate><volume>281</volume><spage>98</spage><epage>105</epage><pages>98-105</pages><issn>0379-0738</issn><eissn>1872-6283</eissn><abstract>•Five new synthetic cannabinoids containing a cumyl moiety are characterized.•Constitutional isomers 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA are differentiated.•Constitutional isomers CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are differentiated.
Synthetic cannabinoids are a group of new psychoactive compounds (NPS) that act as agonists at the cannabinoid receptor. First reported in 2008, they currently represent one of the largest groups of NPS that are monitored by the European Monitoring Centre for Drugs and Drug Addiction (EMCDDA). Five samples (4 from the European RESPONSE project and one from daily casework) containing different synthetic cannabinoids were analyzed by a complex of analytical methods including gas chromatography–electron ionization mass spectrometry (GC–EI-MS), liquid chromatography–high resolution mass spectrometry (LC–HRMS), infrared spectroscopy (IR) and nuclear magnetic resonance spectroscopy (NMR). Five new synthetic cannabinoids containing a cumyl moiety as a linked group were identified: CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA, CUMYL-4CN-B7AICA. 5F-CUMYL-PINACA and 5F-CUMYL-P7AICA as well as CUMYL-4CN-BINACA and CUMYL-4CN-B7AICA are constitutional isomers and only differ in the position of a nitrogen atom. The article contains all analytical data for a proper identification and differentiation of the five cumyl compounds.</abstract><cop>Ireland</cop><pub>Elsevier B.V</pub><pmid>29125990</pmid><doi>10.1016/j.forsciint.2017.10.020</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0002-3283-606X</orcidid></addata></record> |
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| ispartof | Forensic science international, 2017-12, Vol.281, p.98-105 |
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| source | ScienceDirect Journals (5 years ago - present); ProQuest Central UK/Ireland |
| subjects | 5F-CUMYL-P7AICA 5F-CUMYL-PINACA Analytical methods Cannabinoid receptors Cannabinoids CUMYL-4CN-B7AICA CUMYL-4CN-BINACA CUMYL-PINACA Data processing Drug abuse Drug addiction Drug testing Drugs Forensic sciences Gas chromatography Identification Infrared spectroscopy Ionization Isomers Laboratories Liquid chromatography Magnetic resonance spectroscopy Mass spectrometry Mass spectroscopy Metabolism Metabolites Names NMR Nuclear magnetic resonance Spectroscopy Structural analysis Synthetic cannabinoids Trends Urine |
| title | Structural characterization of the new synthetic cannabinoids CUMYL-PINACA, 5F-CUMYL-PINACA, CUMYL-4CN-BINACA, 5F-CUMYL-P7AICA and CUMYL-4CN-B7AICA |
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