Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria
LC–MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set t...
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| Veröffentlicht in: | Environmental pollution (1987) 2007-07, Vol.148 (2), p.570-579 |
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| container_title | Environmental pollution (1987) |
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| creator | Martínez-Carballo, Elena González-Barreiro, Carmen Scharf, Sigrid Gans, Oliver |
| description | LC–MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set to 100
μg/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46
mg/kg chlortetracycline, 29
mg/kg oxytetracycline and 23
mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91
mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study.
Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria. |
| doi_str_mv | 10.1016/j.envpol.2006.11.035 |
| format | Article |
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μg/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46
mg/kg chlortetracycline, 29
mg/kg oxytetracycline and 23
mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91
mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study.
Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria.</description><identifier>ISSN: 0269-7491</identifier><identifier>EISSN: 1873-6424</identifier><identifier>DOI: 10.1016/j.envpol.2006.11.035</identifier><identifier>PMID: 17291647</identifier><identifier>CODEN: ENVPAF</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Agriculture, rearing and food industries wastes ; Agronomy. Soil science and plant productions ; Animal manure ; Animals ; Anti-Infective Agents - analysis ; Antineoplastic Agents - analysis ; Applied sciences ; Austria ; Biological and medical sciences ; Biological and physicochemical properties of pollutants. Interaction in the soil ; Chickens ; Ciprofloxacin - analysis ; Earth sciences ; Earth, ocean, space ; Engineering and environment geology. Geothermics ; Environmental Monitoring - methods ; Environmental Pollutants - analysis ; Exact sciences and technology ; Fluoroquinolones - analysis ; Fundamental and applied biological sciences. Psychology ; Liquid chromatography/tandem mass spectrometry ; Manure - analysis ; Pollution ; Pollution, environment geology ; Soil ; Soil - analysis ; Soil and sediments pollution ; Soil and water pollution ; Soil Pollutants - analysis ; Soil science ; Sulfonamides - analysis ; Swine ; Tetracyclines - analysis ; Trimethoprim - analysis ; Turkeys ; Veterinary antibiotics ; Wastes</subject><ispartof>Environmental pollution (1987), 2007-07, Vol.148 (2), p.570-579</ispartof><rights>2006 Elsevier Ltd</rights><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a541t-d8f96e91f5f7c3afef092b89fb8f011e9fe3e7d8bfdeb621f29eba1f8dce8bb33</citedby><cites>FETCH-LOGICAL-a541t-d8f96e91f5f7c3afef092b89fb8f011e9fe3e7d8bfdeb621f29eba1f8dce8bb33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0269749106006816$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18834423$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17291647$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Martínez-Carballo, Elena</creatorcontrib><creatorcontrib>González-Barreiro, Carmen</creatorcontrib><creatorcontrib>Scharf, Sigrid</creatorcontrib><creatorcontrib>Gans, Oliver</creatorcontrib><title>Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria</title><title>Environmental pollution (1987)</title><addtitle>Environ Pollut</addtitle><description>LC–MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set to 100
μg/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46
mg/kg chlortetracycline, 29
mg/kg oxytetracycline and 23
mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91
mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study.
Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria.</description><subject>Agriculture, rearing and food industries wastes</subject><subject>Agronomy. Soil science and plant productions</subject><subject>Animal manure</subject><subject>Animals</subject><subject>Anti-Infective Agents - analysis</subject><subject>Antineoplastic Agents - analysis</subject><subject>Applied sciences</subject><subject>Austria</subject><subject>Biological and medical sciences</subject><subject>Biological and physicochemical properties of pollutants. Interaction in the soil</subject><subject>Chickens</subject><subject>Ciprofloxacin - analysis</subject><subject>Earth sciences</subject><subject>Earth, ocean, space</subject><subject>Engineering and environment geology. Geothermics</subject><subject>Environmental Monitoring - methods</subject><subject>Environmental Pollutants - analysis</subject><subject>Exact sciences and technology</subject><subject>Fluoroquinolones - analysis</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Liquid chromatography/tandem mass spectrometry</subject><subject>Manure - analysis</subject><subject>Pollution</subject><subject>Pollution, environment geology</subject><subject>Soil</subject><subject>Soil - analysis</subject><subject>Soil and sediments pollution</subject><subject>Soil and water pollution</subject><subject>Soil Pollutants - analysis</subject><subject>Soil science</subject><subject>Sulfonamides - analysis</subject><subject>Swine</subject><subject>Tetracyclines - analysis</subject><subject>Trimethoprim - analysis</subject><subject>Turkeys</subject><subject>Veterinary antibiotics</subject><subject>Wastes</subject><issn>0269-7491</issn><issn>1873-6424</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkcGKFDEQhoMo7uzqG4j0RW_dpjrp7uQiLMu6Cgte9BzSSWXJ0JOMSXpg3n4zzsDe9BSK-v4iVR8hH4B2QGH8su0wHPZx6XpKxw6go2x4RTYgJtaOvOevyYb2o2wnLuGKXOe8pZRyxthbcgVTL2Hk04Y83YeDTzHsMBS9NLsYfInJh6cml9Uem-iajAuagrY5YMHa0unY6FD87GPxJjc-1NLvTmkd1oS1sk2Ofvnbul1zSV6_I2-cXjK-v7w35Pe3-19339vHnw8_7m4fWz1wKK0VTo4owQ1uMkw7dFT2s5BuFo4CoHTIcLJidhbnsQfXS5w1OGENinlm7IZ8Ps_dp_hnxVzUzmeDy6IDxjUrkMPE-DD8H-QCuOSygvwMmhRzTujUPtVt01EBVScTaqvOJtTJhAJQ1USNfbzMX-cd2pfQ5fQV-HQBdDZ6cUkH4_MLJwTjvD9t9PXMYT3bwWNS2XgMBq1P1Yuy0f_7J8_UuKyd</recordid><startdate>20070701</startdate><enddate>20070701</enddate><creator>Martínez-Carballo, Elena</creator><creator>González-Barreiro, Carmen</creator><creator>Scharf, Sigrid</creator><creator>Gans, Oliver</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7ST</scope><scope>C1K</scope><scope>SOI</scope><scope>7TV</scope><scope>7U7</scope></search><sort><creationdate>20070701</creationdate><title>Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria</title><author>Martínez-Carballo, Elena ; González-Barreiro, Carmen ; Scharf, Sigrid ; Gans, Oliver</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a541t-d8f96e91f5f7c3afef092b89fb8f011e9fe3e7d8bfdeb621f29eba1f8dce8bb33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Agriculture, rearing and food industries wastes</topic><topic>Agronomy. Soil science and plant productions</topic><topic>Animal manure</topic><topic>Animals</topic><topic>Anti-Infective Agents - analysis</topic><topic>Antineoplastic Agents - analysis</topic><topic>Applied sciences</topic><topic>Austria</topic><topic>Biological and medical sciences</topic><topic>Biological and physicochemical properties of pollutants. Interaction in the soil</topic><topic>Chickens</topic><topic>Ciprofloxacin - analysis</topic><topic>Earth sciences</topic><topic>Earth, ocean, space</topic><topic>Engineering and environment geology. Geothermics</topic><topic>Environmental Monitoring - methods</topic><topic>Environmental Pollutants - analysis</topic><topic>Exact sciences and technology</topic><topic>Fluoroquinolones - analysis</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Liquid chromatography/tandem mass spectrometry</topic><topic>Manure - analysis</topic><topic>Pollution</topic><topic>Pollution, environment geology</topic><topic>Soil</topic><topic>Soil - analysis</topic><topic>Soil and sediments pollution</topic><topic>Soil and water pollution</topic><topic>Soil Pollutants - analysis</topic><topic>Soil science</topic><topic>Sulfonamides - analysis</topic><topic>Swine</topic><topic>Tetracyclines - analysis</topic><topic>Trimethoprim - analysis</topic><topic>Turkeys</topic><topic>Veterinary antibiotics</topic><topic>Wastes</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Martínez-Carballo, Elena</creatorcontrib><creatorcontrib>González-Barreiro, Carmen</creatorcontrib><creatorcontrib>Scharf, Sigrid</creatorcontrib><creatorcontrib>Gans, Oliver</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Environment Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Environment Abstracts</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><jtitle>Environmental pollution (1987)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Martínez-Carballo, Elena</au><au>González-Barreiro, Carmen</au><au>Scharf, Sigrid</au><au>Gans, Oliver</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria</atitle><jtitle>Environmental pollution (1987)</jtitle><addtitle>Environ Pollut</addtitle><date>2007-07-01</date><risdate>2007</risdate><volume>148</volume><issue>2</issue><spage>570</spage><epage>579</epage><pages>570-579</pages><issn>0269-7491</issn><eissn>1873-6424</eissn><coden>ENVPAF</coden><abstract>LC–MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set to 100
μg/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46
mg/kg chlortetracycline, 29
mg/kg oxytetracycline and 23
mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91
mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study.
Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><pmid>17291647</pmid><doi>10.1016/j.envpol.2006.11.035</doi><tpages>10</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0269-7491 |
| ispartof | Environmental pollution (1987), 2007-07, Vol.148 (2), p.570-579 |
| issn | 0269-7491 1873-6424 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_19573455 |
| source | MEDLINE; ScienceDirect Journals (5 years ago - present) |
| subjects | Agriculture, rearing and food industries wastes Agronomy. Soil science and plant productions Animal manure Animals Anti-Infective Agents - analysis Antineoplastic Agents - analysis Applied sciences Austria Biological and medical sciences Biological and physicochemical properties of pollutants. Interaction in the soil Chickens Ciprofloxacin - analysis Earth sciences Earth, ocean, space Engineering and environment geology. Geothermics Environmental Monitoring - methods Environmental Pollutants - analysis Exact sciences and technology Fluoroquinolones - analysis Fundamental and applied biological sciences. Psychology Liquid chromatography/tandem mass spectrometry Manure - analysis Pollution Pollution, environment geology Soil Soil - analysis Soil and sediments pollution Soil and water pollution Soil Pollutants - analysis Soil science Sulfonamides - analysis Swine Tetracyclines - analysis Trimethoprim - analysis Turkeys Veterinary antibiotics Wastes |
| title | Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria |
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