Identification of atractyloside by LC–ESI–MS in alleged herbal poisonings

An LC–MS screening method was developed to detect the presence of atractyloside (ATR), the toxic principle of a commonly used medicinal plant in South Africa, Callilepis laureola, in biological matrices such as body fluids and human viscera.

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Bibliographische Detailangaben
Veröffentlicht in:	Forensic science international 2006-11, Vol.163 (1), p.81-92
Hauptverfasser:	Steenkamp, P.A., Harding, N.M., van Heerden, F.R., van Wyk, B.-E.
Format:	Artikel
Sprache:	eng
Schlagworte:	Asteraceae Atractylodes Atractyloside Atractyloside - analysis Atractyloside - poisoning Biological and medical sciences Body Fluids - chemistry Callilepis - chemistry Callilepis - poisoning Callilepis laureola Carboxyatractyloside Chemistry, Forensic Chromatography Chromatography, Liquid Forensic chemistry Forensic medicine Forensic Pathology Forensic sciences General aspects Herbal medicine High performance liquid chromatography HPLC Humans Identification and classification Investigative techniques, diagnostic techniques (general aspects) LC–MS Mass spectrometry Medical sciences Methods Plant Extracts - chemistry Plant Extracts - poisoning Plant Poisoning - diagnosis Plant Poisoning - pathology Plant Roots - chemistry Poisoning Public health. Hygiene Public health. Hygiene-occupational medicine Spectrometry, Mass, Electrospray Ionization Studies Viscera - chemistry
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Beschreibung
Zusammenfassung:	An LC–MS screening method was developed to detect the presence of atractyloside (ATR), the toxic principle of a commonly used medicinal plant in South Africa, Callilepis laureola, in biological matrices such as body fluids and human viscera.
ISSN:	0379-0738 1872-6283
DOI:	10.1016/j.forsciint.2005.11.010