Semiautomated determination of neonicotinoids and characteristic metabolite in urine samples using TurboFlow™ coupled to ultra high performance liquid chromatography coupled to Orbitrap analyzer

[Display omitted] •Seven neonicotinoids and one metabolite have been determined by LC-Orbitrap.•Two online extraction systems were evaluated: TurboFlow™ and SPE.•Thirty six urine samples were analyzed by the developed method.•Three neonicotinoids and one metabolite were detected in urine samples. A...

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Veröffentlicht in:	Journal of pharmaceutical and biomedical analysis 2017-11, Vol.146, p.378-386
Hauptverfasser:	López-García, Marina, Romero-González, Roberto, Lacasaña, Marina, Garrido Frenich, Antonia
Format:	Artikel
Sprache:	eng
Schlagworte:	Chromatography, High Pressure Liquid - methods Female Humans Insecticides - chemistry Insecticides - urine Limit of Detection Metabolite Neonicotinoids Neonicotinoids - chemistry Neonicotinoids - urine Online SPE Orbitrap Pregnancy Reproducibility of Results Solid Phase Extraction - methods Spain Tandem Mass Spectrometry - methods TurboFlow Urine Urine - chemistry
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