Physical characterization using diffusion NMR spectroscopy
NMR diffusion measurements (or dNMR) provide a powerful tool for analysis of solution organization and microgeometry of the environment by probing random molecular motion. Being a very versatile method, dNMR can be applied to a large variety of samples and systems. Here, a brief introduction into dN...
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| Veröffentlicht in: | Magnetic resonance in chemistry 2017-05, Vol.55 (5), p.414-424 |
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| container_title | Magnetic resonance in chemistry |
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| creator | Zubkov, Mikhail Dennis, Gary R. Stait‐Gardner, Tim Torres, Allan M. Willis, Scott A. Zheng, Gang Price, William S. |
| description | NMR diffusion measurements (or dNMR) provide a powerful tool for analysis of solution organization and microgeometry of the environment by probing random molecular motion. Being a very versatile method, dNMR can be applied to a large variety of samples and systems. Here, a brief introduction into dNMR and a summary of recent advances in the field are presented. The research topics include restricted diffusion, anisotropic diffusion, polymer dynamics, solution structuring and dNMR method development. The dNMR studied systems include plants, cells (cell models), liquid crystals, polymer solutions, ionic liquids, supercooled solutions, untreated water, amino acid solutions and more. It is demonstrated how a variety of dNMR methods can be applied to a system to extract the data on particular structures present among, formed by or surrounding the diffusing particles. It is also demonstrated how dNMR methods can be developed to allow probing larger geometries, low sample concentrations and faster processes. Copyright © 2016 John Wiley & Sons, Ltd.
The article represents the recent advances in studying the interactions and structuring of the solutions as well as the methods of probing the molecular environment by diffusion NMR. An overview of recent advances in diffusion NMR method development is also presented. |
| doi_str_mv | 10.1002/mrc.4530 |
| format | Article |
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The article represents the recent advances in studying the interactions and structuring of the solutions as well as the methods of probing the molecular environment by diffusion NMR. An overview of recent advances in diffusion NMR method development is also presented.</description><identifier>ISSN: 0749-1581</identifier><identifier>EISSN: 1097-458X</identifier><identifier>DOI: 10.1002/mrc.4530</identifier><identifier>PMID: 27657736</identifier><language>eng</language><publisher>England: Wiley Subscription Services, Inc</publisher><subject>Amino acids ; anisotropic diffusion ; Chain dynamics ; Diffusion ; diffusion NMR ; Dynamic structural analysis ; Dynamical systems ; hydrogen bonding ; Ionic liquids ; isomer diffusion ; Liquid crystals ; Mathematical models ; Molecular motion ; NMR spectroscopy ; Nuclear magnetic resonance ; polymer dynamics ; restricted diffusion ; solution structuring ; Spectroscopic analysis</subject><ispartof>Magnetic resonance in chemistry, 2017-05, Vol.55 (5), p.414-424</ispartof><rights>Copyright © 2016 John Wiley & Sons, Ltd.</rights><rights>Copyright © 2017 John Wiley & Sons, Ltd.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4100-9be547f45936700cffd392eb4dcdb4f931bf1bf39657cf16f5db8cab628be3753</citedby><cites>FETCH-LOGICAL-c4100-9be547f45936700cffd392eb4dcdb4f931bf1bf39657cf16f5db8cab628be3753</cites><orcidid>0000-0002-8549-4665</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fmrc.4530$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fmrc.4530$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,777,781,1413,27906,27907,45556,45557</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/27657736$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Zubkov, Mikhail</creatorcontrib><creatorcontrib>Dennis, Gary R.</creatorcontrib><creatorcontrib>Stait‐Gardner, Tim</creatorcontrib><creatorcontrib>Torres, Allan M.</creatorcontrib><creatorcontrib>Willis, Scott A.</creatorcontrib><creatorcontrib>Zheng, Gang</creatorcontrib><creatorcontrib>Price, William S.</creatorcontrib><title>Physical characterization using diffusion NMR spectroscopy</title><title>Magnetic resonance in chemistry</title><addtitle>Magn Reson Chem</addtitle><description>NMR diffusion measurements (or dNMR) provide a powerful tool for analysis of solution organization and microgeometry of the environment by probing random molecular motion. Being a very versatile method, dNMR can be applied to a large variety of samples and systems. Here, a brief introduction into dNMR and a summary of recent advances in the field are presented. The research topics include restricted diffusion, anisotropic diffusion, polymer dynamics, solution structuring and dNMR method development. The dNMR studied systems include plants, cells (cell models), liquid crystals, polymer solutions, ionic liquids, supercooled solutions, untreated water, amino acid solutions and more. It is demonstrated how a variety of dNMR methods can be applied to a system to extract the data on particular structures present among, formed by or surrounding the diffusing particles. It is also demonstrated how dNMR methods can be developed to allow probing larger geometries, low sample concentrations and faster processes. Copyright © 2016 John Wiley & Sons, Ltd.
The article represents the recent advances in studying the interactions and structuring of the solutions as well as the methods of probing the molecular environment by diffusion NMR. An overview of recent advances in diffusion NMR method development is also presented.</description><subject>Amino acids</subject><subject>anisotropic diffusion</subject><subject>Chain dynamics</subject><subject>Diffusion</subject><subject>diffusion NMR</subject><subject>Dynamic structural analysis</subject><subject>Dynamical systems</subject><subject>hydrogen bonding</subject><subject>Ionic liquids</subject><subject>isomer diffusion</subject><subject>Liquid crystals</subject><subject>Mathematical models</subject><subject>Molecular motion</subject><subject>NMR spectroscopy</subject><subject>Nuclear magnetic resonance</subject><subject>polymer dynamics</subject><subject>restricted diffusion</subject><subject>solution structuring</subject><subject>Spectroscopic analysis</subject><issn>0749-1581</issn><issn>1097-458X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqNkV1LwzAUhoMobk7BXyAFb7zpTJqkSbyT4RdsKkPBu9Cmievol0mL1F9v5qaCoAgHzjnw8J6PF4BDBMcIwui0tGpMKIZbYIigYCGh_GkbDCEjIkSUowHYc24JIRSC4V0wiFhMGcPxEJzdL3qXq6QI1CKxiWq1zd-SNq-roHN59RxkuTG-8v3tbB64RqvW1k7VTb8PdkxSOH2wySPweHnxMLkOp3dXN5PzaaiIXy4UqaaEGUIFjhmEypgMi0inJFNZSozAKDU-sPArKYNiQ7OUqySNI55qzCgegZO1bmPrl067Vpa5U7ookkrXnZOICyygQBj_A8WUYI4j6NHjH-iy7mzlD5FIIBr5yRH_k-IccyIIjL_HKv8aZ7WRjc3LxPYSQbkySHqD5Mogjx5tBLu01NkX-OmIB8I18JoXuv9VSM7mkw_BdwaRl8M</recordid><startdate>201705</startdate><enddate>201705</enddate><creator>Zubkov, Mikhail</creator><creator>Dennis, Gary R.</creator><creator>Stait‐Gardner, Tim</creator><creator>Torres, Allan M.</creator><creator>Willis, Scott A.</creator><creator>Zheng, Gang</creator><creator>Price, William S.</creator><general>Wiley Subscription Services, Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>JQ2</scope><scope>K9.</scope><scope>L7M</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0002-8549-4665</orcidid></search><sort><creationdate>201705</creationdate><title>Physical characterization using diffusion NMR spectroscopy</title><author>Zubkov, Mikhail ; 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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Amino acids anisotropic diffusion Chain dynamics Diffusion diffusion NMR Dynamic structural analysis Dynamical systems hydrogen bonding Ionic liquids isomer diffusion Liquid crystals Mathematical models Molecular motion NMR spectroscopy Nuclear magnetic resonance polymer dynamics restricted diffusion solution structuring Spectroscopic analysis |
| title | Physical characterization using diffusion NMR spectroscopy |
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