Preparation and investigation of Ga5[GeSx]85I10 glasses
The Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 are prepared; their thermal and optical properties and stability against crystallization are investigated. The values of glass transition temperature, energy bandgap and volume fraction of crystalline phase in glasses after annealing have...
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| Veröffentlicht in: | Journal of non-crystalline solids 2017-02, Vol.457, p.60-64 |
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| container_title | Journal of non-crystalline solids |
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| creator | Velmuzhov, A.P. Sukhanov, M.V. Plekhovich, A.D. Shiryaev, V.S. Churbanov, M.F. |
| description | The Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 are prepared; their thermal and optical properties and stability against crystallization are investigated. The values of glass transition temperature, energy bandgap and volume fraction of crystalline phase in glasses after annealing have nonmonotonic dependence on the macro-composition with a maximum value at x=2.0. In the DSC curves of glasses with x=2.0, 2.3 and 2.6, two glass transition temperatures are registered. The glass samples containing 1.2ppm(at) hydrogen impurity in the form of SH-group and |
| doi_str_mv | 10.1016/j.jnoncrysol.2016.11.027 |
| format | Article |
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•The pure Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 were prepared.•The thermal, optical and crystallization properties of Ga5[GeSx]85I10 glasses were investigated.•The glasses in the Ga5[GeSx]85I10 system with low tendency to crystallization were determined.•The single-index Ga5[GeS1.5]85I10 and Ga5[GeS1.7]85I10 glass fibers were drawn.</description><identifier>ISSN: 0022-3093</identifier><identifier>EISSN: 1873-4812</identifier><identifier>DOI: 10.1016/j.jnoncrysol.2016.11.027</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Annealing ; Chalcoiodide Ga-Ge-S-I glasses ; Crystal structure ; Crystallization ; Glass ; Glass transition temperature ; Impurities ; Optical properties ; Stability ; Stability against crystallization ; Synthesis ; Thermal properties ; Transmittance</subject><ispartof>Journal of non-crystalline solids, 2017-02, Vol.457, p.60-64</ispartof><rights>2016 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c266t-d9efaf441184a56453fdca09e42a2e8ec2f65d10e77ba97af9151ed4b49722af3</citedby><cites>FETCH-LOGICAL-c266t-d9efaf441184a56453fdca09e42a2e8ec2f65d10e77ba97af9151ed4b49722af3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0022309316305257$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids></links><search><creatorcontrib>Velmuzhov, A.P.</creatorcontrib><creatorcontrib>Sukhanov, M.V.</creatorcontrib><creatorcontrib>Plekhovich, A.D.</creatorcontrib><creatorcontrib>Shiryaev, V.S.</creatorcontrib><creatorcontrib>Churbanov, M.F.</creatorcontrib><title>Preparation and investigation of Ga5[GeSx]85I10 glasses</title><title>Journal of non-crystalline solids</title><description>The Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 are prepared; their thermal and optical properties and stability against crystallization are investigated. The values of glass transition temperature, energy bandgap and volume fraction of crystalline phase in glasses after annealing have nonmonotonic dependence on the macro-composition with a maximum value at x=2.0. In the DSC curves of glasses with x=2.0, 2.3 and 2.6, two glass transition temperatures are registered. The glass samples containing 1.2ppm(at) hydrogen impurity in the form of SH-group and <1ppm(at) oxygen impurity in the form of GeO were produced.
•The pure Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 were prepared.•The thermal, optical and crystallization properties of Ga5[GeSx]85I10 glasses were investigated.•The glasses in the Ga5[GeSx]85I10 system with low tendency to crystallization were determined.•The single-index Ga5[GeS1.5]85I10 and Ga5[GeS1.7]85I10 glass fibers were drawn.</description><subject>Annealing</subject><subject>Chalcoiodide Ga-Ge-S-I glasses</subject><subject>Crystal structure</subject><subject>Crystallization</subject><subject>Glass</subject><subject>Glass transition temperature</subject><subject>Impurities</subject><subject>Optical properties</subject><subject>Stability</subject><subject>Stability against crystallization</subject><subject>Synthesis</subject><subject>Thermal properties</subject><subject>Transmittance</subject><issn>0022-3093</issn><issn>1873-4812</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqFkEFLAzEQhYMoWKv_YY9eds1ks5vkqEVroaCgnkRCmp2UlO2mJtti_70rK3h0LgOP9x4zHyEZ0AIo1DebYtOFzsZjCm3BBqUAKCgTJ2QCUpQ5l8BOyYRSxvKSqvKcXKS0ocOIUk6IeI64M9H0PnSZ6ZrMdwdMvV-PSnDZ3FTvc3z5-pDVAmi2bk1KmC7JmTNtwqvfPSVvD_evs8d8-TRfzG6XuWV13eeNQmcc5wCSm6rmVekaa6hCzgxDiZa5umqAohAro4RxCirAhq-4EowZV07J9di7i-FzP1ymtz5ZbFvTYdgnPfyolKoFk4NVjlYbQ0oRnd5FvzXxqIHqH1Z6o_9Y6R9WGkAPrIbo3RjF4ZWDx6iT9dhZbHxE2-sm-P9LvgFGEXeI</recordid><startdate>20170201</startdate><enddate>20170201</enddate><creator>Velmuzhov, A.P.</creator><creator>Sukhanov, M.V.</creator><creator>Plekhovich, A.D.</creator><creator>Shiryaev, V.S.</creator><creator>Churbanov, M.F.</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20170201</creationdate><title>Preparation and investigation of Ga5[GeSx]85I10 glasses</title><author>Velmuzhov, A.P. ; Sukhanov, M.V. ; Plekhovich, A.D. ; Shiryaev, V.S. ; Churbanov, M.F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c266t-d9efaf441184a56453fdca09e42a2e8ec2f65d10e77ba97af9151ed4b49722af3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Annealing</topic><topic>Chalcoiodide Ga-Ge-S-I glasses</topic><topic>Crystal structure</topic><topic>Crystallization</topic><topic>Glass</topic><topic>Glass transition temperature</topic><topic>Impurities</topic><topic>Optical properties</topic><topic>Stability</topic><topic>Stability against crystallization</topic><topic>Synthesis</topic><topic>Thermal properties</topic><topic>Transmittance</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Velmuzhov, A.P.</creatorcontrib><creatorcontrib>Sukhanov, M.V.</creatorcontrib><creatorcontrib>Plekhovich, A.D.</creatorcontrib><creatorcontrib>Shiryaev, V.S.</creatorcontrib><creatorcontrib>Churbanov, M.F.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of non-crystalline solids</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Velmuzhov, A.P.</au><au>Sukhanov, M.V.</au><au>Plekhovich, A.D.</au><au>Shiryaev, V.S.</au><au>Churbanov, M.F.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and investigation of Ga5[GeSx]85I10 glasses</atitle><jtitle>Journal of non-crystalline solids</jtitle><date>2017-02-01</date><risdate>2017</risdate><volume>457</volume><spage>60</spage><epage>64</epage><pages>60-64</pages><issn>0022-3093</issn><eissn>1873-4812</eissn><abstract>The Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 are prepared; their thermal and optical properties and stability against crystallization are investigated. The values of glass transition temperature, energy bandgap and volume fraction of crystalline phase in glasses after annealing have nonmonotonic dependence on the macro-composition with a maximum value at x=2.0. In the DSC curves of glasses with x=2.0, 2.3 and 2.6, two glass transition temperatures are registered. The glass samples containing 1.2ppm(at) hydrogen impurity in the form of SH-group and <1ppm(at) oxygen impurity in the form of GeO were produced.
•The pure Ga5[GeSx]85I10 glasses with x=1.5, 1.7, 2.0, 2.3 and 2.6 were prepared.•The thermal, optical and crystallization properties of Ga5[GeSx]85I10 glasses were investigated.•The glasses in the Ga5[GeSx]85I10 system with low tendency to crystallization were determined.•The single-index Ga5[GeS1.5]85I10 and Ga5[GeS1.7]85I10 glass fibers were drawn.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jnoncrysol.2016.11.027</doi><tpages>5</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Annealing Chalcoiodide Ga-Ge-S-I glasses Crystal structure Crystallization Glass Glass transition temperature Impurities Optical properties Stability Stability against crystallization Synthesis Thermal properties Transmittance |
| title | Preparation and investigation of Ga5[GeSx]85I10 glasses |
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