Quantitative elemental determination in water and oil by laser induced breakdown spectroscopy
Laser induced breakdown spectroscopy has been used to evaluate the potentiality of the technique for the determination of trace amounts of elements in different types of liquids, in the framework of nuclear applications. A specific set-up using a pulsed laser focussed with a tilted angle on the surf...
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| Veröffentlicht in: | Analytica chimica acta 2001-02, Vol.429 (2), p.269-278 |
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| container_title | Analytica chimica acta |
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| creator | Fichet, Pascal Mauchien, Patrick Wagner, Jean-François Moulin, Christophe |
| description | Laser induced breakdown spectroscopy has been used to evaluate the potentiality of the technique for the determination of trace amounts of elements in different types of liquids, in the framework of nuclear applications. A specific set-up using a pulsed laser focussed with a tilted angle on the surface of the liquid is presented. It allows on-line quantitative measurements with good reliability and reproducibility. Twelve elements (Pb, Si, Ca, Na, Zn, Sn, Al, Cu, Ni, Fe, Mg, Cr) have been studied in two different liquid matrices: water and oil. Detection limits (0.3–120
μg
ml
−1) and reproducibilities (ca. 3%) are reported. Moreover, the use of an echelle spectrometer for such elemental analysis is also proposed. |
| doi_str_mv | 10.1016/S0003-2670(00)01277-0 |
| format | Article |
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μg
ml
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μg
ml
−1) and reproducibilities (ca. 3%) are reported. Moreover, the use of an echelle spectrometer for such elemental analysis is also proposed.</description><subject>Analysis of liquids</subject><subject>Analytical chemistry</subject><subject>Atomic emission spectroscopy</subject><subject>Chemistry</subject><subject>Echelle spectrometer</subject><subject>Exact sciences and technology</subject><subject>Laser ablation</subject><subject>Laser induced breakdown spectroscopy</subject><subject>Spectrometric and optical methods</subject><issn>0003-2670</issn><issn>1873-4324</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2001</creationdate><recordtype>article</recordtype><recordid>eNqFkF1LwzAUhoMoOKc_QQgIohfVkyZNuyuR4RcMRNRLCWlyCtE2nUm3sX9v5oa3kkDIy3POSR5CThlcMWDy-hUAeJbLEi4ALoHlZZnBHhmxquSZ4LnYJ6M_5JAcxfiZrjkDMSIfLwvtBzfowS2RYosd-kG31OKAoXM-5b2nztOVTgHV3tLetbRe01bHFDhvFwYtrQPqL9uvPI1zNEPoo-nn62Ny0Og24snuHJP3-7u36WM2e354mt7OMsOlHLImRy50w_NJI0UtclkwIwwCqyeFKW0lpagYq7Uu02pYY5EDstoWppYTIS0fk_Nt33novxcYB9W5aLBttcd-EVUyUcKEQwKLLWjSC2PARs2D63RYKwZqI1P9ylQbUwrS3shUm7qz3QAdjW6boL1x8a-4KgvIRaJuthSmvy4dBhWNQ5_8uJCkKNu7f-b8AMbCih0</recordid><startdate>20010223</startdate><enddate>20010223</enddate><creator>Fichet, Pascal</creator><creator>Mauchien, Patrick</creator><creator>Wagner, Jean-François</creator><creator>Moulin, Christophe</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QH</scope></search><sort><creationdate>20010223</creationdate><title>Quantitative elemental determination in water and oil by laser induced breakdown spectroscopy</title><author>Fichet, Pascal ; Mauchien, Patrick ; Wagner, Jean-François ; Moulin, Christophe</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c366t-f2e34af329f64b42651c4ce01b95c7d8664811baa7a7af1fde30e1bd5cb6946d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2001</creationdate><topic>Analysis of liquids</topic><topic>Analytical chemistry</topic><topic>Atomic emission spectroscopy</topic><topic>Chemistry</topic><topic>Echelle spectrometer</topic><topic>Exact sciences and technology</topic><topic>Laser ablation</topic><topic>Laser induced breakdown spectroscopy</topic><topic>Spectrometric and optical methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fichet, Pascal</creatorcontrib><creatorcontrib>Mauchien, Patrick</creatorcontrib><creatorcontrib>Wagner, Jean-François</creatorcontrib><creatorcontrib>Moulin, Christophe</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Aqualine</collection><jtitle>Analytica chimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Fichet, Pascal</au><au>Mauchien, Patrick</au><au>Wagner, Jean-François</au><au>Moulin, Christophe</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Quantitative elemental determination in water and oil by laser induced breakdown spectroscopy</atitle><jtitle>Analytica chimica acta</jtitle><date>2001-02-23</date><risdate>2001</risdate><volume>429</volume><issue>2</issue><spage>269</spage><epage>278</epage><pages>269-278</pages><issn>0003-2670</issn><eissn>1873-4324</eissn><coden>ACACAM</coden><abstract>Laser induced breakdown spectroscopy has been used to evaluate the potentiality of the technique for the determination of trace amounts of elements in different types of liquids, in the framework of nuclear applications. A specific set-up using a pulsed laser focussed with a tilted angle on the surface of the liquid is presented. It allows on-line quantitative measurements with good reliability and reproducibility. Twelve elements (Pb, Si, Ca, Na, Zn, Sn, Al, Cu, Ni, Fe, Mg, Cr) have been studied in two different liquid matrices: water and oil. Detection limits (0.3–120
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ml
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| ispartof | Analytica chimica acta, 2001-02, Vol.429 (2), p.269-278 |
| issn | 0003-2670 1873-4324 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_18770930 |
| source | Elsevier ScienceDirect Journals |
| subjects | Analysis of liquids Analytical chemistry Atomic emission spectroscopy Chemistry Echelle spectrometer Exact sciences and technology Laser ablation Laser induced breakdown spectroscopy Spectrometric and optical methods |
| title | Quantitative elemental determination in water and oil by laser induced breakdown spectroscopy |
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