Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites
This study prepared Magnesium-Partially Stabilized Zirconia (Mg-PSZ) filler synthesis and direct foaming technique using egg whites, and impregnated by PMMA. The results were evaluated systematically by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Transmission Electron Microscope...
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| Veröffentlicht in: | Key engineering materials 2016-11, Vol.720, p.290-295 |
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| creator | Rudyawan, Alfend Takarini, Veni Hardiansyah, Andri Purwasasmita, Bambang Sunendar Djustiana, Nina Hasratiningsih, Zulia Septawendar, Rifki Prastomo, Niki |
| description | This study prepared Magnesium-Partially Stabilized Zirconia (Mg-PSZ) filler synthesis and direct foaming technique using egg whites, and impregnated by PMMA. The results were evaluated systematically by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Transmission Electron Microscope (TEM). XRD results denote that the powder sample of MgPSZ was successfully formed with various crystal size of tetragonal and monoclinic phase. SEM and TEM observations revealed that nanoparticles MgPSZ were in spherical and long rounded shapes. Furthermore, SEM observation revealed that the direct foaming method were also successful in the formation of porous structures which favourable for impregnation process by PMMA. The use of egg whites as a polymer precursor in both methods demonstrates that porous specimens contained nanosized, predominantly tetragonal, Mg-PSZ powders were successfully synthesized. This shall yield an interesting prospect towards cheap, reliable, and biocompatible product to resemble the modulus elasticity of dentin. |
| doi_str_mv | 10.4028/www.scientific.net/KEM.720.290 |
| format | Article |
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The results were evaluated systematically by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Transmission Electron Microscope (TEM). XRD results denote that the powder sample of MgPSZ was successfully formed with various crystal size of tetragonal and monoclinic phase. SEM and TEM observations revealed that nanoparticles MgPSZ were in spherical and long rounded shapes. Furthermore, SEM observation revealed that the direct foaming method were also successful in the formation of porous structures which favourable for impregnation process by PMMA. The use of egg whites as a polymer precursor in both methods demonstrates that porous specimens contained nanosized, predominantly tetragonal, Mg-PSZ powders were successfully synthesized. This shall yield an interesting prospect towards cheap, reliable, and biocompatible product to resemble the modulus elasticity of dentin.</description><identifier>ISSN: 1013-9826</identifier><identifier>ISSN: 1662-9795</identifier><identifier>ISBN: 3038357561</identifier><identifier>ISBN: 9783038357568</identifier><identifier>EISSN: 1662-9795</identifier><identifier>DOI: 10.4028/www.scientific.net/KEM.720.290</identifier><language>eng</language><publisher>Zurich: Trans Tech Publications Ltd</publisher><subject>Egg white ; Electron microscopes ; Foaming ; Nanostructure ; Polymethyl methacrylate ; Polymethyl methacrylates ; Prepolymers ; Scanning electron microscopy ; Sol-gel processes ; Synthesis ; Transmission electron microscopy ; X-ray diffraction</subject><ispartof>Key engineering materials, 2016-11, Vol.720, p.290-295</ispartof><rights>2017 Trans Tech Publications Ltd</rights><rights>Copyright Trans Tech Publications Ltd. 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The results were evaluated systematically by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Transmission Electron Microscope (TEM). XRD results denote that the powder sample of MgPSZ was successfully formed with various crystal size of tetragonal and monoclinic phase. SEM and TEM observations revealed that nanoparticles MgPSZ were in spherical and long rounded shapes. Furthermore, SEM observation revealed that the direct foaming method were also successful in the formation of porous structures which favourable for impregnation process by PMMA. The use of egg whites as a polymer precursor in both methods demonstrates that porous specimens contained nanosized, predominantly tetragonal, Mg-PSZ powders were successfully synthesized. This shall yield an interesting prospect towards cheap, reliable, and biocompatible product to resemble the modulus elasticity of dentin.</abstract><cop>Zurich</cop><pub>Trans Tech Publications Ltd</pub><doi>10.4028/www.scientific.net/KEM.720.290</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0002-9673-0766</orcidid></addata></record> |
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| subjects | Egg white Electron microscopes Foaming Nanostructure Polymethyl methacrylate Polymethyl methacrylates Prepolymers Scanning electron microscopy Sol-gel processes Synthesis Transmission electron microscopy X-ray diffraction |
| title | Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites |
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