Mercury Intrusion Porosimetry and Image Analysis of Cement-Based Materials
Mercury intrusion porosimetry (MIP) is a widely used technique for characterizing the distribution of pore sizes in cement-based materials. It is a simple and quick indirect technique, but it has limitations when applied to materials that have irregular pore geometry. The relationship between MIP re...
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| Veröffentlicht in: | Journal of Colloid and Interface Science 1999-03, Vol.211 (1), p.39-44 |
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| creator | Abell, A.B. Willis, K.L. Lange, D.A. |
| description | Mercury intrusion porosimetry (MIP) is a widely used technique for characterizing the distribution of pore sizes in cement-based materials. It is a simple and quick indirect technique, but it has limitations when applied to materials that have irregular pore geometry. The relationship between MIP results and the actual pore distribution and connectivity can be better understood with the use of image analysis. This paper discusses the use of MIP to describe the pore structure of cements and the efforts to validate the technique with microscopy. In particular, a study using molten Wood's metal as an alternate intrusion liquid that is solid in the pores at room temperature and can be examined by scanning electron microscopy will be presented. Results of the image analysis and the intrusion behavior of Portland cement mortars will be discussed. |
| doi_str_mv | 10.1006/jcis.1998.5986 |
| format | Article |
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It is a simple and quick indirect technique, but it has limitations when applied to materials that have irregular pore geometry. The relationship between MIP results and the actual pore distribution and connectivity can be better understood with the use of image analysis. This paper discusses the use of MIP to describe the pore structure of cements and the efforts to validate the technique with microscopy. In particular, a study using molten Wood's metal as an alternate intrusion liquid that is solid in the pores at room temperature and can be examined by scanning electron microscopy will be presented. 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It is a simple and quick indirect technique, but it has limitations when applied to materials that have irregular pore geometry. The relationship between MIP results and the actual pore distribution and connectivity can be better understood with the use of image analysis. This paper discusses the use of MIP to describe the pore structure of cements and the efforts to validate the technique with microscopy. In particular, a study using molten Wood's metal as an alternate intrusion liquid that is solid in the pores at room temperature and can be examined by scanning electron microscopy will be presented. Results of the image analysis and the intrusion behavior of Portland cement mortars will be discussed.</description><subject>cement-based materials</subject><subject>Chemistry</subject><subject>Colloidal gels. Colloidal sols</subject><subject>Colloidal state and disperse state</subject><subject>ENGINEERING NOT INCLUDED IN OTHER CATEGORIES</subject><subject>Exact sciences and technology</subject><subject>General and physical chemistry</subject><subject>image analysis</subject><subject>IMAGE PROCESSING</subject><subject>MATERIALS SCIENCE</subject><subject>mercury porosimetry</subject><subject>MORTARS</subject><subject>PORE STRUCTURE</subject><subject>POROSIMETERS</subject><subject>POROSITY</subject><subject>PORTLAND CEMENT</subject><subject>Wood's metal</subject><issn>0021-9797</issn><issn>1095-7103</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1999</creationdate><recordtype>article</recordtype><recordid>eNp1kE1v1DAQhi0EKtvClRtSkDj0ksV27MQ-tis-FrWCA5wt73gMrhK72AnS_nsc7ao3TiN5nnnl9yHkDaNbRmn_4QFC2TKt1VZq1T8jG0a1bAdGu-dkQylnrR708JJclvJAKWNS6gtyoTXXous25Os9ZljysdnHOS8lpNh8TzmVMOFcX210zX6yv7C5iXY8llCa5JsdThjn9tYWdM29nTEHO5ZX5IWvA1-f5xX5-enjj92X9u7b5_3u5q4F0fO5RZAChBicPvQUvO-t14IyJwd1AOoPYLl3vVTCKV43HoTuQHHJGaK3VnRX5N0pN5U5mAJhRvgNKUaE2XRcdYxX5vrEPOb0Z8EymykUwHG0EdNSDFNSc1EzWUW3JxRq7ZLRm8ccJpuPhlGzKjarYrMqNqvievD2nL0cJnRP-Nlp3b8_720BO_ps4xrwlDoI1ou1hjphWF39DZjXKhgBXchrE5fC_37wDz9hl40</recordid><startdate>19990301</startdate><enddate>19990301</enddate><creator>Abell, A.B.</creator><creator>Willis, K.L.</creator><creator>Lange, D.A.</creator><general>Elsevier Inc</general><general>Elsevier</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>OTOTI</scope></search><sort><creationdate>19990301</creationdate><title>Mercury Intrusion Porosimetry and Image Analysis of Cement-Based Materials</title><author>Abell, A.B. ; Willis, K.L. ; Lange, D.A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c462t-ec54c447d9b60cff6af9401d578bc0fbca2fd6584d82f94fc493c82521eefaa43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1999</creationdate><topic>cement-based materials</topic><topic>Chemistry</topic><topic>Colloidal gels. Colloidal sols</topic><topic>Colloidal state and disperse state</topic><topic>ENGINEERING NOT INCLUDED IN OTHER CATEGORIES</topic><topic>Exact sciences and technology</topic><topic>General and physical chemistry</topic><topic>image analysis</topic><topic>IMAGE PROCESSING</topic><topic>MATERIALS SCIENCE</topic><topic>mercury porosimetry</topic><topic>MORTARS</topic><topic>PORE STRUCTURE</topic><topic>POROSIMETERS</topic><topic>POROSITY</topic><topic>PORTLAND CEMENT</topic><topic>Wood's metal</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abell, A.B.</creatorcontrib><creatorcontrib>Willis, K.L.</creatorcontrib><creatorcontrib>Lange, D.A.</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>OSTI.GOV</collection><jtitle>Journal of Colloid and Interface Science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abell, A.B.</au><au>Willis, K.L.</au><au>Lange, D.A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Mercury Intrusion Porosimetry and Image Analysis of Cement-Based Materials</atitle><jtitle>Journal of Colloid and Interface Science</jtitle><addtitle>J Colloid Interface Sci</addtitle><date>1999-03-01</date><risdate>1999</risdate><volume>211</volume><issue>1</issue><spage>39</spage><epage>44</epage><pages>39-44</pages><issn>0021-9797</issn><eissn>1095-7103</eissn><coden>JCISA5</coden><abstract>Mercury intrusion porosimetry (MIP) is a widely used technique for characterizing the distribution of pore sizes in cement-based materials. It is a simple and quick indirect technique, but it has limitations when applied to materials that have irregular pore geometry. The relationship between MIP results and the actual pore distribution and connectivity can be better understood with the use of image analysis. This paper discusses the use of MIP to describe the pore structure of cements and the efforts to validate the technique with microscopy. In particular, a study using molten Wood's metal as an alternate intrusion liquid that is solid in the pores at room temperature and can be examined by scanning electron microscopy will be presented. Results of the image analysis and the intrusion behavior of Portland cement mortars will be discussed.</abstract><cop>San Diego, CA</cop><pub>Elsevier Inc</pub><pmid>9929433</pmid><doi>10.1006/jcis.1998.5986</doi><tpages>6</tpages></addata></record> |
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| subjects | cement-based materials Chemistry Colloidal gels. Colloidal sols Colloidal state and disperse state ENGINEERING NOT INCLUDED IN OTHER CATEGORIES Exact sciences and technology General and physical chemistry image analysis IMAGE PROCESSING MATERIALS SCIENCE mercury porosimetry MORTARS PORE STRUCTURE POROSIMETERS POROSITY PORTLAND CEMENT Wood's metal |
| title | Mercury Intrusion Porosimetry and Image Analysis of Cement-Based Materials |
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