Novel Direct Synthesis of Mesoporous Tin Dioxide Network Intact up to 500 degree C

We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 degree C and 500 degree C and has a relatively high BET surface area of 220 and 100 m2 g-1, respectively. TEM, BET and XRD results confirm that both crys...

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Veröffentlicht in:Journal of nano research 2016-03, Vol.40, p.79-89
Hauptverfasser: Aqeel, Tariq, Greer, Heather F, Zhou, Wu Zong, Bruce, Duncan W, Bumajdad, Ali
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container_title Journal of nano research
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creator Aqeel, Tariq
Greer, Heather F
Zhou, Wu Zong
Bruce, Duncan W
Bumajdad, Ali
description We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 degree C and 500 degree C and has a relatively high BET surface area of 220 and 100 m2 g-1, respectively. TEM, BET and XRD results confirm that both crystal and pore sizes increase as a result of increasing the temperatures during the calcination step. This method is highly reproducible.
doi_str_mv 10.4028/www.scientific.net/JNanoR.40.79
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subjects Calcination
Crystals
Nanostructure
Networks
Porosity
Surface area
Tin dioxide
Tin oxides
title Novel Direct Synthesis of Mesoporous Tin Dioxide Network Intact up to 500 degree C
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