Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction
BACKGROUND Among active components in Rabdosia rubescens, oridonin has been considered a key component and the most valuable compound because it has a wide range of activities beneficial to human health. To produce a high‐quality oridonin extract, an alternative hyphenated procedure involving an ult...
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| Veröffentlicht in: | Journal of the science of food and agriculture 2017-08, Vol.97 (10), p.3323-3332 |
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| creator | Yang, Yu‐Chiao Lin, Pei‐Hui Wei, Ming‐Chi |
| description | BACKGROUND
Among active components in Rabdosia rubescens, oridonin has been considered a key component and the most valuable compound because it has a wide range of activities beneficial to human health. To produce a high‐quality oridonin extract, an alternative hyphenated procedure involving an ultrasound‐assisted and supercritical carbon dioxide (HSC‐CO2) extraction method to extract oridonin from R. rubescens was developed in this study. Fictitious solubilities of oridonin in supercritical CO2 (SC‐CO2) with ultrasound assistance were measured by using the dynamic method at temperatures ranging from 305.15 K to 342.15 K over a pressure range of 11.5 to 33.5 MPa.
RESULTS
Fictitious solubilities of oridonin at different temperatures and pressures were over the range of 2.13 × 10−6 to 10.09 × 10−6 (mole fraction) and correlated well with the density‐based models, including the Bartle model, the Chrastil model, the Kumar and Johnston model and the Mendez‐Santiago and Teja model, with overall average absolute relative deviations (AARDs) of 6.29%, 4.39%, 3.12% and 5.07%, respectively.
CONCLUSION
Oridonin exhibits retrograde solubility behaviour in the supercritical state. Fictitious solubility data were further determined and obtained a good fit with four semi‐empirical models. Simultaneously, the values of the total heat of solution, vaporisation and solvation of oridonin were estimated. © 2016 Society of Chemical Industry |
| doi_str_mv | 10.1002/jsfa.8182 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1852688746</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1852688746</sourcerecordid><originalsourceid>FETCH-LOGICAL-c3532-dd115fcba652968dd1936393804f7eea5010950e65e53ce052e15a5e87d25f0e3</originalsourceid><addsrcrecordid>eNp1kc9uFSEUh4mxsdfqwhcwJG50MS0wAwPLprFa06TGP2vCwBkvN3PhCkPau_MFTPqMfZJyva0LE1cEzsd3zskPoVeUHFNC2Mkqj-ZYUsmeoAUlqm8IoeQpWtQaazjt2CF6nvOKEKKUEM_QIeuVpILQBfr9OUVX7OxjwHHEMXkXgw93v26Tt0sMN3Myds54THGNv5jBxewNTmWAbCFkXLIPP_Byu1lCMDM4XKb6I8cSXHWYnH3eveaygWSTn701E7YmDbWf8_HGO3hsUkd4gQ5GM2V4-XAeoe_n77-dfWwurz5cnJ1eNrblLWuco5SPdjCCMyVkvapWtKqVpBt7AMPr-ooTEBx4a4FwBpQbDrJ3jI8E2iP0du_dpPizQJ712td9pskEiCVrKjkTUvadqOibf9BVLCnU6TRVpGedIl1fqXd7yqaYc4JRb5Jfm7TVlOhdRnqXkd5lVNnXD8YyrMH9JR9DqcDJHrj2E2z_b9Kfvp6f_lHeA3nRoM8</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1907249047</pqid></control><display><type>article</type><title>Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction</title><source>Wiley-Blackwell Journals</source><source>MEDLINE</source><creator>Yang, Yu‐Chiao ; Lin, Pei‐Hui ; Wei, Ming‐Chi</creator><creatorcontrib>Yang, Yu‐Chiao ; Lin, Pei‐Hui ; Wei, Ming‐Chi</creatorcontrib><description>BACKGROUND
Among active components in Rabdosia rubescens, oridonin has been considered a key component and the most valuable compound because it has a wide range of activities beneficial to human health. To produce a high‐quality oridonin extract, an alternative hyphenated procedure involving an ultrasound‐assisted and supercritical carbon dioxide (HSC‐CO2) extraction method to extract oridonin from R. rubescens was developed in this study. Fictitious solubilities of oridonin in supercritical CO2 (SC‐CO2) with ultrasound assistance were measured by using the dynamic method at temperatures ranging from 305.15 K to 342.15 K over a pressure range of 11.5 to 33.5 MPa.
RESULTS
Fictitious solubilities of oridonin at different temperatures and pressures were over the range of 2.13 × 10−6 to 10.09 × 10−6 (mole fraction) and correlated well with the density‐based models, including the Bartle model, the Chrastil model, the Kumar and Johnston model and the Mendez‐Santiago and Teja model, with overall average absolute relative deviations (AARDs) of 6.29%, 4.39%, 3.12% and 5.07%, respectively.
CONCLUSION
Oridonin exhibits retrograde solubility behaviour in the supercritical state. Fictitious solubility data were further determined and obtained a good fit with four semi‐empirical models. Simultaneously, the values of the total heat of solution, vaporisation and solvation of oridonin were estimated. © 2016 Society of Chemical Industry</description><identifier>ISSN: 0022-5142</identifier><identifier>EISSN: 1097-0010</identifier><identifier>DOI: 10.1002/jsfa.8182</identifier><identifier>PMID: 27981601</identifier><language>eng</language><publisher>Chichester, UK: John Wiley & Sons, Ltd</publisher><subject>Behavior ; Carbon dioxide ; Chrastil model ; Chromatography, Supercritical Fluid - methods ; Correlation ; Density ; Diterpenes, Kaurane - analysis ; Diterpenes, Kaurane - isolation & purification ; Enthalpy ; Extraction ; fictitious solubility ; Heat ; Heat of solution ; Isodon - chemistry ; oridonin ; Plant Extracts - analysis ; Plant Extracts - isolation & purification ; Pressure ; Rabdosia rubescens ; Solubility ; Solvation ; supercritical CO2 extraction ; Ultrasonic imaging ; Ultrasonics - methods ; Ultrasound ; Vaporization</subject><ispartof>Journal of the science of food and agriculture, 2017-08, Vol.97 (10), p.3323-3332</ispartof><rights>2016 Society of Chemical Industry</rights><rights>2016 Society of Chemical Industry.</rights><rights>2017 Society of Chemical Industry</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3532-dd115fcba652968dd1936393804f7eea5010950e65e53ce052e15a5e87d25f0e3</citedby><cites>FETCH-LOGICAL-c3532-dd115fcba652968dd1936393804f7eea5010950e65e53ce052e15a5e87d25f0e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fjsfa.8182$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fjsfa.8182$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/27981601$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Yang, Yu‐Chiao</creatorcontrib><creatorcontrib>Lin, Pei‐Hui</creatorcontrib><creatorcontrib>Wei, Ming‐Chi</creatorcontrib><title>Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction</title><title>Journal of the science of food and agriculture</title><addtitle>J Sci Food Agric</addtitle><description>BACKGROUND
Among active components in Rabdosia rubescens, oridonin has been considered a key component and the most valuable compound because it has a wide range of activities beneficial to human health. To produce a high‐quality oridonin extract, an alternative hyphenated procedure involving an ultrasound‐assisted and supercritical carbon dioxide (HSC‐CO2) extraction method to extract oridonin from R. rubescens was developed in this study. Fictitious solubilities of oridonin in supercritical CO2 (SC‐CO2) with ultrasound assistance were measured by using the dynamic method at temperatures ranging from 305.15 K to 342.15 K over a pressure range of 11.5 to 33.5 MPa.
RESULTS
Fictitious solubilities of oridonin at different temperatures and pressures were over the range of 2.13 × 10−6 to 10.09 × 10−6 (mole fraction) and correlated well with the density‐based models, including the Bartle model, the Chrastil model, the Kumar and Johnston model and the Mendez‐Santiago and Teja model, with overall average absolute relative deviations (AARDs) of 6.29%, 4.39%, 3.12% and 5.07%, respectively.
CONCLUSION
Oridonin exhibits retrograde solubility behaviour in the supercritical state. Fictitious solubility data were further determined and obtained a good fit with four semi‐empirical models. Simultaneously, the values of the total heat of solution, vaporisation and solvation of oridonin were estimated. © 2016 Society of Chemical Industry</description><subject>Behavior</subject><subject>Carbon dioxide</subject><subject>Chrastil model</subject><subject>Chromatography, Supercritical Fluid - methods</subject><subject>Correlation</subject><subject>Density</subject><subject>Diterpenes, Kaurane - analysis</subject><subject>Diterpenes, Kaurane - isolation & purification</subject><subject>Enthalpy</subject><subject>Extraction</subject><subject>fictitious solubility</subject><subject>Heat</subject><subject>Heat of solution</subject><subject>Isodon - chemistry</subject><subject>oridonin</subject><subject>Plant Extracts - analysis</subject><subject>Plant Extracts - isolation & purification</subject><subject>Pressure</subject><subject>Rabdosia rubescens</subject><subject>Solubility</subject><subject>Solvation</subject><subject>supercritical CO2 extraction</subject><subject>Ultrasonic imaging</subject><subject>Ultrasonics - methods</subject><subject>Ultrasound</subject><subject>Vaporization</subject><issn>0022-5142</issn><issn>1097-0010</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp1kc9uFSEUh4mxsdfqwhcwJG50MS0wAwPLprFa06TGP2vCwBkvN3PhCkPau_MFTPqMfZJyva0LE1cEzsd3zskPoVeUHFNC2Mkqj-ZYUsmeoAUlqm8IoeQpWtQaazjt2CF6nvOKEKKUEM_QIeuVpILQBfr9OUVX7OxjwHHEMXkXgw93v26Tt0sMN3Myds54THGNv5jBxewNTmWAbCFkXLIPP_Byu1lCMDM4XKb6I8cSXHWYnH3eveaygWSTn701E7YmDbWf8_HGO3hsUkd4gQ5GM2V4-XAeoe_n77-dfWwurz5cnJ1eNrblLWuco5SPdjCCMyVkvapWtKqVpBt7AMPr-ooTEBx4a4FwBpQbDrJ3jI8E2iP0du_dpPizQJ712td9pskEiCVrKjkTUvadqOibf9BVLCnU6TRVpGedIl1fqXd7yqaYc4JRb5Jfm7TVlOhdRnqXkd5lVNnXD8YyrMH9JR9DqcDJHrj2E2z_b9Kfvp6f_lHeA3nRoM8</recordid><startdate>201708</startdate><enddate>201708</enddate><creator>Yang, Yu‐Chiao</creator><creator>Lin, Pei‐Hui</creator><creator>Wei, Ming‐Chi</creator><general>John Wiley & Sons, Ltd</general><general>John Wiley and Sons, Limited</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QL</scope><scope>7QQ</scope><scope>7QR</scope><scope>7SC</scope><scope>7SE</scope><scope>7SN</scope><scope>7SP</scope><scope>7SR</scope><scope>7ST</scope><scope>7T5</scope><scope>7T7</scope><scope>7TA</scope><scope>7TB</scope><scope>7TM</scope><scope>7U5</scope><scope>7U9</scope><scope>8BQ</scope><scope>8FD</scope><scope>C1K</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>H94</scope><scope>JG9</scope><scope>JQ2</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>M7N</scope><scope>P64</scope><scope>SOI</scope><scope>7X8</scope></search><sort><creationdate>201708</creationdate><title>Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction</title><author>Yang, Yu‐Chiao ; Lin, Pei‐Hui ; Wei, Ming‐Chi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3532-dd115fcba652968dd1936393804f7eea5010950e65e53ce052e15a5e87d25f0e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Behavior</topic><topic>Carbon dioxide</topic><topic>Chrastil model</topic><topic>Chromatography, Supercritical Fluid - methods</topic><topic>Correlation</topic><topic>Density</topic><topic>Diterpenes, Kaurane - analysis</topic><topic>Diterpenes, Kaurane - isolation & purification</topic><topic>Enthalpy</topic><topic>Extraction</topic><topic>fictitious solubility</topic><topic>Heat</topic><topic>Heat of solution</topic><topic>Isodon - chemistry</topic><topic>oridonin</topic><topic>Plant Extracts - analysis</topic><topic>Plant Extracts - isolation & purification</topic><topic>Pressure</topic><topic>Rabdosia rubescens</topic><topic>Solubility</topic><topic>Solvation</topic><topic>supercritical CO2 extraction</topic><topic>Ultrasonic imaging</topic><topic>Ultrasonics - methods</topic><topic>Ultrasound</topic><topic>Vaporization</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Yu‐Chiao</creatorcontrib><creatorcontrib>Lin, Pei‐Hui</creatorcontrib><creatorcontrib>Wei, Ming‐Chi</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Bacteriology Abstracts (Microbiology B)</collection><collection>Ceramic Abstracts</collection><collection>Chemoreception Abstracts</collection><collection>Computer and Information Systems Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Ecology Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Environment Abstracts</collection><collection>Immunology Abstracts</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Materials Business File</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Nucleic Acids Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Virology and AIDS Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Aerospace Database</collection><collection>Copper Technical Reference Library</collection><collection>AIDS and Cancer Research Abstracts</collection><collection>Materials Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>Civil Engineering Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Computer and Information Systems Abstracts Academic</collection><collection>Computer and Information Systems Abstracts Professional</collection><collection>Algology Mycology and Protozoology Abstracts (Microbiology C)</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Environment Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of the science of food and agriculture</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Yu‐Chiao</au><au>Lin, Pei‐Hui</au><au>Wei, Ming‐Chi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction</atitle><jtitle>Journal of the science of food and agriculture</jtitle><addtitle>J Sci Food Agric</addtitle><date>2017-08</date><risdate>2017</risdate><volume>97</volume><issue>10</issue><spage>3323</spage><epage>3332</epage><pages>3323-3332</pages><issn>0022-5142</issn><eissn>1097-0010</eissn><abstract>BACKGROUND
Among active components in Rabdosia rubescens, oridonin has been considered a key component and the most valuable compound because it has a wide range of activities beneficial to human health. To produce a high‐quality oridonin extract, an alternative hyphenated procedure involving an ultrasound‐assisted and supercritical carbon dioxide (HSC‐CO2) extraction method to extract oridonin from R. rubescens was developed in this study. Fictitious solubilities of oridonin in supercritical CO2 (SC‐CO2) with ultrasound assistance were measured by using the dynamic method at temperatures ranging from 305.15 K to 342.15 K over a pressure range of 11.5 to 33.5 MPa.
RESULTS
Fictitious solubilities of oridonin at different temperatures and pressures were over the range of 2.13 × 10−6 to 10.09 × 10−6 (mole fraction) and correlated well with the density‐based models, including the Bartle model, the Chrastil model, the Kumar and Johnston model and the Mendez‐Santiago and Teja model, with overall average absolute relative deviations (AARDs) of 6.29%, 4.39%, 3.12% and 5.07%, respectively.
CONCLUSION
Oridonin exhibits retrograde solubility behaviour in the supercritical state. Fictitious solubility data were further determined and obtained a good fit with four semi‐empirical models. Simultaneously, the values of the total heat of solution, vaporisation and solvation of oridonin were estimated. © 2016 Society of Chemical Industry</abstract><cop>Chichester, UK</cop><pub>John Wiley & Sons, Ltd</pub><pmid>27981601</pmid><doi>10.1002/jsfa.8182</doi><tpages>10</tpages></addata></record> |
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| ispartof | Journal of the science of food and agriculture, 2017-08, Vol.97 (10), p.3323-3332 |
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| source | Wiley-Blackwell Journals; MEDLINE |
| subjects | Behavior Carbon dioxide Chrastil model Chromatography, Supercritical Fluid - methods Correlation Density Diterpenes, Kaurane - analysis Diterpenes, Kaurane - isolation & purification Enthalpy Extraction fictitious solubility Heat Heat of solution Isodon - chemistry oridonin Plant Extracts - analysis Plant Extracts - isolation & purification Pressure Rabdosia rubescens Solubility Solvation supercritical CO2 extraction Ultrasonic imaging Ultrasonics - methods Ultrasound Vaporization |
| title | Production of oridonin‐rich extracts from Rabdosia rubescens using hyphenated ultrasound‐assisted supercritical carbon dioxide extraction |
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