Synthesis and Properties of Tin Sulfide Thin Films from Nanocolloids Prepared by Pulsed Laser Ablation in Liquid

Tin sulfide (SnS) nanoparticles were synthesized by pulsed laser ablation in liquid (PLAL) technique using an Nd:YAG laser operated at 532 nm. SnS thin films were deposited by spraying the colloidal suspension onto the heated substrates. The influence of different liquid media (dimethyl formamide an...

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Veröffentlicht in:Chemphyschem 2017-05, Vol.18 (9), p.1061-1068
Hauptverfasser: Johny, Jacob, Sepulveda‐Guzman, Selene, Krishnan, Bindu, Avellaneda, David A., Aguilar Martinez, Josue A., Shaji, Sadasivan
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container_end_page 1068
container_issue 9
container_start_page 1061
container_title Chemphyschem
container_volume 18
creator Johny, Jacob
Sepulveda‐Guzman, Selene
Krishnan, Bindu
Avellaneda, David A.
Aguilar Martinez, Josue A.
Shaji, Sadasivan
description Tin sulfide (SnS) nanoparticles were synthesized by pulsed laser ablation in liquid (PLAL) technique using an Nd:YAG laser operated at 532 nm. SnS thin films were deposited by spraying the colloidal suspension onto the heated substrates. The influence of different liquid media (dimethyl formamide and isopropyl alcohol) on the thin film properties were studied. Morphology, crystalline structure, and chemical composition of the nanoparticles were identified using transmission electron microscopy with energy dispersive X‐ray analysis. The crystalline structure of the thin films was analyzed by using grazing incidence X‐ray diffraction, and the chemical states by X‐ray photoelectron spectroscopy. Scanning electron microscopy was employed for the morphological analysis of the thin films. Annealing the films at 380 °C improved the crystallinity of the films exhibiting a layered morphology, which may be useful in optoelectronic and sensing applications. Cyclic voltammetry studies showed that the films have good electrochemical properties. Nanostructured SnS thin films were synthesized combining PLAL with spray technique. Layer‐like morphology was obtained for the films (see Figure). Electrochemical and opto‐electronic properties of the films were investigated in addition to the characterization of SnS thin films as well as nanoparticles.
doi_str_mv 10.1002/cphc.201601186
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source Wiley Online Library Journals Frontfile Complete
subjects Chemical composition
Colloid chemistry
Crystal structure
cyclic voltammetry
Grazing incidence
Laser ablation
Lasers
Morphology
Nanoparticles
photoelectron spectroscopy
Scanning electron microscopy
semiconductors
Thin films
Voltammetry
title Synthesis and Properties of Tin Sulfide Thin Films from Nanocolloids Prepared by Pulsed Laser Ablation in Liquid
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