A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods
A rapid dialysis method for the analysis of stevioside (SS) and rebaudioside A (RS) in foods was developed. Minced samples (10 g) were packed into 30 cm net length dialysis tubing with 30% methanol to increase the dialysis efficiency. The dialysis tubing was put in a 100 mL centrifuge tube, and the...
Gespeichert in:
| Veröffentlicht in: | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 2016/10/25, Vol.57(5), pp.155-159 |
|---|---|
| Hauptverfasser: | , , , , , , , |
| Format: | Artikel |
| Sprache: | eng ; jpn |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 159 |
|---|---|
| container_issue | 5 |
| container_start_page | 155 |
| container_title | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) |
| container_volume | 57 |
| creator | YAMAMOTO, Sumiyo TAHARA, Shoichi SUGIKI, Mikio MIYAKAWA, Hiroyuki UEMATSU, Yoko YAMAJIMA, Yukiko SAKAMAKI, Narue MONMA, Kimio |
| description | A rapid dialysis method for the analysis of stevioside (SS) and rebaudioside A (RS) in foods was developed. Minced samples (10 g) were packed into 30 cm net length dialysis tubing with 30% methanol to increase the dialysis efficiency. The dialysis tubing was put in a 100 mL centrifuge tube, and the total fluid volume was made up to 100 mL with 30% methanol. Dialysis was done with shaking while heating at 50℃. The dialysis times were reduced from 48–72 hr in the conventional method to 2 hr under these conditions. The dialysate was loaded on a C18 solid- phase extraction cartridge, and the cartridge was washed with 40% methanol. SS and RS were eluted from the cartridge with 80% methanol, and separated by reversed-phase HPLC. Recovery yields (%)of SS and RS, spiked at 0.02 g/kg in various foods, were 83.0–105.1% and the relative standard deviations were mostly less than 5%. |
| doi_str_mv | 10.3358/shokueishi.57.155 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1850791937</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1850791937</sourcerecordid><originalsourceid>FETCH-LOGICAL-c438t-6a2b69956766c7886fa4e9daa6bb936e45749d273390c3f5cd38a4e60e2d89783</originalsourceid><addsrcrecordid>eNpdkMtOwzAQRS0EolXpB7BBXrJJseP4tazKUyogFVhbTjyhhjQucYLE3xPUUCRWI9059ywuQqeUzBjj6iKuw3sHPq79jMsZ5fwAjalSaUIJEYdoTAjlichSMULTGH1OUpLJVGpxjEaplCpTQozRwxyv7NY7fOlt9RV9xPfQroPDZWjwvB6yUOKnFj59iN4BtrXDK8ht54Zgjn2Nr0Nw8QQdlbaKMB3uBL1cXz0vbpPl483dYr5MioypNhE2zYXWXEghCqmUKG0G2lkr8lwzARmXmXapZEyTgpW8cEz1hCCQOqWlYhN0vvNum_DRQWzNxscCqsrWELpoqOJEaqqZ7FG6Q4smxNhAabaN39jmy1BifpY0f0saLk2_ZN85G_RdvgG3b_zu1gOXO-AttvYV9oBtWl9U8E_JB-_-XaxtY6Bm3-LsihQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1850791937</pqid></control><display><type>article</type><title>A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods</title><source>MEDLINE</source><source>EZB-FREE-00999 freely available EZB journals</source><source>AgriKnowledge（アグリナレッジ）AGROLib</source><creator>YAMAMOTO, Sumiyo ; TAHARA, Shoichi ; SUGIKI, Mikio ; MIYAKAWA, Hiroyuki ; UEMATSU, Yoko ; YAMAJIMA, Yukiko ; SAKAMAKI, Narue ; MONMA, Kimio</creator><creatorcontrib>YAMAMOTO, Sumiyo ; TAHARA, Shoichi ; SUGIKI, Mikio ; MIYAKAWA, Hiroyuki ; UEMATSU, Yoko ; YAMAJIMA, Yukiko ; SAKAMAKI, Narue ; MONMA, Kimio</creatorcontrib><description>A rapid dialysis method for the analysis of stevioside (SS) and rebaudioside A (RS) in foods was developed. Minced samples (10 g) were packed into 30 cm net length dialysis tubing with 30% methanol to increase the dialysis efficiency. The dialysis tubing was put in a 100 mL centrifuge tube, and the total fluid volume was made up to 100 mL with 30% methanol. Dialysis was done with shaking while heating at 50℃. The dialysis times were reduced from 48–72 hr in the conventional method to 2 hr under these conditions. The dialysate was loaded on a C18 solid- phase extraction cartridge, and the cartridge was washed with 40% methanol. SS and RS were eluted from the cartridge with 80% methanol, and separated by reversed-phase HPLC. Recovery yields (%)of SS and RS, spiked at 0.02 g/kg in various foods, were 83.0–105.1% and the relative standard deviations were mostly less than 5%.</description><identifier>ISSN: 0015-6426</identifier><identifier>EISSN: 1882-1006</identifier><identifier>DOI: 10.3358/shokueishi.57.155</identifier><identifier>PMID: 27784866</identifier><language>eng ; jpn</language><publisher>Japan: Japanese Society for Food Hygiene and Safety</publisher><subject>Chromatography, High Pressure Liquid - methods ; Dialysis - methods ; dialysis method ; Diterpenes, Kaurane - analysis ; Diterpenes, Kaurane - isolation & purification ; food ; Food Additives - analysis ; Food Additives - isolation & purification ; Food Analysis - methods ; Glucosides - analysis ; Glucosides - isolation & purification ; heating ; HPLC ; rebaudioside A ; shaking ; Solid Phase Extraction ; stevioside ; Temperature ; Time Factors</subject><ispartof>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi), 2016/10/25, Vol.57(5), pp.155-159</ispartof><rights>2016 Japanese Society for Food Hygiene and Safety</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c438t-6a2b69956766c7886fa4e9daa6bb936e45749d273390c3f5cd38a4e60e2d89783</citedby><cites>FETCH-LOGICAL-c438t-6a2b69956766c7886fa4e9daa6bb936e45749d273390c3f5cd38a4e60e2d89783</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,4009,27902,27903,27904</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/27784866$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>YAMAMOTO, Sumiyo</creatorcontrib><creatorcontrib>TAHARA, Shoichi</creatorcontrib><creatorcontrib>SUGIKI, Mikio</creatorcontrib><creatorcontrib>MIYAKAWA, Hiroyuki</creatorcontrib><creatorcontrib>UEMATSU, Yoko</creatorcontrib><creatorcontrib>YAMAJIMA, Yukiko</creatorcontrib><creatorcontrib>SAKAMAKI, Narue</creatorcontrib><creatorcontrib>MONMA, Kimio</creatorcontrib><title>A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods</title><title>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)</title><addtitle>Food Hyg. Saf. Sci.</addtitle><description>A rapid dialysis method for the analysis of stevioside (SS) and rebaudioside A (RS) in foods was developed. Minced samples (10 g) were packed into 30 cm net length dialysis tubing with 30% methanol to increase the dialysis efficiency. The dialysis tubing was put in a 100 mL centrifuge tube, and the total fluid volume was made up to 100 mL with 30% methanol. Dialysis was done with shaking while heating at 50℃. The dialysis times were reduced from 48–72 hr in the conventional method to 2 hr under these conditions. The dialysate was loaded on a C18 solid- phase extraction cartridge, and the cartridge was washed with 40% methanol. SS and RS were eluted from the cartridge with 80% methanol, and separated by reversed-phase HPLC. Recovery yields (%)of SS and RS, spiked at 0.02 g/kg in various foods, were 83.0–105.1% and the relative standard deviations were mostly less than 5%.</description><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Dialysis - methods</subject><subject>dialysis method</subject><subject>Diterpenes, Kaurane - analysis</subject><subject>Diterpenes, Kaurane - isolation & purification</subject><subject>food</subject><subject>Food Additives - analysis</subject><subject>Food Additives - isolation & purification</subject><subject>Food Analysis - methods</subject><subject>Glucosides - analysis</subject><subject>Glucosides - isolation & purification</subject><subject>heating</subject><subject>HPLC</subject><subject>rebaudioside A</subject><subject>shaking</subject><subject>Solid Phase Extraction</subject><subject>stevioside</subject><subject>Temperature</subject><subject>Time Factors</subject><issn>0015-6426</issn><issn>1882-1006</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpdkMtOwzAQRS0EolXpB7BBXrJJseP4tazKUyogFVhbTjyhhjQucYLE3xPUUCRWI9059ywuQqeUzBjj6iKuw3sHPq79jMsZ5fwAjalSaUIJEYdoTAjlichSMULTGH1OUpLJVGpxjEaplCpTQozRwxyv7NY7fOlt9RV9xPfQroPDZWjwvB6yUOKnFj59iN4BtrXDK8ht54Zgjn2Nr0Nw8QQdlbaKMB3uBL1cXz0vbpPl483dYr5MioypNhE2zYXWXEghCqmUKG0G2lkr8lwzARmXmXapZEyTgpW8cEz1hCCQOqWlYhN0vvNum_DRQWzNxscCqsrWELpoqOJEaqqZ7FG6Q4smxNhAabaN39jmy1BifpY0f0saLk2_ZN85G_RdvgG3b_zu1gOXO-AttvYV9oBtWl9U8E_JB-_-XaxtY6Bm3-LsihQ</recordid><startdate>2016</startdate><enddate>2016</enddate><creator>YAMAMOTO, Sumiyo</creator><creator>TAHARA, Shoichi</creator><creator>SUGIKI, Mikio</creator><creator>MIYAKAWA, Hiroyuki</creator><creator>UEMATSU, Yoko</creator><creator>YAMAJIMA, Yukiko</creator><creator>SAKAMAKI, Narue</creator><creator>MONMA, Kimio</creator><general>Japanese Society for Food Hygiene and Safety</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7T2</scope><scope>7U2</scope><scope>C1K</scope><scope>F1W</scope><scope>H95</scope><scope>L.G</scope></search><sort><creationdate>2016</creationdate><title>A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods</title><author>YAMAMOTO, Sumiyo ; TAHARA, Shoichi ; SUGIKI, Mikio ; MIYAKAWA, Hiroyuki ; UEMATSU, Yoko ; YAMAJIMA, Yukiko ; SAKAMAKI, Narue ; MONMA, Kimio</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c438t-6a2b69956766c7886fa4e9daa6bb936e45749d273390c3f5cd38a4e60e2d89783</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng ; jpn</language><creationdate>2016</creationdate><topic>Chromatography, High Pressure Liquid - methods</topic><topic>Dialysis - methods</topic><topic>dialysis method</topic><topic>Diterpenes, Kaurane - analysis</topic><topic>Diterpenes, Kaurane - isolation & purification</topic><topic>food</topic><topic>Food Additives - analysis</topic><topic>Food Additives - isolation & purification</topic><topic>Food Analysis - methods</topic><topic>Glucosides - analysis</topic><topic>Glucosides - isolation & purification</topic><topic>heating</topic><topic>HPLC</topic><topic>rebaudioside A</topic><topic>shaking</topic><topic>Solid Phase Extraction</topic><topic>stevioside</topic><topic>Temperature</topic><topic>Time Factors</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>YAMAMOTO, Sumiyo</creatorcontrib><creatorcontrib>TAHARA, Shoichi</creatorcontrib><creatorcontrib>SUGIKI, Mikio</creatorcontrib><creatorcontrib>MIYAKAWA, Hiroyuki</creatorcontrib><creatorcontrib>UEMATSU, Yoko</creatorcontrib><creatorcontrib>YAMAJIMA, Yukiko</creatorcontrib><creatorcontrib>SAKAMAKI, Narue</creatorcontrib><creatorcontrib>MONMA, Kimio</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Health and Safety Science Abstracts (Full archive)</collection><collection>Safety Science and Risk</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 1: Biological Sciences & Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><jtitle>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>YAMAMOTO, Sumiyo</au><au>TAHARA, Shoichi</au><au>SUGIKI, Mikio</au><au>MIYAKAWA, Hiroyuki</au><au>UEMATSU, Yoko</au><au>YAMAJIMA, Yukiko</au><au>SAKAMAKI, Narue</au><au>MONMA, Kimio</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods</atitle><jtitle>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)</jtitle><addtitle>Food Hyg. Saf. Sci.</addtitle><date>2016</date><risdate>2016</risdate><volume>57</volume><issue>5</issue><spage>155</spage><epage>159</epage><pages>155-159</pages><issn>0015-6426</issn><eissn>1882-1006</eissn><abstract>A rapid dialysis method for the analysis of stevioside (SS) and rebaudioside A (RS) in foods was developed. Minced samples (10 g) were packed into 30 cm net length dialysis tubing with 30% methanol to increase the dialysis efficiency. The dialysis tubing was put in a 100 mL centrifuge tube, and the total fluid volume was made up to 100 mL with 30% methanol. Dialysis was done with shaking while heating at 50℃. The dialysis times were reduced from 48–72 hr in the conventional method to 2 hr under these conditions. The dialysate was loaded on a C18 solid- phase extraction cartridge, and the cartridge was washed with 40% methanol. SS and RS were eluted from the cartridge with 80% methanol, and separated by reversed-phase HPLC. Recovery yields (%)of SS and RS, spiked at 0.02 g/kg in various foods, were 83.0–105.1% and the relative standard deviations were mostly less than 5%.</abstract><cop>Japan</cop><pub>Japanese Society for Food Hygiene and Safety</pub><pmid>27784866</pmid><doi>10.3358/shokueishi.57.155</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0015-6426 |
| ispartof | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi), 2016/10/25, Vol.57(5), pp.155-159 |
| issn | 0015-6426 1882-1006 |
| language | eng ; jpn |
| recordid | cdi_proquest_miscellaneous_1850791937 |
| source | MEDLINE; EZB-FREE-00999 freely available EZB journals; AgriKnowledge（アグリナレッジ）AGROLib |
| subjects | Chromatography, High Pressure Liquid - methods Dialysis - methods dialysis method Diterpenes, Kaurane - analysis Diterpenes, Kaurane - isolation & purification food Food Additives - analysis Food Additives - isolation & purification Food Analysis - methods Glucosides - analysis Glucosides - isolation & purification heating HPLC rebaudioside A shaking Solid Phase Extraction stevioside Temperature Time Factors |
| title | A Rapid Dialysis Method for Analysis of Stevioside and Rebaudioside A in Foods |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-22T08%3A41%3A45IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20Rapid%20Dialysis%20Method%20for%20Analysis%20of%20Stevioside%20and%20Rebaudioside%20A%20in%20Foods&rft.jtitle=Food%20Hygiene%20and%20Safety%20Science%20(Shokuhin%20Eiseigaku%20Zasshi)&rft.au=YAMAMOTO,%20Sumiyo&rft.date=2016&rft.volume=57&rft.issue=5&rft.spage=155&rft.epage=159&rft.pages=155-159&rft.issn=0015-6426&rft.eissn=1882-1006&rft_id=info:doi/10.3358/shokueishi.57.155&rft_dat=%3Cproquest_cross%3E1850791937%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1850791937&rft_id=info:pmid/27784866&rfr_iscdi=true |