Influence of ethanol content in the precipitation medium on the composition, structure and reactivity of magnesium–calcium phosphate
Biocompatible amorphous magnesium calcium phosphate (AMCP) particles were synthesized using ethanol in precipitation medium from moderately supersaturated solution at pH10. Some synthesis parameters such as, (Mg+Ca):P, Mg:Ca ratio and different drying methods on the structure and stability of as-pro...
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| Veröffentlicht in: | Materials Science & Engineering C 2015-08, Vol.53, p.204-211 |
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| creator | Babaie, Elham Zhou, Huan Lin, Boren Bhaduri, Sarit B. |
| description | Biocompatible amorphous magnesium calcium phosphate (AMCP) particles were synthesized using ethanol in precipitation medium from moderately supersaturated solution at pH10. Some synthesis parameters such as, (Mg+Ca):P, Mg:Ca ratio and different drying methods on the structure and stability of as-produced powder was studied and characterized using SEM, XRD and cell cytocompatibility. The results showed that depending on the Mg2+ concentration, nano crystalline Struvite (MgNH4PO4·6H2O) can also be alternatively formed. However, the as-formed AMCP preserved its amorphous structure after 7days of incubation in SBF for tested phosphate concentration, and equally ionic concentration of magnesium and calcium. |
| doi_str_mv | 10.1016/j.msec.2015.04.011 |
| format | Article |
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Some synthesis parameters such as, (Mg+Ca):P, Mg:Ca ratio and different drying methods on the structure and stability of as-produced powder was studied and characterized using SEM, XRD and cell cytocompatibility. The results showed that depending on the Mg2+ concentration, nano crystalline Struvite (MgNH4PO4·6H2O) can also be alternatively formed. 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However, the as-formed AMCP preserved its amorphous structure after 7days of incubation in SBF for tested phosphate concentration, and equally ionic concentration of magnesium and calcium.</description><subject>Amorphous phase</subject><subject>Animals</subject><subject>Biocompatible Materials - chemistry</subject><subject>Biocompatible Materials - toxicity</subject><subject>Calcium</subject><subject>Calcium phosphate</subject><subject>Calcium Phosphates - chemistry</subject><subject>Calcium Phosphates - toxicity</subject><subject>Cell Line</subject><subject>Cell Survival - drug effects</subject><subject>Chemical Precipitation</subject><subject>Drug Stability</subject><subject>Drying</subject><subject>Ethanol</subject><subject>Ethanol - chemistry</subject><subject>Ethyl alcohol</subject><subject>Magnesium</subject><subject>Magnesium Compounds - chemistry</subject><subject>Magnesium Compounds - toxicity</subject><subject>Magnesium phosphate</subject><subject>Mice</subject><subject>Phosphates</subject><subject>Phosphates - chemistry</subject><subject>Phosphates - toxicity</subject><subject>Precipitation</subject><issn>0928-4931</issn><issn>1873-0191</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkb1uFDEUhS0EIkvgBSiQSwpm8N96PBINiviJFIkGasu5vsN6NWMPtidSulS8AG_IkzCjDZSkusX9zinOR8hLzlrOuH57bKeC0ArG9y1TLeP8Edlx08mG8Z4_JjvWC9OoXvIz8qyUI2PayE48JWdCMyU6Znbk52UcxgUjIE0DxXpwMY0UUqwYKw2R1gPSOSOEOVRXQ4p0Qh-WiabTD9I0pxK2zxtaal6gLhmpi55mdFDDTai3W_fkvkcsa_L33S9wI2wd8yGV-eAqPidPBjcWfHF_z8m3jx--Xnxurr58urx4f9WA0ro2AsV-AGPAKTdodq072XvsNBgQXgwcHQfBPXq-N4iomenlHkAJhR6EE_KcvD71zjn9WLBUO4UCOI4uYlqK5etAUnDdm4fRrmNSSqH0w6g2WgnO-n5FxQmFnErJONg5h8nlW8uZ3azao92s2s2qZcquVtfQq_v-5Xpd_1_kr8YVeHcCcN3uJmC2BcIm1YdVXbU-hf_1_wFiF7dH</recordid><startdate>20150801</startdate><enddate>20150801</enddate><creator>Babaie, Elham</creator><creator>Zhou, Huan</creator><creator>Lin, Boren</creator><creator>Bhaduri, Sarit B.</creator><general>Elsevier B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7QF</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><scope>7QP</scope></search><sort><creationdate>20150801</creationdate><title>Influence of ethanol content in the precipitation medium on the composition, structure and reactivity of magnesium–calcium phosphate</title><author>Babaie, Elham ; 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| fulltext | fulltext |
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| ispartof | Materials Science & Engineering C, 2015-08, Vol.53, p.204-211 |
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| source | MEDLINE; ScienceDirect Journals (5 years ago - present) |
| subjects | Amorphous phase Animals Biocompatible Materials - chemistry Biocompatible Materials - toxicity Calcium Calcium phosphate Calcium Phosphates - chemistry Calcium Phosphates - toxicity Cell Line Cell Survival - drug effects Chemical Precipitation Drug Stability Drying Ethanol Ethanol - chemistry Ethyl alcohol Magnesium Magnesium Compounds - chemistry Magnesium Compounds - toxicity Magnesium phosphate Mice Phosphates Phosphates - chemistry Phosphates - toxicity Precipitation |
| title | Influence of ethanol content in the precipitation medium on the composition, structure and reactivity of magnesium–calcium phosphate |
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