Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation
[Display omitted] •This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation. A family of novel ionic liqu...
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| Veröffentlicht in: | Ultrasonics sonochemistry 2017-01, Vol.34, p.916-923 |
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| container_title | Ultrasonics sonochemistry |
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| creator | Safaei Ghomi, Javad Zahedi, Safura |
| description | [Display omitted]
•This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation.
A family of novel ionic liquid with l-alanine and choline chloride as environmentally benign materials have been synthesized and grafted on Fe3O4 nanoparticles using easy preparation techniques. The structure of ionic liquid supported on Fe3O4 nanoparticles (IL-Fe3O4 NPs) characterized by various analyses such as FE-SEM, EDX, XRD, NMR, FTIR and VSM. The catalytic activities of this catalyst are examined in the Mannich reaction for synthesis of β-aminocarbonyl compounds under ultrasonic irradiation. The recyclability of catalyst is investigated, and the results have indicated that the catalyst can be recycled six times without obvious activity decreasing. |
| doi_str_mv | 10.1016/j.ultsonch.2016.08.003 |
| format | Article |
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•This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation.
A family of novel ionic liquid with l-alanine and choline chloride as environmentally benign materials have been synthesized and grafted on Fe3O4 nanoparticles using easy preparation techniques. The structure of ionic liquid supported on Fe3O4 nanoparticles (IL-Fe3O4 NPs) characterized by various analyses such as FE-SEM, EDX, XRD, NMR, FTIR and VSM. The catalytic activities of this catalyst are examined in the Mannich reaction for synthesis of β-aminocarbonyl compounds under ultrasonic irradiation. The recyclability of catalyst is investigated, and the results have indicated that the catalyst can be recycled six times without obvious activity decreasing.</description><identifier>ISSN: 1350-4177</identifier><identifier>EISSN: 1873-2828</identifier><identifier>DOI: 10.1016/j.ultsonch.2016.08.003</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Ionic liquid ; l-alanine ; Magnetite nanoparticles ; Mannich reaction ; Ultrasonic irradiation</subject><ispartof>Ultrasonics sonochemistry, 2017-01, Vol.34, p.916-923</ispartof><rights>2016 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c415t-f80a790b06d0e656822dfb1804c01b50b450756150e1953a8bb9375fc4e9bbfd3</citedby><cites>FETCH-LOGICAL-c415t-f80a790b06d0e656822dfb1804c01b50b450756150e1953a8bb9375fc4e9bbfd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.ultsonch.2016.08.003$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Safaei Ghomi, Javad</creatorcontrib><creatorcontrib>Zahedi, Safura</creatorcontrib><title>Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation</title><title>Ultrasonics sonochemistry</title><description>[Display omitted]
•This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation.
A family of novel ionic liquid with l-alanine and choline chloride as environmentally benign materials have been synthesized and grafted on Fe3O4 nanoparticles using easy preparation techniques. The structure of ionic liquid supported on Fe3O4 nanoparticles (IL-Fe3O4 NPs) characterized by various analyses such as FE-SEM, EDX, XRD, NMR, FTIR and VSM. The catalytic activities of this catalyst are examined in the Mannich reaction for synthesis of β-aminocarbonyl compounds under ultrasonic irradiation. The recyclability of catalyst is investigated, and the results have indicated that the catalyst can be recycled six times without obvious activity decreasing.</description><subject>Ionic liquid</subject><subject>l-alanine</subject><subject>Magnetite nanoparticles</subject><subject>Mannich reaction</subject><subject>Ultrasonic irradiation</subject><issn>1350-4177</issn><issn>1873-2828</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqFkM1KxTAQhYsoqFdfQbJ00zppmzbdKeIf-LPRdUiTKeYSk5qkgi_gcxvv1bWrmYFzzsx8RXFCoaJAu7N1tdgUvVOvVZ3nCngF0OwUB5T3TVnzmu_mvmFQtrTv94vDGNeQFUMNB8XXo_9AS4x3RhFr3hejSVzm2YeEmnhHrrF5aomTzs8yJKMsRiKdJiblOs_WKJmym8g8ktxL-xkTMY48SJczX0lAqTaKxWkMJN8aZNysMyFIbTb2o2Jvkjbi8W9dFS_XV8-Xt-X9083d5cV9qVrKUjlxkP0AI3QasGMdr2s9jZRDq4CODMaWQc86ygDpwBrJx3FoejapFodxnHSzKk63uXPw7wvGJN5MVGitdOiXKChvGKv7DCpLu61UBR9jwEnMwbzJ8CkoiB_wYi3-wIsf8AK4yFiz8XxrxPzIh8EgojLoFGoTUCWhvfkv4hvtj5Je</recordid><startdate>201701</startdate><enddate>201701</enddate><creator>Safaei Ghomi, Javad</creator><creator>Zahedi, Safura</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>201701</creationdate><title>Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation</title><author>Safaei Ghomi, Javad ; Zahedi, Safura</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c415t-f80a790b06d0e656822dfb1804c01b50b450756150e1953a8bb9375fc4e9bbfd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Ionic liquid</topic><topic>l-alanine</topic><topic>Magnetite nanoparticles</topic><topic>Mannich reaction</topic><topic>Ultrasonic irradiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Safaei Ghomi, Javad</creatorcontrib><creatorcontrib>Zahedi, Safura</creatorcontrib><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Ultrasonics sonochemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Safaei Ghomi, Javad</au><au>Zahedi, Safura</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation</atitle><jtitle>Ultrasonics sonochemistry</jtitle><date>2017-01</date><risdate>2017</risdate><volume>34</volume><spage>916</spage><epage>923</epage><pages>916-923</pages><issn>1350-4177</issn><eissn>1873-2828</eissn><abstract>[Display omitted]
•This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation.
A family of novel ionic liquid with l-alanine and choline chloride as environmentally benign materials have been synthesized and grafted on Fe3O4 nanoparticles using easy preparation techniques. The structure of ionic liquid supported on Fe3O4 nanoparticles (IL-Fe3O4 NPs) characterized by various analyses such as FE-SEM, EDX, XRD, NMR, FTIR and VSM. The catalytic activities of this catalyst are examined in the Mannich reaction for synthesis of β-aminocarbonyl compounds under ultrasonic irradiation. The recyclability of catalyst is investigated, and the results have indicated that the catalyst can be recycled six times without obvious activity decreasing.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.ultsonch.2016.08.003</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Ionic liquid l-alanine Magnetite nanoparticles Mannich reaction Ultrasonic irradiation |
| title | Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation |
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