Novel ionic liquid supported on Fe3O4 nanoparticles and its application as a catalyst in Mannich reaction under ultrasonic irradiation

[Display omitted] •This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation. A family of novel ionic liqu...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Ultrasonics sonochemistry 2017-01, Vol.34, p.916-923
Hauptverfasser: Safaei Ghomi, Javad, Zahedi, Safura
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:[Display omitted] •This work has been successful in achieving the comparison trend under different conditions.•We used IL-Fe3O4 as catalyst for diastereoselective Mannich reaction.•The products were synthesised in short times and high yields under ultrasonic irradiation. A family of novel ionic liquid with l-alanine and choline chloride as environmentally benign materials have been synthesized and grafted on Fe3O4 nanoparticles using easy preparation techniques. The structure of ionic liquid supported on Fe3O4 nanoparticles (IL-Fe3O4 NPs) characterized by various analyses such as FE-SEM, EDX, XRD, NMR, FTIR and VSM. The catalytic activities of this catalyst are examined in the Mannich reaction for synthesis of β-aminocarbonyl compounds under ultrasonic irradiation. The recyclability of catalyst is investigated, and the results have indicated that the catalyst can be recycled six times without obvious activity decreasing.
ISSN:1350-4177
1873-2828
DOI:10.1016/j.ultsonch.2016.08.003