Conceptual and instrumental progress in dissolution DNP
[Display omitted] •What are key points in dissolution DNP methodology and instrumentation?•How can one boost polarization levels and polarization build-up times?•How can one minimize polarization losses during sample transfer? We discuss conceptual and instrumental progress in dissolution DNP since...
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| Veröffentlicht in: | Journal of magnetic resonance (1997) 2016-03, Vol.264, p.22-29 |
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| container_title | Journal of magnetic resonance (1997) |
| container_volume | 264 |
| creator | Jähnig, Fabian Kwiatkowski, Grzegorz Ernst, Matthias |
| description | [Display omitted]
•What are key points in dissolution DNP methodology and instrumentation?•How can one boost polarization levels and polarization build-up times?•How can one minimize polarization losses during sample transfer?
We discuss conceptual and instrumental progress in dissolution DNP since its introduction in 2003. In our view there are three critical steps in the dissolution DNP process: (i) The achievable polarization level in a sample. (ii) The time required to build up the polarization. (iii) The transfer of the sample to the measurement system with minimum loss of polarization. In this review we describe in detail these steps and the different methodological and instrumental implementations, which have been proposed to optimize them. |
| doi_str_mv | 10.1016/j.jmr.2015.12.024 |
| format | Article |
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•What are key points in dissolution DNP methodology and instrumentation?•How can one boost polarization levels and polarization build-up times?•How can one minimize polarization losses during sample transfer?
We discuss conceptual and instrumental progress in dissolution DNP since its introduction in 2003. In our view there are three critical steps in the dissolution DNP process: (i) The achievable polarization level in a sample. (ii) The time required to build up the polarization. (iii) The transfer of the sample to the measurement system with minimum loss of polarization. In this review we describe in detail these steps and the different methodological and instrumental implementations, which have been proposed to optimize them.</description><identifier>ISSN: 1090-7807</identifier><identifier>EISSN: 1096-0856</identifier><identifier>DOI: 10.1016/j.jmr.2015.12.024</identifier><identifier>PMID: 26920827</identifier><language>eng</language><publisher>United States: Elsevier Inc</publisher><subject>Accumulation ; Dissolution ; Dissolution DNP ; Hardware development ; Magnetic resonance ; Methodology in dissolution DNP ; Polarization</subject><ispartof>Journal of magnetic resonance (1997), 2016-03, Vol.264, p.22-29</ispartof><rights>2016 Elsevier Inc.</rights><rights>Copyright © 2016 Elsevier Inc. All rights reserved.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c429t-18a8c3136e7e6c44f1b12be83edfcdbf42017e4d302baffc7a6ef97c40ce14903</citedby><cites>FETCH-LOGICAL-c429t-18a8c3136e7e6c44f1b12be83edfcdbf42017e4d302baffc7a6ef97c40ce14903</cites><orcidid>0000-0002-9538-6086</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1090780716000239$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/26920827$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Jähnig, Fabian</creatorcontrib><creatorcontrib>Kwiatkowski, Grzegorz</creatorcontrib><creatorcontrib>Ernst, Matthias</creatorcontrib><title>Conceptual and instrumental progress in dissolution DNP</title><title>Journal of magnetic resonance (1997)</title><addtitle>J Magn Reson</addtitle><description>[Display omitted]
•What are key points in dissolution DNP methodology and instrumentation?•How can one boost polarization levels and polarization build-up times?•How can one minimize polarization losses during sample transfer?
We discuss conceptual and instrumental progress in dissolution DNP since its introduction in 2003. In our view there are three critical steps in the dissolution DNP process: (i) The achievable polarization level in a sample. (ii) The time required to build up the polarization. (iii) The transfer of the sample to the measurement system with minimum loss of polarization. In this review we describe in detail these steps and the different methodological and instrumental implementations, which have been proposed to optimize them.</description><subject>Accumulation</subject><subject>Dissolution</subject><subject>Dissolution DNP</subject><subject>Hardware development</subject><subject>Magnetic resonance</subject><subject>Methodology in dissolution DNP</subject><subject>Polarization</subject><issn>1090-7807</issn><issn>1096-0856</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFkE1LxDAQhoMofqz-AC-yRy-tM2mapHiS9RNEPeg5tOlUsvRjTVrBf2_WVY96mmF43pfhYewYIUVAebZMl51POWCeIk-Biy22j1DIBHQut792SJQGtccOQlgCIOYKdtkelwUHzdU-U4uht7Qap7Kdl309d30Y_dRRP8bDyg-vnkKI13ntQhjaaXRDP798eDpkO03ZBjr6njP2cn31vLhN7h9v7hYX94kVvBgT1KW2GWaSFEkrRIMV8op0RnVj66oR8XlFos6AV2XTWFVKagplBVhCUUA2Y6eb3vjL20RhNJ0Lltq27GmYgkGNEgouM_k_qqTOc50JjChuUOuHEDw1ZuVdV_oPg2DWas3SRLVmrdYgN1FtzJx8109VR_Vv4sdlBM43AEUf7468CdZRtFs7T3Y09eD-qP8EgjqJKg</recordid><startdate>201603</startdate><enddate>201603</enddate><creator>Jähnig, Fabian</creator><creator>Kwiatkowski, Grzegorz</creator><creator>Ernst, Matthias</creator><general>Elsevier Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0002-9538-6086</orcidid></search><sort><creationdate>201603</creationdate><title>Conceptual and instrumental progress in dissolution DNP</title><author>Jähnig, Fabian ; Kwiatkowski, Grzegorz ; Ernst, Matthias</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c429t-18a8c3136e7e6c44f1b12be83edfcdbf42017e4d302baffc7a6ef97c40ce14903</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Accumulation</topic><topic>Dissolution</topic><topic>Dissolution DNP</topic><topic>Hardware development</topic><topic>Magnetic resonance</topic><topic>Methodology in dissolution DNP</topic><topic>Polarization</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jähnig, Fabian</creatorcontrib><creatorcontrib>Kwiatkowski, Grzegorz</creatorcontrib><creatorcontrib>Ernst, Matthias</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of magnetic resonance (1997)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jähnig, Fabian</au><au>Kwiatkowski, Grzegorz</au><au>Ernst, Matthias</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Conceptual and instrumental progress in dissolution DNP</atitle><jtitle>Journal of magnetic resonance (1997)</jtitle><addtitle>J Magn Reson</addtitle><date>2016-03</date><risdate>2016</risdate><volume>264</volume><spage>22</spage><epage>29</epage><pages>22-29</pages><issn>1090-7807</issn><eissn>1096-0856</eissn><abstract>[Display omitted]
•What are key points in dissolution DNP methodology and instrumentation?•How can one boost polarization levels and polarization build-up times?•How can one minimize polarization losses during sample transfer?
We discuss conceptual and instrumental progress in dissolution DNP since its introduction in 2003. In our view there are three critical steps in the dissolution DNP process: (i) The achievable polarization level in a sample. (ii) The time required to build up the polarization. (iii) The transfer of the sample to the measurement system with minimum loss of polarization. In this review we describe in detail these steps and the different methodological and instrumental implementations, which have been proposed to optimize them.</abstract><cop>United States</cop><pub>Elsevier Inc</pub><pmid>26920827</pmid><doi>10.1016/j.jmr.2015.12.024</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0002-9538-6086</orcidid><oa>free_for_read</oa></addata></record> |
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| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Accumulation Dissolution Dissolution DNP Hardware development Magnetic resonance Methodology in dissolution DNP Polarization |
| title | Conceptual and instrumental progress in dissolution DNP |
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