Multiresidue analysis of endocrine-disrupting compounds and perfluorinated sulfates and carboxylic acids in sediments by ultra-high-performance liquid chromatography–tandem mass spectrometry

•Method developed and validated for determining 32 endocrine disruptors in sediments.•Perfluorinated compounds determined with estrogenic compounds for the first time.•Clean up with carbon black cartridge reduced matrix effect keeping good recovery.•A robust matrix matched calibration ensured good t...

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Veröffentlicht in:	Journal of Chromatography A 2016-03, Vol.1438, p.133-142
Hauptverfasser:	Cavaliere, Chiara, Capriotti, Anna Laura, Ferraris, Francesca, Foglia, Patrizia, Samperi, Roberto, Ventura, Salvatore, Laganà, Aldo
Format:	Artikel
Sprache:	eng
Schlagworte:	Bisphenol A Carboxylic Acids - analysis Chromatography Chromatography, High Pressure Liquid Chromatography, Liquid Cleaning Endocrine Disruptors - analysis Endocrine-disrupting compounds Environmental Monitoring - instrumentation Environmental Monitoring - methods Environmental Pollutants - analysis Experimental design Extraction Freshwater Geologic Sediments - chemistry Graphitized carbon black Italy Liquid chromatography–mass spectrometry (LC–MS) Mass spectrometry Recovery Rivers Sediments Solid Phase Extraction Solid phase extraction (SPE) Solvents Sulfates - analysis Tandem Mass Spectrometry
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