Micro-2D-TLC separation of phenolics in some species of mint and their fingerprints on diol bonded polar stationary phase
Micro-thin-layer chromatography in two dimensional (2D-mTLC) mode in normal and reversed phase systems by use of diol bonded stationary phase was applied to make fingerprints of 11 species of Mentha genus and two finished pharmaceutical products. Nonaqueous eluents (propan-2-ol or ethyl acetate diss...
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| Veröffentlicht in: | Acta chromatographica 2016-03, Vol.28 (1), p.119-127 |
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| container_title | Acta chromatographica |
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| creator | Hawrył, M.A. Niemiec, M. Słomka, K. Waksmundzka-Hajnos, M. Szymczak, G. |
| description | Micro-thin-layer chromatography in two dimensional (2D-mTLC) mode in normal and reversed phase systems by use of diol bonded stationary phase was applied to make fingerprints of 11 species of Mentha genus and two finished pharmaceutical products. Nonaqueous eluents (propan-2-ol or ethyl acetate dissolved in n-heptane) were used in normal phase systems. Mixtures of acetonitrile with water were used in reversed phase chromatographic systems. Optimization of one dimensional systems was performed by determining of R sub(F) vs. composition of mobile phases dependencies for standards occurring in various species of Mentha. Most selective eluents were chosen to optimize two-dimensional systems by creating R sub(F) in normal-phase (NP) systems vs. R sub(F) in reversed-phase (RP) systems correlations. 2D-mTLC on diol polar bonded stationary phase were optimized to separate phenolic compounds and make fingerprints of examined plant materials and this method was never applied earlier in the chromatographic analysis. |
| doi_str_mv | 10.1556/AChrom.28.2016.1.9 |
| format | Article |
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Most selective eluents were chosen to optimize two-dimensional systems by creating R sub(F) in normal-phase (NP) systems vs. R sub(F) in reversed-phase (RP) systems correlations. 2D-mTLC on diol polar bonded stationary phase were optimized to separate phenolic compounds and make fingerprints of examined plant materials and this method was never applied earlier in the chromatographic analysis.</description><identifier>ISSN: 1233-2356</identifier><identifier>EISSN: 2083-5736</identifier><identifier>DOI: 10.1556/AChrom.28.2016.1.9</identifier><language>eng</language><publisher>Akademiai Kiado</publisher><subject>Chemical properties ; Composition ; Identification and classification ; Mentha ; Methods ; Mints (Plants) ; Phenols (Class of compounds) ; Thin layer chromatography</subject><ispartof>Acta chromatographica, 2016-03, Vol.28 (1), p.119-127</ispartof><rights>COPYRIGHT 2016 Akademiai Kiado</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c363t-840cad53b99c13624af953064b3c240d048809208a1b76e04048d6f775fae00b3</citedby><cites>FETCH-LOGICAL-c363t-840cad53b99c13624af953064b3c240d048809208a1b76e04048d6f775fae00b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Hawrył, M.A.</creatorcontrib><creatorcontrib>Niemiec, M.</creatorcontrib><creatorcontrib>Słomka, K.</creatorcontrib><creatorcontrib>Waksmundzka-Hajnos, M.</creatorcontrib><creatorcontrib>Szymczak, G.</creatorcontrib><title>Micro-2D-TLC separation of phenolics in some species of mint and their fingerprints on diol bonded polar stationary phase</title><title>Acta chromatographica</title><description>Micro-thin-layer chromatography in two dimensional (2D-mTLC) mode in normal and reversed phase systems by use of diol bonded stationary phase was applied to make fingerprints of 11 species of Mentha genus and two finished pharmaceutical products. 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| ispartof | Acta chromatographica, 2016-03, Vol.28 (1), p.119-127 |
| issn | 1233-2356 2083-5736 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1808734502 |
| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals |
| subjects | Chemical properties Composition Identification and classification Mentha Methods Mints (Plants) Phenols (Class of compounds) Thin layer chromatography |
| title | Micro-2D-TLC separation of phenolics in some species of mint and their fingerprints on diol bonded polar stationary phase |
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