Determination of residual fipronil in chicken egg and muscle by LC–MS/MS

•Fipronil residues in chicken egg and muscle were extracted with acetronitrile.•C18 SPE cartridge was better than common sorbents for purifying fipronil.•A novel and reliable LC–MS/MS method was established to assay fipronil residue.•The CCα for fipronil in chicken egg and muscle was 0.002μgkg−1. A...

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Veröffentlicht in:	Journal of chromatography. B, Analytical technologies in the biomedical and life sciences Analytical technologies in the biomedical and life sciences, 2016-03, Vol.1014, p.31-36
Hauptverfasser:	Zhang, Meiyu, Bian, Kui, Zhou, Tong, Song, Xuqin, Liu, Qingying, Meng, Chenying, He, Limin
Format:	Artikel
Sprache:	eng
Schlagworte:	Animals Calibration Cartridges Chicken Chickens Chickens - metabolism Chromatography Chromatography, High Pressure Liquid - methods Egg Eggs - analysis Fipronil Insecticides - analysis Limit of Detection Liquid chromatography–tandem mass spectrometry Liquids Monitoring Muscles Muscles - chemistry Pyrazoles - analysis Residue Solid Phase Extraction - methods Standard deviation Tandem Mass Spectrometry - methods
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