Synthesis, characterization, and conditions optima for thin film assembly of a light lanthanide nanocomplex
A light lanthanide thin film nanocomplex of Ce(III) with 2-mercaptopyridine-3-carboxylic acid (MPC) was synthesized via the layer-by-layer self-assembly (LbL-SA) chemical deposition method. The synthesized nanolanthanide complex was subjected to a number of analytical measurements to characterize an...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2016-01, Vol.123 (1), p.135-144 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Haggag, Sawsan M. S. Abdel-Hamid, Ibrahim A. M. |
| description | A light lanthanide thin film nanocomplex of Ce(III) with 2-mercaptopyridine-3-carboxylic acid (MPC) was synthesized via the layer-by-layer self-assembly (LbL-SA) chemical deposition method. The synthesized nanolanthanide complex was subjected to a number of analytical measurements to characterize and confirm its structure such as elemental analysis, electron impact mass spectra, FT-IR spectra, and UV–Vis spectra. The morphology and structure of the thin films of MPC ligand and its Ce(III) nanocomplex (CeMPC) were inspected with scanning electron microscopy. The nanothin films of CeMPC were subjected to X-ray powder diffraction analysis. The thermal decomposition of CeMPC nanothin films was studied and discussed. The thermal decomposition included seven steps. The optima of various controlling conditions for thin films of CeMPC nanocomplex assembly via LbL-SA were investigated and discussed. |
| doi_str_mv | 10.1007/s10973-015-4877-5 |
| format | Article |
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S.</creatorcontrib><creatorcontrib>Abdel-Hamid, Ibrahim A. M.</creatorcontrib><title>Synthesis, characterization, and conditions optima for thin film assembly of a light lanthanide nanocomplex</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>A light lanthanide thin film nanocomplex of Ce(III) with 2-mercaptopyridine-3-carboxylic acid (MPC) was synthesized via the layer-by-layer self-assembly (LbL-SA) chemical deposition method. The synthesized nanolanthanide complex was subjected to a number of analytical measurements to characterize and confirm its structure such as elemental analysis, electron impact mass spectra, FT-IR spectra, and UV–Vis spectra. The morphology and structure of the thin films of MPC ligand and its Ce(III) nanocomplex (CeMPC) were inspected with scanning electron microscopy. The nanothin films of CeMPC were subjected to X-ray powder diffraction analysis. The thermal decomposition of CeMPC nanothin films was studied and discussed. The thermal decomposition included seven steps. The optima of various controlling conditions for thin films of CeMPC nanocomplex assembly via LbL-SA were investigated and discussed.</description><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Assembly</subject><subject>Calorimetry</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Dielectric films</subject><subject>Diffraction</subject><subject>Inorganic Chemistry</subject><subject>Lanthanides</subject><subject>Measurement Science and Instrumentation</subject><subject>Nanostructure</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Rare earth metals</subject><subject>Self assembly</subject><subject>Spectra</subject><subject>Thermal decomposition</subject><subject>Thin films</subject><subject>X-rays</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNp9kU9r3DAQxU1IIX_aD5Cbjg3E6ciS1tYxhKQNBAJNexayNNpVYktbSQvZfvpqcS-5hDnMCH5v0LzXNBcUrilA_y1TkD1rgYqWD33fiqPmlIphaDvZrY7rzOq8ogJOmrOcXwBASqCnzevzPpQNZp-viNnopE3B5P_q4mO4IjpYYmKw_vDMJG6LnzVxMZGy8YE4P81E54zzOO1JdESTya83hUy6LtXBWyRBh2jivJ3w7XPzyekp45f__bz5fX_36_ZH-_j0_eH25rE1XLDSGsZoJ6XTIA0wy_tucKNwXHILI1gEKbhApLznXFpu-7EiKyvtCGCBG3befF32blP8s8Nc1Oyzwan-CuMuKzrAAD1QBhW9XtC1nlD54GKpFtSyOPt6OdYTUd1w3g2SCcGr4PKdoDIF38pa73JWD88_37N0YU2KOSd0apuqf2mvKKhDampJTdXU1CE1JaqmWzS5smGNSb3EXQrVrg9E_wBlqJpE</recordid><startdate>20160101</startdate><enddate>20160101</enddate><creator>Haggag, Sawsan M. 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S.</creatorcontrib><creatorcontrib>Abdel-Hamid, Ibrahim A. M.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Haggag, Sawsan M. S.</au><au>Abdel-Hamid, Ibrahim A. 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The morphology and structure of the thin films of MPC ligand and its Ce(III) nanocomplex (CeMPC) were inspected with scanning electron microscopy. The nanothin films of CeMPC were subjected to X-ray powder diffraction analysis. The thermal decomposition of CeMPC nanothin films was studied and discussed. The thermal decomposition included seven steps. The optima of various controlling conditions for thin films of CeMPC nanocomplex assembly via LbL-SA were investigated and discussed.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-015-4877-5</doi><tpages>10</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Analysis Analytical Chemistry Assembly Calorimetry Chemical properties Chemistry Chemistry and Materials Science Dielectric films Diffraction Inorganic Chemistry Lanthanides Measurement Science and Instrumentation Nanostructure Physical Chemistry Polymer Sciences Rare earth metals Self assembly Spectra Thermal decomposition Thin films X-rays |
| title | Synthesis, characterization, and conditions optima for thin film assembly of a light lanthanide nanocomplex |
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