Ex-situ Antimony Screen-printed Carbon Electrode for Voltammetric Determination of Ni(II)-ions in Wastewater
An Ex‐situ antimony film screen‐printed carbon electrode (Ex‐situ SbSPCE) was successfully applied for the determination of Ni(II), by means of adsorptive stripping voltammetry using dimethylglyoxime as complexing agent, in a certified reference wastewater sample. This electrode is proposed as an al...
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| Veröffentlicht in: | Electroanalysis (New York, N.Y.) N.Y.), 2016-03, Vol.28 (3), p.640-644 |
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| container_title | Electroanalysis (New York, N.Y.) |
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| creator | Barceló, Cristian Serrano, Núria Ariño, Cristina Díaz-Cruz, José Manuel Esteban, Miquel |
| description | An Ex‐situ antimony film screen‐printed carbon electrode (Ex‐situ SbSPCE) was successfully applied for the determination of Ni(II), by means of adsorptive stripping voltammetry using dimethylglyoxime as complexing agent, in a certified reference wastewater sample. This electrode is proposed as an alternative to more conventional antimony film electrodes. Ex‐situ SbSPCE was analytically characterized and the obtained parameters suggest that Ex‐situ SbSPCE behaves much better than both Ex‐situ BiSPCE and BispSPE for Ni(II) determination. The results confirm the applicability of Ex‐situ SbSPCE for the determination of low concentration levels of Ni(II) in natural samples with a very high reproducibility and good trueness. |
| doi_str_mv | 10.1002/elan.201500511 |
| format | Article |
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This electrode is proposed as an alternative to more conventional antimony film electrodes. Ex‐situ SbSPCE was analytically characterized and the obtained parameters suggest that Ex‐situ SbSPCE behaves much better than both Ex‐situ BiSPCE and BispSPE for Ni(II) determination. The results confirm the applicability of Ex‐situ SbSPCE for the determination of low concentration levels of Ni(II) in natural samples with a very high reproducibility and good trueness.</description><identifier>ISSN: 1040-0397</identifier><identifier>EISSN: 1521-4109</identifier><identifier>DOI: 10.1002/elan.201500511</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>adsorptive stripping voltammetry ; Antimony ; antimony film electrodes ; Carbon ; Electrodes ; Mathematical analysis ; nickel ; Reproducibility ; screen-printed electrodes ; Stripping ; Voltammetry ; Waste water</subject><ispartof>Electroanalysis (New York, N.Y.), 2016-03, Vol.28 (3), p.640-644</ispartof><rights>2016 WILEY‐VCH Verlag GmbH & Co. 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The results confirm the applicability of Ex‐situ SbSPCE for the determination of low concentration levels of Ni(II) in natural samples with a very high reproducibility and good trueness.</description><subject>adsorptive stripping voltammetry</subject><subject>Antimony</subject><subject>antimony film electrodes</subject><subject>Carbon</subject><subject>Electrodes</subject><subject>Mathematical analysis</subject><subject>nickel</subject><subject>Reproducibility</subject><subject>screen-printed electrodes</subject><subject>Stripping</subject><subject>Voltammetry</subject><subject>Waste water</subject><issn>1040-0397</issn><issn>1521-4109</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFkE1P4zAQQCPESnzsXjn7CAd3x7ETN8dSClSquivBwtFynLFkSGKwXdH-e4y6Qtw4jUd6z9K8ojhjMGEA5W_s9TgpgVUAFWMHxTGrSkYFg-Ywv0EABd7Io-IkxicAaGrRHBf9YkujSxsyG5Mb_LgjdyYgjvQluDFhR-Y6tH4kix5NCr5DYn0gD75PehgwBWfIFSYMgxt1chn0lqzd-XJ5QfMWiRvJo44J33SGfhY_rO4j_vo_T4t_14v7-S1d_blZzmcraoRgjHbTus0n2LZDkNC0vCx5J7XhlklhubGCTxFQSiu6lmNVTnklrWa1AclLVvPT4nz_70vwrxuMSQ0uGuxzIPSbqNgUQEhZNlVGJ3vUBB9jQKvy4YMOO8VAfWRVH1nVZ9YsNHvhzfW4-4ZWi9Vs_dWle9flIttPV4dnVUsuK_W4vlH3l3wl7q7_qoa_A3Cmi1w</recordid><startdate>201603</startdate><enddate>201603</enddate><creator>Barceló, Cristian</creator><creator>Serrano, Núria</creator><creator>Ariño, Cristina</creator><creator>Díaz-Cruz, José Manuel</creator><creator>Esteban, Miquel</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>201603</creationdate><title>Ex-situ Antimony Screen-printed Carbon Electrode for Voltammetric Determination of Ni(II)-ions in Wastewater</title><author>Barceló, Cristian ; Serrano, Núria ; Ariño, Cristina ; Díaz-Cruz, José Manuel ; Esteban, Miquel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4411-d86b051fbde0709b3223d7ac3f174f3cf438e0e77f4db3e528357fa16c0732163</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>adsorptive stripping voltammetry</topic><topic>Antimony</topic><topic>antimony film electrodes</topic><topic>Carbon</topic><topic>Electrodes</topic><topic>Mathematical analysis</topic><topic>nickel</topic><topic>Reproducibility</topic><topic>screen-printed electrodes</topic><topic>Stripping</topic><topic>Voltammetry</topic><topic>Waste water</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Barceló, Cristian</creatorcontrib><creatorcontrib>Serrano, Núria</creatorcontrib><creatorcontrib>Ariño, Cristina</creatorcontrib><creatorcontrib>Díaz-Cruz, José Manuel</creatorcontrib><creatorcontrib>Esteban, Miquel</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Electroanalysis (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Barceló, Cristian</au><au>Serrano, Núria</au><au>Ariño, Cristina</au><au>Díaz-Cruz, José Manuel</au><au>Esteban, Miquel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ex-situ Antimony Screen-printed Carbon Electrode for Voltammetric Determination of Ni(II)-ions in Wastewater</atitle><jtitle>Electroanalysis (New York, N.Y.)</jtitle><addtitle>Electroanalysis</addtitle><date>2016-03</date><risdate>2016</risdate><volume>28</volume><issue>3</issue><spage>640</spage><epage>644</epage><pages>640-644</pages><issn>1040-0397</issn><eissn>1521-4109</eissn><abstract>An Ex‐situ antimony film screen‐printed carbon electrode (Ex‐situ SbSPCE) was successfully applied for the determination of Ni(II), by means of adsorptive stripping voltammetry using dimethylglyoxime as complexing agent, in a certified reference wastewater sample. This electrode is proposed as an alternative to more conventional antimony film electrodes. Ex‐situ SbSPCE was analytically characterized and the obtained parameters suggest that Ex‐situ SbSPCE behaves much better than both Ex‐situ BiSPCE and BispSPE for Ni(II) determination. The results confirm the applicability of Ex‐situ SbSPCE for the determination of low concentration levels of Ni(II) in natural samples with a very high reproducibility and good trueness.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/elan.201500511</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | adsorptive stripping voltammetry Antimony antimony film electrodes Carbon Electrodes Mathematical analysis nickel Reproducibility screen-printed electrodes Stripping Voltammetry Waste water |
| title | Ex-situ Antimony Screen-printed Carbon Electrode for Voltammetric Determination of Ni(II)-ions in Wastewater |
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