A novel approach for extracting cellulose nanofibers from lignocellulosic biomass by ball milling combined with chemical treatment
ABSTRACT Cellulose nanofibers (CNFs) were isolated from kenaf fibers and wheat straw by formic acid (FA)/acetic acid (AA), peroxyformic acid (PFA)/peroxyacetic acid (PAA), hydrogen peroxide (H2O2) treatment; and subsequently through ball milling treatment. Characterization of extracted cellulose and...
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| Veröffentlicht in: | Journal of applied polymer science 2016-03, Vol.133 (9), p.np-n/a |
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| creator | Nuruddin, Md Hosur, Mahesh Uddin, Md. Jamal Baah, David Jeelani, Shaik |
| description | ABSTRACT
Cellulose nanofibers (CNFs) were isolated from kenaf fibers and wheat straw by formic acid (FA)/acetic acid (AA), peroxyformic acid (PFA)/peroxyacetic acid (PAA), hydrogen peroxide (H2O2) treatment; and subsequently through ball milling treatment. Characterization of extracted cellulose and cellulose nanofibers was carried out through Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X‐ray diffraction (XRD), and thermogravimetric analysis (TGA). TEM images showed that extracted cellulose nanofibers had diameter in the range of 8–100 nm. FTIR and XRD results implied that hemicellulose and lignin were mostly removed from lignocellulosic biomass with an increase in crystallinity, and isolation of cellulose nanofibers was successful. The TGA results showed that decomposition temperature of cellulose nanofibers increased by about 27°C when compared with that of untreated lignocellulosic biomass. No significant change was observed in the decomposition temperature of bleached celluloses after ball milling. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 42990. |
| doi_str_mv | 10.1002/app.42990 |
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Cellulose nanofibers (CNFs) were isolated from kenaf fibers and wheat straw by formic acid (FA)/acetic acid (AA), peroxyformic acid (PFA)/peroxyacetic acid (PAA), hydrogen peroxide (H2O2) treatment; and subsequently through ball milling treatment. Characterization of extracted cellulose and cellulose nanofibers was carried out through Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X‐ray diffraction (XRD), and thermogravimetric analysis (TGA). TEM images showed that extracted cellulose nanofibers had diameter in the range of 8–100 nm. FTIR and XRD results implied that hemicellulose and lignin were mostly removed from lignocellulosic biomass with an increase in crystallinity, and isolation of cellulose nanofibers was successful. The TGA results showed that decomposition temperature of cellulose nanofibers increased by about 27°C when compared with that of untreated lignocellulosic biomass. No significant change was observed in the decomposition temperature of bleached celluloses after ball milling. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 42990.</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.42990</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Blackwell Publishing Ltd</publisher><subject>Ball milling ; biodegradable ; Biomass ; Cellulose ; cellulose and other wood products ; Fourier transforms ; Infrared spectroscopy ; Lignocellulose ; Materials science ; Nanofibers ; Polymers ; Transmission electron microscopy ; X-ray</subject><ispartof>Journal of applied polymer science, 2016-03, Vol.133 (9), p.np-n/a</ispartof><rights>2015 Wiley Periodicals, Inc.</rights><rights>2016 Wiley Periodicals, Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4750-631842e92c92fa8fe4b40937be7b772c6b0032058bc0352286aa982ead974da83</citedby><cites>FETCH-LOGICAL-c4750-631842e92c92fa8fe4b40937be7b772c6b0032058bc0352286aa982ead974da83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.42990$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.42990$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids></links><search><creatorcontrib>Nuruddin, Md</creatorcontrib><creatorcontrib>Hosur, Mahesh</creatorcontrib><creatorcontrib>Uddin, Md. Jamal</creatorcontrib><creatorcontrib>Baah, David</creatorcontrib><creatorcontrib>Jeelani, Shaik</creatorcontrib><title>A novel approach for extracting cellulose nanofibers from lignocellulosic biomass by ball milling combined with chemical treatment</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>ABSTRACT
Cellulose nanofibers (CNFs) were isolated from kenaf fibers and wheat straw by formic acid (FA)/acetic acid (AA), peroxyformic acid (PFA)/peroxyacetic acid (PAA), hydrogen peroxide (H2O2) treatment; and subsequently through ball milling treatment. Characterization of extracted cellulose and cellulose nanofibers was carried out through Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X‐ray diffraction (XRD), and thermogravimetric analysis (TGA). TEM images showed that extracted cellulose nanofibers had diameter in the range of 8–100 nm. FTIR and XRD results implied that hemicellulose and lignin were mostly removed from lignocellulosic biomass with an increase in crystallinity, and isolation of cellulose nanofibers was successful. The TGA results showed that decomposition temperature of cellulose nanofibers increased by about 27°C when compared with that of untreated lignocellulosic biomass. No significant change was observed in the decomposition temperature of bleached celluloses after ball milling. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 42990.</description><subject>Ball milling</subject><subject>biodegradable</subject><subject>Biomass</subject><subject>Cellulose</subject><subject>cellulose and other wood products</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Lignocellulose</subject><subject>Materials science</subject><subject>Nanofibers</subject><subject>Polymers</subject><subject>Transmission electron microscopy</subject><subject>X-ray</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNp1kTFvFDEQhS0EEkeg4B9YooFik7G9u7bLU0QCUggpgpBoLNs3m3Pw2oe9R3Itv5y9HKFAoprife_pzQwhrxkcMwB-Yjeb45ZrDU_IgoGWTdtz9ZQsZo01SuvuOXlR6y0AYx30C_JrSVP-iZHOxpKtX9MhF4r3U7F-CumGeoxxG3NFmmzKQ3BYKh1KHmkMNyk_ysFTF_Joa6VuR52NkY4hxoeEPLqQcEXvwrSmfo1j8DbSqaCdRkzTS_JssLHiqz_ziHw5e399-qG5-Hz-8XR50fhWdtD0gqmWo-Ze88GqAVvXghbSoXRSct87AMGhU86D6DhXvbVacbQrLduVVeKIvD3kzov-2GKdzBjqvr9NmLfVMAXQylb1Ykbf_IPe5m1JczvDZCdB9p3YU-8OlC-51oKD2ZQw2rIzDMz-G2Y-qnn4xsyeHNi7EHH3f9Asr64eHc3BEeqE938dtnw3vRSyM18vz03H5KfrS1Dmm_gNCXWcOA</recordid><startdate>20160305</startdate><enddate>20160305</enddate><creator>Nuruddin, Md</creator><creator>Hosur, Mahesh</creator><creator>Uddin, Md. Jamal</creator><creator>Baah, David</creator><creator>Jeelani, Shaik</creator><general>Blackwell Publishing Ltd</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20160305</creationdate><title>A novel approach for extracting cellulose nanofibers from lignocellulosic biomass by ball milling combined with chemical treatment</title><author>Nuruddin, Md ; Hosur, Mahesh ; Uddin, Md. Jamal ; Baah, David ; Jeelani, Shaik</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4750-631842e92c92fa8fe4b40937be7b772c6b0032058bc0352286aa982ead974da83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Ball milling</topic><topic>biodegradable</topic><topic>Biomass</topic><topic>Cellulose</topic><topic>cellulose and other wood products</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Lignocellulose</topic><topic>Materials science</topic><topic>Nanofibers</topic><topic>Polymers</topic><topic>Transmission electron microscopy</topic><topic>X-ray</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nuruddin, Md</creatorcontrib><creatorcontrib>Hosur, Mahesh</creatorcontrib><creatorcontrib>Uddin, Md. Jamal</creatorcontrib><creatorcontrib>Baah, David</creatorcontrib><creatorcontrib>Jeelani, Shaik</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nuruddin, Md</au><au>Hosur, Mahesh</au><au>Uddin, Md. Jamal</au><au>Baah, David</au><au>Jeelani, Shaik</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A novel approach for extracting cellulose nanofibers from lignocellulosic biomass by ball milling combined with chemical treatment</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. Appl. Polym. Sci</addtitle><date>2016-03-05</date><risdate>2016</risdate><volume>133</volume><issue>9</issue><spage>np</spage><epage>n/a</epage><pages>np-n/a</pages><issn>0021-8995</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>ABSTRACT
Cellulose nanofibers (CNFs) were isolated from kenaf fibers and wheat straw by formic acid (FA)/acetic acid (AA), peroxyformic acid (PFA)/peroxyacetic acid (PAA), hydrogen peroxide (H2O2) treatment; and subsequently through ball milling treatment. Characterization of extracted cellulose and cellulose nanofibers was carried out through Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X‐ray diffraction (XRD), and thermogravimetric analysis (TGA). TEM images showed that extracted cellulose nanofibers had diameter in the range of 8–100 nm. FTIR and XRD results implied that hemicellulose and lignin were mostly removed from lignocellulosic biomass with an increase in crystallinity, and isolation of cellulose nanofibers was successful. The TGA results showed that decomposition temperature of cellulose nanofibers increased by about 27°C when compared with that of untreated lignocellulosic biomass. No significant change was observed in the decomposition temperature of bleached celluloses after ball milling. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 42990.</abstract><cop>Hoboken</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1002/app.42990</doi><tpages>11</tpages></addata></record> |
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| subjects | Ball milling biodegradable Biomass Cellulose cellulose and other wood products Fourier transforms Infrared spectroscopy Lignocellulose Materials science Nanofibers Polymers Transmission electron microscopy X-ray |
| title | A novel approach for extracting cellulose nanofibers from lignocellulosic biomass by ball milling combined with chemical treatment |
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