Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route
In this paper, (Ba,Ti)-doped lanthanum silicate nano-sized powders have been synthesized via microwave assisted sol-gel auto-combustion route by using TEOS and lanthanum nitrate as the starting materials, citric acid and glycol as chelators. Both the phase compositions and morphologies of the obtain...
Gespeichert in:
| Veröffentlicht in: | Advanced Materials Research 2013-01, Vol.652-654, p.882-885 |
|---|---|
| Hauptverfasser: | , , , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 885 |
|---|---|
| container_issue | |
| container_start_page | 882 |
| container_title | Advanced Materials Research |
| container_volume | 652-654 |
| creator | Zhang, Ming Tan, Gang Li, Qi Zhao Wu, Ran Ye, Jia Mei Liu, Jun Liang Wang, Sheng Yun Chen, Xiu Lei Yang, Jian Ming |
| description | In this paper, (Ba,Ti)-doped lanthanum silicate nano-sized powders have been synthesized via microwave assisted sol-gel auto-combustion route by using TEOS and lanthanum nitrate as the starting materials, citric acid and glycol as chelators. Both the phase compositions and morphologies of the obtained powders have been characterized. The results indicated that: the synthesized nano powders were characterized as fluffy aggregates with the particle size ranging from 50 to 100nm. As the doping contents of Ba increased, the crystalline sizes decreased and the aggregation were deteriorated, while the particle size decreased from 120nm to 80nm and the aggregation between particles were halted as the doping contents of Ti increased. |
| doi_str_mv | 10.4028/www.scientific.net/AMR.652-654.882 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1800470515</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1800470515</sourcerecordid><originalsourceid>FETCH-LOGICAL-c373t-bbf6ec702cc67b294d591fc7a00b1a18de3f88648d1f8e3e4fc2d6555bdfa3de3</originalsourceid><addsrcrecordid>eNqVkU1v1DAQhi0-JNrCf_CxIJzaTux4j-mWFqRti7rL2XKcseoqG4fYabQ98ssxWiTOHEZzeB-90syD0CdGi4pydbEsSxGthyF5520xQLpobh8KKTiRoiqU4q_QCZOSE7VS4jU6LWlZKyE5Ld_kgPLMSUXfodMYnyiVFePiBP3aHob0CNFHHBw-vzSfd_4juQojdLgZTfIJyO4wAt6YzJlh3uOt7701CfCdGQLZ-peMfg9LB1PEz97gW2-nsJhnIE3MvSnH29CTG-hxM6dA1mHfzjH5MOCHMCd4j94600f48HefoR_XX3brr2Rzf_Nt3WyILesykbZ1EmxNubWybvmq6sSKOVsbSltmmOqgdErJSnXMKSihcpZ3UgjRds6UOT1D58fecQo_Z4hJ73200PdmgDBHzRSlVU0FExm9PKL5khgncHqc_N5MB82o_mNDZxv6nw2dbehsQ2cbeSqdbeSSq2NJmsyQ32Af9VOYpyHf-D81vwHGpJ2P</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1800470515</pqid></control><display><type>article</type><title>Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route</title><source>Scientific.net Journals</source><creator>Zhang, Ming ; Tan, Gang ; Li, Qi Zhao ; Wu, Ran ; Ye, Jia Mei ; Liu, Jun Liang ; Wang, Sheng Yun ; Chen, Xiu Lei ; Yang, Jian Ming</creator><creatorcontrib>Zhang, Ming ; Tan, Gang ; Li, Qi Zhao ; Wu, Ran ; Ye, Jia Mei ; Liu, Jun Liang ; Wang, Sheng Yun ; Chen, Xiu Lei ; Yang, Jian Ming</creatorcontrib><description>In this paper, (Ba,Ti)-doped lanthanum silicate nano-sized powders have been synthesized via microwave assisted sol-gel auto-combustion route by using TEOS and lanthanum nitrate as the starting materials, citric acid and glycol as chelators. Both the phase compositions and morphologies of the obtained powders have been characterized. The results indicated that: the synthesized nano powders were characterized as fluffy aggregates with the particle size ranging from 50 to 100nm. As the doping contents of Ba increased, the crystalline sizes decreased and the aggregation were deteriorated, while the particle size decreased from 120nm to 80nm and the aggregation between particles were halted as the doping contents of Ti increased.</description><identifier>ISSN: 1022-6680</identifier><identifier>ISSN: 1662-8985</identifier><identifier>ISBN: 3037856203</identifier><identifier>ISBN: 9783037856208</identifier><identifier>EISSN: 1662-8985</identifier><identifier>DOI: 10.4028/www.scientific.net/AMR.652-654.882</identifier><language>eng</language><publisher>Trans Tech Publications Ltd</publisher><subject>Agglomeration ; Doping ; Lanthanum ; Nanostructure ; Particle size ; Silicates ; Sol gel process ; Titanium</subject><ispartof>Advanced Materials Research, 2013-01, Vol.652-654, p.882-885</ispartof><rights>2013 Trans Tech Publications Ltd</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c373t-bbf6ec702cc67b294d591fc7a00b1a18de3f88648d1f8e3e4fc2d6555bdfa3de3</citedby><cites>FETCH-LOGICAL-c373t-bbf6ec702cc67b294d591fc7a00b1a18de3f88648d1f8e3e4fc2d6555bdfa3de3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttps://www.scientific.net/Image/TitleCover/2262?width=600</thumbnail><link.rule.ids>314,780,784,27922,27923</link.rule.ids></links><search><creatorcontrib>Zhang, Ming</creatorcontrib><creatorcontrib>Tan, Gang</creatorcontrib><creatorcontrib>Li, Qi Zhao</creatorcontrib><creatorcontrib>Wu, Ran</creatorcontrib><creatorcontrib>Ye, Jia Mei</creatorcontrib><creatorcontrib>Liu, Jun Liang</creatorcontrib><creatorcontrib>Wang, Sheng Yun</creatorcontrib><creatorcontrib>Chen, Xiu Lei</creatorcontrib><creatorcontrib>Yang, Jian Ming</creatorcontrib><title>Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route</title><title>Advanced Materials Research</title><description>In this paper, (Ba,Ti)-doped lanthanum silicate nano-sized powders have been synthesized via microwave assisted sol-gel auto-combustion route by using TEOS and lanthanum nitrate as the starting materials, citric acid and glycol as chelators. Both the phase compositions and morphologies of the obtained powders have been characterized. The results indicated that: the synthesized nano powders were characterized as fluffy aggregates with the particle size ranging from 50 to 100nm. As the doping contents of Ba increased, the crystalline sizes decreased and the aggregation were deteriorated, while the particle size decreased from 120nm to 80nm and the aggregation between particles were halted as the doping contents of Ti increased.</description><subject>Agglomeration</subject><subject>Doping</subject><subject>Lanthanum</subject><subject>Nanostructure</subject><subject>Particle size</subject><subject>Silicates</subject><subject>Sol gel process</subject><subject>Titanium</subject><issn>1022-6680</issn><issn>1662-8985</issn><issn>1662-8985</issn><isbn>3037856203</isbn><isbn>9783037856208</isbn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqVkU1v1DAQhi0-JNrCf_CxIJzaTux4j-mWFqRti7rL2XKcseoqG4fYabQ98ssxWiTOHEZzeB-90syD0CdGi4pydbEsSxGthyF5520xQLpobh8KKTiRoiqU4q_QCZOSE7VS4jU6LWlZKyE5Ld_kgPLMSUXfodMYnyiVFePiBP3aHob0CNFHHBw-vzSfd_4juQojdLgZTfIJyO4wAt6YzJlh3uOt7701CfCdGQLZ-peMfg9LB1PEz97gW2-nsJhnIE3MvSnH29CTG-hxM6dA1mHfzjH5MOCHMCd4j94600f48HefoR_XX3brr2Rzf_Nt3WyILesykbZ1EmxNubWybvmq6sSKOVsbSltmmOqgdErJSnXMKSihcpZ3UgjRds6UOT1D58fecQo_Z4hJ73200PdmgDBHzRSlVU0FExm9PKL5khgncHqc_N5MB82o_mNDZxv6nw2dbehsQ2cbeSqdbeSSq2NJmsyQ32Af9VOYpyHf-D81vwHGpJ2P</recordid><startdate>20130101</startdate><enddate>20130101</enddate><creator>Zhang, Ming</creator><creator>Tan, Gang</creator><creator>Li, Qi Zhao</creator><creator>Wu, Ran</creator><creator>Ye, Jia Mei</creator><creator>Liu, Jun Liang</creator><creator>Wang, Sheng Yun</creator><creator>Chen, Xiu Lei</creator><creator>Yang, Jian Ming</creator><general>Trans Tech Publications Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20130101</creationdate><title>Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route</title><author>Zhang, Ming ; Tan, Gang ; Li, Qi Zhao ; Wu, Ran ; Ye, Jia Mei ; Liu, Jun Liang ; Wang, Sheng Yun ; Chen, Xiu Lei ; Yang, Jian Ming</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c373t-bbf6ec702cc67b294d591fc7a00b1a18de3f88648d1f8e3e4fc2d6555bdfa3de3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Agglomeration</topic><topic>Doping</topic><topic>Lanthanum</topic><topic>Nanostructure</topic><topic>Particle size</topic><topic>Silicates</topic><topic>Sol gel process</topic><topic>Titanium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhang, Ming</creatorcontrib><creatorcontrib>Tan, Gang</creatorcontrib><creatorcontrib>Li, Qi Zhao</creatorcontrib><creatorcontrib>Wu, Ran</creatorcontrib><creatorcontrib>Ye, Jia Mei</creatorcontrib><creatorcontrib>Liu, Jun Liang</creatorcontrib><creatorcontrib>Wang, Sheng Yun</creatorcontrib><creatorcontrib>Chen, Xiu Lei</creatorcontrib><creatorcontrib>Yang, Jian Ming</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Advanced Materials Research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhang, Ming</au><au>Tan, Gang</au><au>Li, Qi Zhao</au><au>Wu, Ran</au><au>Ye, Jia Mei</au><au>Liu, Jun Liang</au><au>Wang, Sheng Yun</au><au>Chen, Xiu Lei</au><au>Yang, Jian Ming</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route</atitle><jtitle>Advanced Materials Research</jtitle><date>2013-01-01</date><risdate>2013</risdate><volume>652-654</volume><spage>882</spage><epage>885</epage><pages>882-885</pages><issn>1022-6680</issn><issn>1662-8985</issn><eissn>1662-8985</eissn><isbn>3037856203</isbn><isbn>9783037856208</isbn><abstract>In this paper, (Ba,Ti)-doped lanthanum silicate nano-sized powders have been synthesized via microwave assisted sol-gel auto-combustion route by using TEOS and lanthanum nitrate as the starting materials, citric acid and glycol as chelators. Both the phase compositions and morphologies of the obtained powders have been characterized. The results indicated that: the synthesized nano powders were characterized as fluffy aggregates with the particle size ranging from 50 to 100nm. As the doping contents of Ba increased, the crystalline sizes decreased and the aggregation were deteriorated, while the particle size decreased from 120nm to 80nm and the aggregation between particles were halted as the doping contents of Ti increased.</abstract><pub>Trans Tech Publications Ltd</pub><doi>10.4028/www.scientific.net/AMR.652-654.882</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1022-6680 |
| ispartof | Advanced Materials Research, 2013-01, Vol.652-654, p.882-885 |
| issn | 1022-6680 1662-8985 1662-8985 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1800470515 |
| source | Scientific.net Journals |
| subjects | Agglomeration Doping Lanthanum Nanostructure Particle size Silicates Sol gel process Titanium |
| title | Synthesis of (Ba,Ti)-Doped Apatite-Type Lanthanum Silicate Nano-Sized Powders via Microwave-Assisted Sol-Gel Auto-Combustion Route |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-09T15%3A55%3A21IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Synthesis%20of%20(Ba,Ti)-Doped%20Apatite-Type%20Lanthanum%20Silicate%20Nano-Sized%20Powders%20via%20Microwave-Assisted%20Sol-Gel%20Auto-Combustion%20Route&rft.jtitle=Advanced%20Materials%20Research&rft.au=Zhang,%20Ming&rft.date=2013-01-01&rft.volume=652-654&rft.spage=882&rft.epage=885&rft.pages=882-885&rft.issn=1022-6680&rft.eissn=1662-8985&rft.isbn=3037856203&rft.isbn_list=9783037856208&rft_id=info:doi/10.4028/www.scientific.net/AMR.652-654.882&rft_dat=%3Cproquest_cross%3E1800470515%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1800470515&rft_id=info:pmid/&rfr_iscdi=true |