Fabrication and deformation of aluminum–manganese microsandwich structure
The combination of low areal density, high flexural rigidity, and open architecture makes metallic microsandwiching a promising candidate for structural frameworks in small-scale multifunctional devices. We demonstrate a one-step electrodeposition procedure to synthesize an aluminum–manganese (Al–Mn...
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Veröffentlicht in: | Journal of materials research 2016-02, Vol.31 (4), p.480-487 |
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creator | Mraied, Hesham Tran, Thanh Hai Cai, Wenjun |
description | The combination of low areal density, high flexural rigidity, and open architecture makes metallic microsandwiching a promising candidate for structural frameworks in small-scale multifunctional devices. We demonstrate a one-step electrodeposition procedure to synthesize an aluminum–manganese (Al–Mn) microsandwich using a porous polycarbonate (PC) membrane template from room-temperature ionic liquid. Mn was added to refine the microstructure and increase the hardness of Al. A cyclic voltammogram study shows Mn codeposit with Al in an acidic chloroaluminate electrolyte. Increasing the MnCl2 concentration in the electrolyte from 0.05 to 0.25 M promoted a crystalline to amorphous phase transition of the deposited structures. Finally, mechanical properties and damage resistance of the microsandwiches were evaluated using nano- and micro-indentation tests as well as finite element methods. |
doi_str_mv | 10.1557/jmr.2016.28 |
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We demonstrate a one-step electrodeposition procedure to synthesize an aluminum–manganese (Al–Mn) microsandwich using a porous polycarbonate (PC) membrane template from room-temperature ionic liquid. Mn was added to refine the microstructure and increase the hardness of Al. A cyclic voltammogram study shows Mn codeposit with Al in an acidic chloroaluminate electrolyte. Increasing the MnCl2 concentration in the electrolyte from 0.05 to 0.25 M promoted a crystalline to amorphous phase transition of the deposited structures. 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Mater. Res</addtitle><description>The combination of low areal density, high flexural rigidity, and open architecture makes metallic microsandwiching a promising candidate for structural frameworks in small-scale multifunctional devices. We demonstrate a one-step electrodeposition procedure to synthesize an aluminum–manganese (Al–Mn) microsandwich using a porous polycarbonate (PC) membrane template from room-temperature ionic liquid. Mn was added to refine the microstructure and increase the hardness of Al. A cyclic voltammogram study shows Mn codeposit with Al in an acidic chloroaluminate electrolyte. Increasing the MnCl2 concentration in the electrolyte from 0.05 to 0.25 M promoted a crystalline to amorphous phase transition of the deposited structures. Finally, mechanical properties and damage resistance of the microsandwiches were evaluated using nano- and micro-indentation tests as well as finite element methods.</description><subject>Aluminum</subject><subject>Aluminum manganese alloys</subject><subject>Analysis</subject><subject>Applied and Technical Physics</subject><subject>Biomaterials</subject><subject>Chemical synthesis</subject><subject>Density</subject><subject>Devices</subject><subject>Electrodes</subject><subject>Electrolytes</subject><subject>Inorganic Chemistry</subject><subject>Ion beams</subject><subject>Manganese</subject><subject>Materials Engineering</subject><subject>Materials research</subject><subject>Materials Science</subject><subject>Metals</subject><subject>Microscopy</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Open architectures</subject><subject>Phase transitions</subject><subject>Plasma etching</subject><subject>Polycarbonate resins</subject><subject>Polycarbonates</subject><subject>Scanning electron microscopy</subject><subject>Studies</subject><issn>0884-2914</issn><issn>2044-5326</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp90M1KxDAUBeAgCo6jK1-g4EbQjrlp_rqUwVFxwM3sQyZNxw5NOyYt4s538A19ElM6CxFxdQl8nNx7EDoHPAPGxM3W-RnBwGdEHqAJwZSmLCP8EE2wlDQlOdBjdBLCFmNgWNAJelrota-M7qq2SXRTJIUtW-_Gd1smuu5d1fTu6-PT6WajGxts4irj2xD1W2VektD53nS9t6foqNR1sGf7OUWrxd1q_pAun-8f57fL1NAs71LQlkimGSW04FjIvMCES4ozaSAXXBRrblgODLAuIKfEcAp5WXJMmWQgsym6HGN3vn3tbeiUq4KxdR2Xa_ugQOJIBfA80otfdNv2vonLKRBcEppxAVFdjWq4Knhbqp2vnPbvCrAaelWxVzX0qsjw_fWoQ1TNxvofmX_ydB-uXWy62Nj__TeUVIiU</recordid><startdate>20160229</startdate><enddate>20160229</enddate><creator>Mraied, Hesham</creator><creator>Tran, Thanh Hai</creator><creator>Cai, Wenjun</creator><general>Cambridge University Press</general><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0U~</scope><scope>1-H</scope><scope>3V.</scope><scope>7SR</scope><scope>7WY</scope><scope>7WZ</scope><scope>7XB</scope><scope>87Z</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8FL</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FRNLG</scope><scope>F~G</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>K60</scope><scope>K6~</scope><scope>KB.</scope><scope>L.-</scope><scope>L.0</scope><scope>M0C</scope><scope>PDBOC</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope><scope>S0W</scope></search><sort><creationdate>20160229</creationdate><title>Fabrication and deformation of aluminum–manganese microsandwich structure</title><author>Mraied, Hesham ; Tran, Thanh Hai ; Cai, Wenjun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c439t-1ae285a5424d60789d02684038c19767db6c591510ad1942c6419ff604585183</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Aluminum</topic><topic>Aluminum manganese alloys</topic><topic>Analysis</topic><topic>Applied and Technical Physics</topic><topic>Biomaterials</topic><topic>Chemical synthesis</topic><topic>Density</topic><topic>Devices</topic><topic>Electrodes</topic><topic>Electrolytes</topic><topic>Inorganic Chemistry</topic><topic>Ion beams</topic><topic>Manganese</topic><topic>Materials Engineering</topic><topic>Materials research</topic><topic>Materials Science</topic><topic>Metals</topic><topic>Microscopy</topic><topic>Nanostructure</topic><topic>Nanotechnology</topic><topic>Open architectures</topic><topic>Phase transitions</topic><topic>Plasma etching</topic><topic>Polycarbonate resins</topic><topic>Polycarbonates</topic><topic>Scanning electron microscopy</topic><topic>Studies</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mraied, Hesham</creatorcontrib><creatorcontrib>Tran, Thanh Hai</creatorcontrib><creatorcontrib>Cai, Wenjun</creatorcontrib><collection>CrossRef</collection><collection>Global News & ABI/Inform Professional</collection><collection>Trade PRO</collection><collection>ProQuest Central (Corporate)</collection><collection>Engineered Materials Abstracts</collection><collection>ABI/INFORM Collection</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Business Premium Collection (Alumni)</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>Materials Science Database</collection><collection>ABI/INFORM Professional Advanced</collection><collection>ABI/INFORM Professional Standard</collection><collection>ABI/INFORM Global</collection><collection>Materials Science Collection</collection><collection>ProQuest One Business</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mraied, Hesham</au><au>Tran, Thanh Hai</au><au>Cai, Wenjun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Fabrication and deformation of aluminum–manganese microsandwich structure</atitle><jtitle>Journal of materials research</jtitle><stitle>Journal of Materials Research</stitle><addtitle>J. Mater. Res</addtitle><date>2016-02-29</date><risdate>2016</risdate><volume>31</volume><issue>4</issue><spage>480</spage><epage>487</epage><pages>480-487</pages><issn>0884-2914</issn><eissn>2044-5326</eissn><coden>JMREEE</coden><abstract>The combination of low areal density, high flexural rigidity, and open architecture makes metallic microsandwiching a promising candidate for structural frameworks in small-scale multifunctional devices. We demonstrate a one-step electrodeposition procedure to synthesize an aluminum–manganese (Al–Mn) microsandwich using a porous polycarbonate (PC) membrane template from room-temperature ionic liquid. Mn was added to refine the microstructure and increase the hardness of Al. A cyclic voltammogram study shows Mn codeposit with Al in an acidic chloroaluminate electrolyte. Increasing the MnCl2 concentration in the electrolyte from 0.05 to 0.25 M promoted a crystalline to amorphous phase transition of the deposited structures. 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subjects | Aluminum Aluminum manganese alloys Analysis Applied and Technical Physics Biomaterials Chemical synthesis Density Devices Electrodes Electrolytes Inorganic Chemistry Ion beams Manganese Materials Engineering Materials research Materials Science Metals Microscopy Nanostructure Nanotechnology Open architectures Phase transitions Plasma etching Polycarbonate resins Polycarbonates Scanning electron microscopy Studies |
title | Fabrication and deformation of aluminum–manganese microsandwich structure |
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