Separation of Be and Al for AMS using single-step column chromatography
With the aim of simplifying AMS target preparation procedures for TCN measurements we tested a new extraction chromatography approach which couples an anion exchange resin (WBEC) to a chelating resin (Beryllium resin) to separate Be and Al from dissolved quartz samples. Results show that WBEC–Beryll...
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| Veröffentlicht in: | Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms Beam interactions with materials and atoms, 2015-10, Vol.361, p.397-401 |
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| container_title | Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms |
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| creator | Binnie, Steven A. Dunai, Tibor J. Voronina, Elena Goral, Tomasz Heinze, Stefan Dewald, Alfred |
| description | With the aim of simplifying AMS target preparation procedures for TCN measurements we tested a new extraction chromatography approach which couples an anion exchange resin (WBEC) to a chelating resin (Beryllium resin) to separate Be and Al from dissolved quartz samples. Results show that WBEC–Beryllium resin stacks can be used to provide high purity Be and Al separations using a combination of hydrochloric/oxalic and nitric acid elutions. 10Be and 26Al concentrations from quartz samples prepared using more standard procedures are compared with results from replicate samples prepared using the coupled WBEC–Beryllium resin approach and show good agreement. The new column procedure is performed in a single step, reducing sample preparation times relative to more traditional methods of TCN target production. |
| doi_str_mv | 10.1016/j.nimb.2015.03.069 |
| format | Article |
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| identifier | ISSN: 0168-583X |
| ispartof | Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 2015-10, Vol.361, p.397-401 |
| issn | 0168-583X 1872-9584 |
| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | 10-Be 26-Al Aluminum AMS target preparation Column chromatography Cosmogenic nuclides Dissolution Exchange Extraction Polymers Quartz Resins Separation |
| title | Separation of Be and Al for AMS using single-step column chromatography |
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