Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach
A novel and selective approach to obtain highly stable and capping nanospheres of crystalline cadmium sulfide (CdS) via solution growth in cadmium nitrate tetrahydrate-thiourea-ligand-pH buffer systems using a Taguchi experimental design is presented. CdS characterization is carried out by laser dif...
Gespeichert in:
| Veröffentlicht in: | Optical materials express 2014-01, Vol.4 (1), p.129-141 |
|---|---|
| Hauptverfasser: | , , , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 141 |
|---|---|
| container_issue | 1 |
| container_start_page | 129 |
| container_title | Optical materials express |
| container_volume | 4 |
| creator | Leal-Cruz, A. L. Vera-Marquina, A. Berman-Mendoza, D. VillaVelázquez-Mendoza, C. Zaldívar-Huerta, I. E. García-Delgado, L. A. García-Juárez, A. Gómez-Fuentes, R. Rojas-Hernández, A. G. |
| description | A novel and selective approach to obtain highly stable and capping nanospheres of crystalline cadmium sulfide (CdS) via solution growth in cadmium nitrate tetrahydrate-thiourea-ligand-pH buffer systems using a Taguchi experimental design is presented. CdS characterization is carried out by laser diffraction particle size analyzer, X-ray diffraction, scanning electron microscope/energy dispersive X-ray spectroscopy, and UV-Vis absorption spectroscopy. Synthesized nanospheres of crystalline CdS with an average crystal particle diameter of 37.5 nm and a capping layer thickness of 17.7-35.7 nm (73 to 115 nm as capped nanoparticles) keep size and form stable in aqueous solution. These crystalline CdS nanospheres exhibit a 2.46 eV band gap, as well as, an optical bandwidth comprises in the visible range with potential applications in solar cells. |
| doi_str_mv | 10.1364/OME.4.000129 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1793290981</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1793290981</sourcerecordid><originalsourceid>FETCH-LOGICAL-c306t-5612109dda87637c0a0d6ea141ef268555b5b6ed7a8486fbe063ee345b8540253</originalsourceid><addsrcrecordid>eNpNkMtOwzAQRS0EElXpjg_wkgUpfsROskRVeUitugDW0cSZECM3CbZTqXw9gbJgNVe6R3ekQ8g1Z0sudXq3266X6ZIxxkVxRmaCqyKRhWTn__IlWYTwMTFMaZELMSNxa43vQ_SjiaMHR6GraT9Ea6ZsWvBgInr7BdH2XaB9Q1v73rojDREqh7SDrg9Dix5_S-OPU-Gc7ZCu6hd6sEADOjTRHpDCMPgeTHtFLhpwARd_d07eHtavq6dks3t8Xt1vEiOZjonSXHBW1DXkmZaZYcBqjcBTjo3QuVKqUpXGOoM8zXVTIdMSUaaqylXKhJJzcnPand5-jhhiubfBoHPQYT-GkmeFFAUrcj6htyf0x0bw2JSDt3vwx5Kz8sdvOfkt0_LkV34D1plvNg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1793290981</pqid></control><display><type>article</type><title>Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach</title><source>DOAJ Directory of Open Access Journals</source><source>EZB-FREE-00999 freely available EZB journals</source><creator>Leal-Cruz, A. L. ; Vera-Marquina, A. ; Berman-Mendoza, D. ; VillaVelázquez-Mendoza, C. ; Zaldívar-Huerta, I. E. ; García-Delgado, L. A. ; García-Juárez, A. ; Gómez-Fuentes, R. ; Rojas-Hernández, A. G.</creator><creatorcontrib>Leal-Cruz, A. L. ; Vera-Marquina, A. ; Berman-Mendoza, D. ; VillaVelázquez-Mendoza, C. ; Zaldívar-Huerta, I. E. ; García-Delgado, L. A. ; García-Juárez, A. ; Gómez-Fuentes, R. ; Rojas-Hernández, A. G.</creatorcontrib><description>A novel and selective approach to obtain highly stable and capping nanospheres of crystalline cadmium sulfide (CdS) via solution growth in cadmium nitrate tetrahydrate-thiourea-ligand-pH buffer systems using a Taguchi experimental design is presented. CdS characterization is carried out by laser diffraction particle size analyzer, X-ray diffraction, scanning electron microscope/energy dispersive X-ray spectroscopy, and UV-Vis absorption spectroscopy. Synthesized nanospheres of crystalline CdS with an average crystal particle diameter of 37.5 nm and a capping layer thickness of 17.7-35.7 nm (73 to 115 nm as capped nanoparticles) keep size and form stable in aqueous solution. These crystalline CdS nanospheres exhibit a 2.46 eV band gap, as well as, an optical bandwidth comprises in the visible range with potential applications in solar cells.</description><identifier>ISSN: 2159-3930</identifier><identifier>EISSN: 2159-3930</identifier><identifier>DOI: 10.1364/OME.4.000129</identifier><language>eng</language><subject>Cadmium ; Cadmium sulfides ; Capping ; Crystal structure ; Design analysis ; Diffraction ; Nanospheres ; Scanning electron microscopy</subject><ispartof>Optical materials express, 2014-01, Vol.4 (1), p.129-141</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c306t-5612109dda87637c0a0d6ea141ef268555b5b6ed7a8486fbe063ee345b8540253</citedby><cites>FETCH-LOGICAL-c306t-5612109dda87637c0a0d6ea141ef268555b5b6ed7a8486fbe063ee345b8540253</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,860,27903,27904</link.rule.ids></links><search><creatorcontrib>Leal-Cruz, A. L.</creatorcontrib><creatorcontrib>Vera-Marquina, A.</creatorcontrib><creatorcontrib>Berman-Mendoza, D.</creatorcontrib><creatorcontrib>VillaVelázquez-Mendoza, C.</creatorcontrib><creatorcontrib>Zaldívar-Huerta, I. E.</creatorcontrib><creatorcontrib>García-Delgado, L. A.</creatorcontrib><creatorcontrib>García-Juárez, A.</creatorcontrib><creatorcontrib>Gómez-Fuentes, R.</creatorcontrib><creatorcontrib>Rojas-Hernández, A. G.</creatorcontrib><title>Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach</title><title>Optical materials express</title><description>A novel and selective approach to obtain highly stable and capping nanospheres of crystalline cadmium sulfide (CdS) via solution growth in cadmium nitrate tetrahydrate-thiourea-ligand-pH buffer systems using a Taguchi experimental design is presented. CdS characterization is carried out by laser diffraction particle size analyzer, X-ray diffraction, scanning electron microscope/energy dispersive X-ray spectroscopy, and UV-Vis absorption spectroscopy. Synthesized nanospheres of crystalline CdS with an average crystal particle diameter of 37.5 nm and a capping layer thickness of 17.7-35.7 nm (73 to 115 nm as capped nanoparticles) keep size and form stable in aqueous solution. These crystalline CdS nanospheres exhibit a 2.46 eV band gap, as well as, an optical bandwidth comprises in the visible range with potential applications in solar cells.</description><subject>Cadmium</subject><subject>Cadmium sulfides</subject><subject>Capping</subject><subject>Crystal structure</subject><subject>Design analysis</subject><subject>Diffraction</subject><subject>Nanospheres</subject><subject>Scanning electron microscopy</subject><issn>2159-3930</issn><issn>2159-3930</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNpNkMtOwzAQRS0EElXpjg_wkgUpfsROskRVeUitugDW0cSZECM3CbZTqXw9gbJgNVe6R3ekQ8g1Z0sudXq3266X6ZIxxkVxRmaCqyKRhWTn__IlWYTwMTFMaZELMSNxa43vQ_SjiaMHR6GraT9Ea6ZsWvBgInr7BdH2XaB9Q1v73rojDREqh7SDrg9Dix5_S-OPU-Gc7ZCu6hd6sEADOjTRHpDCMPgeTHtFLhpwARd_d07eHtavq6dks3t8Xt1vEiOZjonSXHBW1DXkmZaZYcBqjcBTjo3QuVKqUpXGOoM8zXVTIdMSUaaqylXKhJJzcnPand5-jhhiubfBoHPQYT-GkmeFFAUrcj6htyf0x0bw2JSDt3vwx5Kz8sdvOfkt0_LkV34D1plvNg</recordid><startdate>20140101</startdate><enddate>20140101</enddate><creator>Leal-Cruz, A. L.</creator><creator>Vera-Marquina, A.</creator><creator>Berman-Mendoza, D.</creator><creator>VillaVelázquez-Mendoza, C.</creator><creator>Zaldívar-Huerta, I. E.</creator><creator>García-Delgado, L. A.</creator><creator>García-Juárez, A.</creator><creator>Gómez-Fuentes, R.</creator><creator>Rojas-Hernández, A. G.</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7U5</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20140101</creationdate><title>Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach</title><author>Leal-Cruz, A. L. ; Vera-Marquina, A. ; Berman-Mendoza, D. ; VillaVelázquez-Mendoza, C. ; Zaldívar-Huerta, I. E. ; García-Delgado, L. A. ; García-Juárez, A. ; Gómez-Fuentes, R. ; Rojas-Hernández, A. G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c306t-5612109dda87637c0a0d6ea141ef268555b5b6ed7a8486fbe063ee345b8540253</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Cadmium</topic><topic>Cadmium sulfides</topic><topic>Capping</topic><topic>Crystal structure</topic><topic>Design analysis</topic><topic>Diffraction</topic><topic>Nanospheres</topic><topic>Scanning electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Leal-Cruz, A. L.</creatorcontrib><creatorcontrib>Vera-Marquina, A.</creatorcontrib><creatorcontrib>Berman-Mendoza, D.</creatorcontrib><creatorcontrib>VillaVelázquez-Mendoza, C.</creatorcontrib><creatorcontrib>Zaldívar-Huerta, I. E.</creatorcontrib><creatorcontrib>García-Delgado, L. A.</creatorcontrib><creatorcontrib>García-Juárez, A.</creatorcontrib><creatorcontrib>Gómez-Fuentes, R.</creatorcontrib><creatorcontrib>Rojas-Hernández, A. G.</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Optical materials express</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Leal-Cruz, A. L.</au><au>Vera-Marquina, A.</au><au>Berman-Mendoza, D.</au><au>VillaVelázquez-Mendoza, C.</au><au>Zaldívar-Huerta, I. E.</au><au>García-Delgado, L. A.</au><au>García-Juárez, A.</au><au>Gómez-Fuentes, R.</au><au>Rojas-Hernández, A. G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach</atitle><jtitle>Optical materials express</jtitle><date>2014-01-01</date><risdate>2014</risdate><volume>4</volume><issue>1</issue><spage>129</spage><epage>141</epage><pages>129-141</pages><issn>2159-3930</issn><eissn>2159-3930</eissn><abstract>A novel and selective approach to obtain highly stable and capping nanospheres of crystalline cadmium sulfide (CdS) via solution growth in cadmium nitrate tetrahydrate-thiourea-ligand-pH buffer systems using a Taguchi experimental design is presented. CdS characterization is carried out by laser diffraction particle size analyzer, X-ray diffraction, scanning electron microscope/energy dispersive X-ray spectroscopy, and UV-Vis absorption spectroscopy. Synthesized nanospheres of crystalline CdS with an average crystal particle diameter of 37.5 nm and a capping layer thickness of 17.7-35.7 nm (73 to 115 nm as capped nanoparticles) keep size and form stable in aqueous solution. These crystalline CdS nanospheres exhibit a 2.46 eV band gap, as well as, an optical bandwidth comprises in the visible range with potential applications in solar cells.</abstract><doi>10.1364/OME.4.000129</doi><tpages>13</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2159-3930 |
| ispartof | Optical materials express, 2014-01, Vol.4 (1), p.129-141 |
| issn | 2159-3930 2159-3930 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1793290981 |
| source | DOAJ Directory of Open Access Journals; EZB-FREE-00999 freely available EZB journals |
| subjects | Cadmium Cadmium sulfides Capping Crystal structure Design analysis Diffraction Nanospheres Scanning electron microscopy |
| title | Microstructural and optical characterizations of highly stable nanospheres of crystalline CdS via selective approach |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T10%3A15%3A26IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Microstructural%20and%20optical%20characterizations%20of%20highly%20stable%20nanospheres%20of%20crystalline%20CdS%20via%20selective%20approach&rft.jtitle=Optical%20materials%20express&rft.au=Leal-Cruz,%20A.%20L.&rft.date=2014-01-01&rft.volume=4&rft.issue=1&rft.spage=129&rft.epage=141&rft.pages=129-141&rft.issn=2159-3930&rft.eissn=2159-3930&rft_id=info:doi/10.1364/OME.4.000129&rft_dat=%3Cproquest_cross%3E1793290981%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1793290981&rft_id=info:pmid/&rfr_iscdi=true |