Use of multivariate statistical techniques to optimize the separation of 17 capsinoids by ultra performance liquid chromatography using different columns

In this work a multivariate statistical tool (Derringer and Suich optimization) was proposed for the separation of seventeen capsinoids (natural and synthetic) using the UHPLC-DAD chromatography. Capsinoids were analyzed at 280nm. The variables optimized were the mobile phase (water (0.1% acetic aci...

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Veröffentlicht in:	Talanta (Oxford) 2015-03, Vol.134, p.256-263
Hauptverfasser:	Coutinho, Janclei P., Barbero, Gerardo F., Avellán, Oreto F., Garcés-Claver, A., Godoy, Helena T., Palma, Miguel, Barroso, Carmelo G.
Format:	Artikel
Sprache:	eng
Schlagworte:	Acetonitrile Capsaicin - analogs & derivatives Capsaicin - isolation & purification Capsicum - chemistry Capsinoids Chromatography Chromatography, High Pressure Liquid - instrumentation Chromatography, High Pressure Liquid - methods Derringer and Suich optimization Factor Analysis, Statistical Flow rate Limit of Detection Multivariate statistical technique Optimization Peppers Reproducibility Reproducibility of Results Samples Separation Solvents UHPLC
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