Evaluating nuclear magnetic resonance (NMR) as a robust reference method for online spectroscopic measurement of water holding capacity (WHC)
The potential of using NMR as a reference method for WHC measurement in porcine longissimus dorsi was investigated. The accuracy of NMR when measuring small water changes was assessed in a model system and in muscles. Visible/near infrared (Vis/NIR) and X-ray were used as potential online spectrosco...
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| Veröffentlicht in: | Journal of food engineering 2016-04, Vol.175, p.51-57 |
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| creator | Zhu, Han O'Farrell, Marion Bouquet, Gregory Lunde, Kathrine Egelandsdal, Bjørg Alvseike, Ole Berg, Per Gjerlaug-Enger, Eli Hansen, Eddy W. |
| description | The potential of using NMR as a reference method for WHC measurement in porcine longissimus dorsi was investigated. The accuracy of NMR when measuring small water changes was assessed in a model system and in muscles. Visible/near infrared (Vis/NIR) and X-ray were used as potential online spectroscopic methods to assess WHC on 40 muscles. Drip loss and spin–spin relaxation were also measured. Calibration models were built using partial least squares regression (PLSR) with Vis/NIR or X-ray spectra as input and NMR or drip loss values as output. The slowest spin–spin relaxation time (T22) showed higher correlation with both Vis/NIR (RCV2 = 0.66) and X-ray spectra (RCV2 = 0.76) than EZ-DripLoss values, demonstrating NMR has potential as a reference method for WHC measurement. NMR was more robust against variation along the length of the muscle when compared to the EZ-DripLoss method.
•NMR accurately measures water mass.•The slowest spin–spin relaxation time (T22) showed higher correlation with both Vis/NIR and X-ray spectra than drip loss values.•Only NMR was independent on slice number and had the lowest absolute error. |
| doi_str_mv | 10.1016/j.jfoodeng.2015.12.003 |
| format | Article |
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•NMR accurately measures water mass.•The slowest spin–spin relaxation time (T22) showed higher correlation with both Vis/NIR and X-ray spectra than drip loss values.•Only NMR was independent on slice number and had the lowest absolute error.</description><subject>EZ-DripLoss</subject><subject>Infrared</subject><subject>Muscles</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Online</subject><subject>Porcine longissimus dorsi muscles</subject><subject>Spectra</subject><subject>Spectroscopic analysis</subject><subject>Spectroscopy</subject><subject>Vis/NIR spectroscopy</subject><subject>Water holding capacity</subject><subject>X-ray transmission</subject><subject>X-rays</subject><issn>0260-8774</issn><issn>1873-5770</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFkMtu1DAUhiMEEkPhFZCX00XCsXOxZwcaFYpUQEIglpZjH089SuxgO0V9CN4ZRwNrVmfxX47-r6peU2go0OHNuTnbEAz6U8OA9g1lDUD7pNpRwdu65xyeVjtgA9SC8-559SKlMwD0wNiu-n3zoKZVZedPxK96QhXJrE4es9MkYgpeeY1k__nT12uiElEkhnFNuWgWI27ajPk-GGJDJMFPziNJC-ocQ9JhKS0zqrRGnNFnEiz5pTJGch8ms_3UalHa5Uey_3F7vH5ZPbNqSvjq772qvr-_-Xa8re--fPh4fHdX665nuRaHURhlwAA72IEL0ytoheCoRsZH7KhldhxbdRiLr0NqBzAoGMLYM8bF0F5V-0vvEsPPFVOWs0sap0l5DGuSlB9a1nEGrFiHi1WXQamslkt0s4qPkoLc-Muz_MdfbvwlZbLwL8G3lyCWIQ8Oo0zabcCMiwWPNMH9r-IPP7GUsA</recordid><startdate>20160401</startdate><enddate>20160401</enddate><creator>Zhu, Han</creator><creator>O'Farrell, Marion</creator><creator>Bouquet, Gregory</creator><creator>Lunde, Kathrine</creator><creator>Egelandsdal, Bjørg</creator><creator>Alvseike, Ole</creator><creator>Berg, Per</creator><creator>Gjerlaug-Enger, Eli</creator><creator>Hansen, Eddy W.</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope></search><sort><creationdate>20160401</creationdate><title>Evaluating nuclear magnetic resonance (NMR) as a robust reference method for online spectroscopic measurement of water holding capacity (WHC)</title><author>Zhu, Han ; O'Farrell, Marion ; Bouquet, Gregory ; Lunde, Kathrine ; Egelandsdal, Bjørg ; Alvseike, Ole ; Berg, Per ; Gjerlaug-Enger, Eli ; Hansen, Eddy W.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c452t-89b8dad0d029f678d5a03887eab27be41f2fbb3a9bb8d4e1f60de82e0b5227863</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>EZ-DripLoss</topic><topic>Infrared</topic><topic>Muscles</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Online</topic><topic>Porcine longissimus dorsi muscles</topic><topic>Spectra</topic><topic>Spectroscopic analysis</topic><topic>Spectroscopy</topic><topic>Vis/NIR spectroscopy</topic><topic>Water holding capacity</topic><topic>X-ray transmission</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhu, Han</creatorcontrib><creatorcontrib>O'Farrell, Marion</creatorcontrib><creatorcontrib>Bouquet, Gregory</creatorcontrib><creatorcontrib>Lunde, Kathrine</creatorcontrib><creatorcontrib>Egelandsdal, Bjørg</creatorcontrib><creatorcontrib>Alvseike, Ole</creatorcontrib><creatorcontrib>Berg, Per</creatorcontrib><creatorcontrib>Gjerlaug-Enger, Eli</creatorcontrib><creatorcontrib>Hansen, Eddy W.</creatorcontrib><collection>CrossRef</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><jtitle>Journal of food engineering</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhu, Han</au><au>O'Farrell, Marion</au><au>Bouquet, Gregory</au><au>Lunde, Kathrine</au><au>Egelandsdal, Bjørg</au><au>Alvseike, Ole</au><au>Berg, Per</au><au>Gjerlaug-Enger, Eli</au><au>Hansen, Eddy W.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Evaluating nuclear magnetic resonance (NMR) as a robust reference method for online spectroscopic measurement of water holding capacity (WHC)</atitle><jtitle>Journal of food engineering</jtitle><date>2016-04-01</date><risdate>2016</risdate><volume>175</volume><spage>51</spage><epage>57</epage><pages>51-57</pages><issn>0260-8774</issn><eissn>1873-5770</eissn><abstract>The potential of using NMR as a reference method for WHC measurement in porcine longissimus dorsi was investigated. The accuracy of NMR when measuring small water changes was assessed in a model system and in muscles. Visible/near infrared (Vis/NIR) and X-ray were used as potential online spectroscopic methods to assess WHC on 40 muscles. Drip loss and spin–spin relaxation were also measured. Calibration models were built using partial least squares regression (PLSR) with Vis/NIR or X-ray spectra as input and NMR or drip loss values as output. The slowest spin–spin relaxation time (T22) showed higher correlation with both Vis/NIR (RCV2 = 0.66) and X-ray spectra (RCV2 = 0.76) than EZ-DripLoss values, demonstrating NMR has potential as a reference method for WHC measurement. NMR was more robust against variation along the length of the muscle when compared to the EZ-DripLoss method.
•NMR accurately measures water mass.•The slowest spin–spin relaxation time (T22) showed higher correlation with both Vis/NIR and X-ray spectra than drip loss values.•Only NMR was independent on slice number and had the lowest absolute error.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.jfoodeng.2015.12.003</doi><tpages>7</tpages></addata></record> |
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| subjects | EZ-DripLoss Infrared Muscles NMR Nuclear magnetic resonance Online Porcine longissimus dorsi muscles Spectra Spectroscopic analysis Spectroscopy Vis/NIR spectroscopy Water holding capacity X-ray transmission X-rays |
| title | Evaluating nuclear magnetic resonance (NMR) as a robust reference method for online spectroscopic measurement of water holding capacity (WHC) |
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