Synthesis, characterization and photocatalytic properties of rod-shaped titanium dioxide

Rod-shaped titanium dioxide (TiO 2 ) powder was successfully synthesized by simple inexpensive solution growth technique with and without the aid of biosurfactant-palmitic acid. The synthesized TiO 2 powder was characterized using advanced techniques such as X-ray diffraction analysis, Scanning elec...

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Veröffentlicht in:Journal of materials science. Materials in electronics 2016-01, Vol.27 (1), p.458-465
Hauptverfasser: Thamima, M., Karuppuchamy, S.
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Karuppuchamy, S.
description Rod-shaped titanium dioxide (TiO 2 ) powder was successfully synthesized by simple inexpensive solution growth technique with and without the aid of biosurfactant-palmitic acid. The synthesized TiO 2 powder was characterized using advanced techniques such as X-ray diffraction analysis, Scanning electron microscope (SEM) with Energy dispersive analysis, Fourier transform infra red spectroscopy (FT-IR), Photoluminescence and Micro Raman spectral studies. SEM observation of the synthesized TiO 2 powder clearly shows rod-shaped particle formation which was influenced by palmitic acid. The Ti–O–Ti stretching band at 450–800 cm −1 was confirmed by FT-IR studies. The synthesized rod-shaped titanium dioxide strongly decomposes the Alizarin Red S dye under UV light irradiation. The maximum dye decolourization efficiency of 99.4 % was achieved by the addition of rod-shaped TiO 2 powder.
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subjects Characterization and Evaluation of Materials
Chemistry and Materials Science
Diffraction
Dyes
Fourier transforms
Materials Science
Optical and Electronic Materials
Scanning electron microscopy
Spectra
Titanium
Titanium dioxide
title Synthesis, characterization and photocatalytic properties of rod-shaped titanium dioxide
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