Manufacture, electromagnetic properties and microstructure of an 18-filament jelly-roll Nb sub(3)Al superconducting wire with rapid heating and quenching heat-treatment

In this paper, we have reported the manufacture of a novel simple-structured jelly-roll Nb sub(3)Al precursor long wire, and its electromagnetic properties and microstructure with different rapid heating and quenching (RHQ) heat-treatments. By comparing three processing methods, it is found that the...

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Veröffentlicht in:Superconductor science & technology 2016-01, Vol.29 (1), p.1-9
Hauptverfasser: Pan, X F, Feng, Y, Yan, G, Cui, L J, Chen, C, Zhang, Y, Wu, Z X, Liu, X H, Zhang, P X, Bai, Z M, Zhao, Y, Li, L F
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container_end_page 9
container_issue 1
container_start_page 1
container_title Superconductor science & technology
container_volume 29
creator Pan, X F
Feng, Y
Yan, G
Cui, L J
Chen, C
Zhang, Y
Wu, Z X
Liu, X H
Zhang, P X
Bai, Z M
Zhao, Y
Li, L F
description In this paper, we have reported the manufacture of a novel simple-structured jelly-roll Nb sub(3)Al precursor long wire, and its electromagnetic properties and microstructure with different rapid heating and quenching (RHQ) heat-treatments. By comparing three processing methods, it is found that the rolling and drawing (RD) method is more suitable to the fabrication of kilometer-length Nb sub(3)Al precursor wire without annealing. Using homemade RHQ equipment, we have successfully carried out RHQ heat-treatment of Nb sub(3)Al wire samples with various heating conditions. Based on magnetization and magnetoresistivity measurements, the onset superconducting transition temperature, T sub(c) and upper critical field, H sub(c2) (0) of optimal Nb sub(3)Al wire reach 17.9 K-18.0 K and 29.7 T, respectively. Through microstructure and composition analysis, the Nb sub(3)Al superconductor in the optimal wire displays a typical 'layer-to-layer' structure, which comprises alternate crystalline Nb sub(3)Al and amorphous Nb layers, and the Nb sub(3)Al grains sizes are about 100nm-300nm. Furthermore, many small holes are dispersed in the Nb sub(3)Al superconductor due to the diffusion reaction from Al to Nb site. The work suggests the simple-structured Nb sub(3)Al precursor wire with RHQ heat-treatment is very promising for high-field application.
doi_str_mv 10.1088/0953-2048/29/1/015008
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By comparing three processing methods, it is found that the rolling and drawing (RD) method is more suitable to the fabrication of kilometer-length Nb sub(3)Al precursor wire without annealing. Using homemade RHQ equipment, we have successfully carried out RHQ heat-treatment of Nb sub(3)Al wire samples with various heating conditions. Based on magnetization and magnetoresistivity measurements, the onset superconducting transition temperature, T sub(c) and upper critical field, H sub(c2) (0) of optimal Nb sub(3)Al wire reach 17.9 K-18.0 K and 29.7 T, respectively. Through microstructure and composition analysis, the Nb sub(3)Al superconductor in the optimal wire displays a typical 'layer-to-layer' structure, which comprises alternate crystalline Nb sub(3)Al and amorphous Nb layers, and the Nb sub(3)Al grains sizes are about 100nm-300nm. Furthermore, many small holes are dispersed in the Nb sub(3)Al superconductor due to the diffusion reaction from Al to Nb site. The work suggests the simple-structured Nb sub(3)Al precursor wire with RHQ heat-treatment is very promising for high-field application.</abstract><doi>10.1088/0953-2048/29/1/015008</doi></addata></record>
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source IOP Publishing Journals; Institute of Physics (IOP) Journals - HEAL-Link
subjects Electromagnetic properties
Heat treatment
Heating
Intermetallic compounds
Microstructure
Niobium
Precursors
Superconductors
Wire
title Manufacture, electromagnetic properties and microstructure of an 18-filament jelly-roll Nb sub(3)Al superconducting wire with rapid heating and quenching heat-treatment
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