Structure and photoluminescence properties of Er3+-doped TiO2-SiO2 powders prepared by sol-gel method
Er3+-doped TiO2-SiO2 powders are prepared by the sol-gel method, and they are characterized by high resolution transmission electron microscopy (HR-TEM), X-ray diffraction (XRD) spectra, and Raman spectra of the samples. It is shown that the TiO2 nanocrystals are surrounded by an SiO2 glass matrix....
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Veröffentlicht in: | Chinese physics B 2011-08, Vol.20 (8), p.429-434 |
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creator | Zhao Jian-Guo Zhang Wei-Ying Ma Zi-Wei Xie Er-Qing Zhao A-Ke Liu Zhao-Jun |
description | Er3+-doped TiO2-SiO2 powders are prepared by the sol-gel method, and they are characterized by high resolution transmission electron microscopy (HR-TEM), X-ray diffraction (XRD) spectra, and Raman spectra of the samples. It is shown that the TiO2 nanocrystals are surrounded by an SiO2 glass matrix. The photoluminescence (PL) spectra are recorded at room temperature. A strong green luminescence and less intense red emission are observed in the samples when they are excited at 325 nm. The intensity of the emission, which is related to the defect states, is strongest at the annealing temperature of 800℃. The PL intensity of Er3+ ions increases with increasing Ti/Si ratio due to energy transfer between nano-TiO2 particles and Er3+ ions. |
doi_str_mv | 10.1088/1674-1056/20/8/087701 |
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It is shown that the TiO2 nanocrystals are surrounded by an SiO2 glass matrix. The photoluminescence (PL) spectra are recorded at room temperature. A strong green luminescence and less intense red emission are observed in the samples when they are excited at 325 nm. The intensity of the emission, which is related to the defect states, is strongest at the annealing temperature of 800℃. 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It is shown that the TiO2 nanocrystals are surrounded by an SiO2 glass matrix. The photoluminescence (PL) spectra are recorded at room temperature. A strong green luminescence and less intense red emission are observed in the samples when they are excited at 325 nm. The intensity of the emission, which is related to the defect states, is strongest at the annealing temperature of 800℃. The PL intensity of Er3+ ions increases with increasing Ti/Si ratio due to energy transfer between nano-TiO2 particles and Er3+ ions.</description><subject>Annealing</subject><subject>Defect annealing</subject><subject>Emission</subject><subject>Nanomaterials</subject><subject>Nanostructure</subject><subject>Photoluminescence</subject><subject>SiO2</subject><subject>Sol-gel processes</subject><subject>Spectra</subject><subject>TiO2粒子</subject><subject>Titanium dioxide</subject><subject>光致发光特性</subject><subject>凝胶法</subject><subject>溶胶</subject><subject>粉末制备</subject><subject>结构</subject><subject>高分辨透射电子显微镜</subject><issn>1674-1056</issn><issn>2058-3834</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkE1OwzAQhS0EEqVwBCSzYxMy_klsL1FVfqRKXbSso9R20qAkTu1EqGfgStyJK2CpiC2bedK8TzNvBqFbAg8EpExJLnhCIMtTCqlMQQoB5AzNKGQyYZLxczT7Yy7RVQjvADkBymao3ox-0uPkLS57g4e9G107dU1vg7a9tnjwbrB-bGzArsJLz76_PhMTewZvmzVNNrHgwX0Y60OE7VD6aO2OOLg2qW2LOzvunblGF1XZBnvzq3P09rTcLl6S1fr5dfG4SjQRYkxIRqkhVDAllcpBVBwqDVIZDoJa2JWaasO1Ko3MeGY51dFXJct2QuZGMzZH96e5MfdhsmEsuiZe0rZlb90UirhFQp5JTv5HIX5XKaZERO9OqN67vj40fV0MvulKfyyYVJCrjLMfg7R1wg</recordid><startdate>20110801</startdate><enddate>20110801</enddate><creator>Zhao Jian-Guo Zhang Wei-Ying Ma Zi-Wei Xie Er-Qing Zhao A-Ke Liu Zhao-Jun</creator><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>7QQ</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110801</creationdate><title>Structure and photoluminescence properties of Er3+-doped TiO2-SiO2 powders prepared by sol-gel method</title><author>Zhao Jian-Guo Zhang Wei-Ying Ma Zi-Wei Xie Er-Qing Zhao A-Ke Liu Zhao-Jun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c177t-1522d12739899607f40fc089d4072e0bac2cd4c9ad8545e42c0fc9a35b786dc33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Annealing</topic><topic>Defect annealing</topic><topic>Emission</topic><topic>Nanomaterials</topic><topic>Nanostructure</topic><topic>Photoluminescence</topic><topic>SiO2</topic><topic>Sol-gel processes</topic><topic>Spectra</topic><topic>TiO2粒子</topic><topic>Titanium dioxide</topic><topic>光致发光特性</topic><topic>凝胶法</topic><topic>溶胶</topic><topic>粉末制备</topic><topic>结构</topic><topic>高分辨透射电子显微镜</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao Jian-Guo Zhang Wei-Ying Ma Zi-Wei Xie Er-Qing Zhao A-Ke Liu Zhao-Jun</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>Ceramic Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Chinese physics B</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao Jian-Guo Zhang Wei-Ying Ma Zi-Wei Xie Er-Qing Zhao A-Ke Liu Zhao-Jun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structure and photoluminescence properties of Er3+-doped TiO2-SiO2 powders prepared by sol-gel method</atitle><jtitle>Chinese physics B</jtitle><addtitle>Chinese Physics</addtitle><date>2011-08-01</date><risdate>2011</risdate><volume>20</volume><issue>8</issue><spage>429</spage><epage>434</epage><pages>429-434</pages><issn>1674-1056</issn><eissn>2058-3834</eissn><abstract>Er3+-doped TiO2-SiO2 powders are prepared by the sol-gel method, and they are characterized by high resolution transmission electron microscopy (HR-TEM), X-ray diffraction (XRD) spectra, and Raman spectra of the samples. 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subjects | Annealing Defect annealing Emission Nanomaterials Nanostructure Photoluminescence SiO2 Sol-gel processes Spectra TiO2粒子 Titanium dioxide 光致发光特性 凝胶法 溶胶 粉末制备 结构 高分辨透射电子显微镜 |
title | Structure and photoluminescence properties of Er3+-doped TiO2-SiO2 powders prepared by sol-gel method |
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