The effect of calcination temperatures on structural and electrochemical properties of TiO2 film deposited on commercial pure titanium
TiO2 films were deposited on commercial pure titanium (CP-Ti) by sol–gel process, dip coating technique. Coated samples were calcined at various temperatures. The effects of calcination temperature on the structural and electrochemical properties of coated films were investigated. The results showed...
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Veröffentlicht in: | Surface & coatings technology 2016-01, Vol.285, p.298-303 |
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creator | Çomaklı, O. Yazıcı, M. Yetim, T. Yetim, A.F. Çelik, A. |
description | TiO2 films were deposited on commercial pure titanium (CP-Ti) by sol–gel process, dip coating technique. Coated samples were calcined at various temperatures. The effects of calcination temperature on the structural and electrochemical properties of coated films were investigated. The results showed that the anatase peaks were obtained from the samples calcinated at 500°C. When the calcination temperatures increased from 500°C to 700°C, the intensities of the anatase peaks were increased. As the calcination temperature was 900°C, the anatase phase nearly transformed to the rutile phase. Also, thickness of TiO2 films increased with the increasing calcination temperature. Electrochemical behavior of uncoated and coated samples was mainly investigated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) in simulated body fluid (SBF) solution. According to test results, corrosion resistance values of TiO2 film coated samples were higher than the uncoated CP-Ti values. Furthermore, corrosion resistance increased with increasing calcination temperature and the best result was observed from the sample calcinated at 900°C.
•TiO2 films were coated on commercially pure titanium samples by sol-gel dip method.•The influences of calcinations temperature on corrosion performances of TiO2 films were studied.•Corrosion resistance of untreated commercially pure titanium samples improved with TiO2 film coating. |
doi_str_mv | 10.1016/j.surfcoat.2015.11.055 |
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•TiO2 films were coated on commercially pure titanium samples by sol-gel dip method.•The influences of calcinations temperature on corrosion performances of TiO2 films were studied.•Corrosion resistance of untreated commercially pure titanium samples improved with TiO2 film coating.</description><identifier>ISSN: 0257-8972</identifier><identifier>EISSN: 1879-3347</identifier><identifier>DOI: 10.1016/j.surfcoat.2015.11.055</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Anatase ; Calcination ; Coating ; Corrosion resistance ; Deposition ; Electrochemical analysis ; Electrochemical impedance spectroscopy ; Sol–gel ; TiO2 ; Titanium ; Titanium dioxide</subject><ispartof>Surface & coatings technology, 2016-01, Vol.285, p.298-303</ispartof><rights>2015 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c382t-4bac4a76f018957c6a14ff0bf976ec007d0e96f113eb2b761d037f0330a022123</citedby><cites>FETCH-LOGICAL-c382t-4bac4a76f018957c6a14ff0bf976ec007d0e96f113eb2b761d037f0330a022123</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0257897215304291$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids></links><search><creatorcontrib>Çomaklı, O.</creatorcontrib><creatorcontrib>Yazıcı, M.</creatorcontrib><creatorcontrib>Yetim, T.</creatorcontrib><creatorcontrib>Yetim, A.F.</creatorcontrib><creatorcontrib>Çelik, A.</creatorcontrib><title>The effect of calcination temperatures on structural and electrochemical properties of TiO2 film deposited on commercial pure titanium</title><title>Surface & coatings technology</title><description>TiO2 films were deposited on commercial pure titanium (CP-Ti) by sol–gel process, dip coating technique. Coated samples were calcined at various temperatures. The effects of calcination temperature on the structural and electrochemical properties of coated films were investigated. The results showed that the anatase peaks were obtained from the samples calcinated at 500°C. When the calcination temperatures increased from 500°C to 700°C, the intensities of the anatase peaks were increased. As the calcination temperature was 900°C, the anatase phase nearly transformed to the rutile phase. Also, thickness of TiO2 films increased with the increasing calcination temperature. Electrochemical behavior of uncoated and coated samples was mainly investigated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) in simulated body fluid (SBF) solution. According to test results, corrosion resistance values of TiO2 film coated samples were higher than the uncoated CP-Ti values. Furthermore, corrosion resistance increased with increasing calcination temperature and the best result was observed from the sample calcinated at 900°C.
•TiO2 films were coated on commercially pure titanium samples by sol-gel dip method.•The influences of calcinations temperature on corrosion performances of TiO2 films were studied.•Corrosion resistance of untreated commercially pure titanium samples improved with TiO2 film coating.</description><subject>Anatase</subject><subject>Calcination</subject><subject>Coating</subject><subject>Corrosion resistance</subject><subject>Deposition</subject><subject>Electrochemical analysis</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Sol–gel</subject><subject>TiO2</subject><subject>Titanium</subject><subject>Titanium dioxide</subject><issn>0257-8972</issn><issn>1879-3347</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFkMFq3DAQhkVIIJukr1B07MXujGRb9i0lpG0gkMvmLLTyiGixrY0kF_oCee7KbHvuaRj4_p-Zj7HPCDUCdl-PdVqjs8HkWgC2NWINbXvBdtiroZKyUZdsB6JVVT8occ1uUjoCAKqh2bGP_Rtxco5s5sFxaybrF5N9WHim-UTR5DVS4mVPOa62bGbiZhk5TSUTg32j2ZcYP8VQ8Ow32PG9fxHc-WnmI51C8pnGrcOGeaZo_caXXp59Notf5zt25cyU6NPfectevz_uH35Wzy8_nh6-PVdW9iJXzcHYxqjOAfZDq2xnsHEODm5QHVkANQINnUOUdBAH1eEIUjmQEgwIgULesi_n3nLt-0op69knS9NkFgpr0qhUDwJkjwXtzqiNIaVITp-in038rRH0Jl4f9T_xehOvEXURX4L35yCVR355ijpZT4ul0ceiTI_B_6_iDwB4kto</recordid><startdate>20160115</startdate><enddate>20160115</enddate><creator>Çomaklı, O.</creator><creator>Yazıcı, M.</creator><creator>Yetim, T.</creator><creator>Yetim, A.F.</creator><creator>Çelik, A.</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SE</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20160115</creationdate><title>The effect of calcination temperatures on structural and electrochemical properties of TiO2 film deposited on commercial pure titanium</title><author>Çomaklı, O. ; Yazıcı, M. ; Yetim, T. ; Yetim, A.F. ; Çelik, A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c382t-4bac4a76f018957c6a14ff0bf976ec007d0e96f113eb2b761d037f0330a022123</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Anatase</topic><topic>Calcination</topic><topic>Coating</topic><topic>Corrosion resistance</topic><topic>Deposition</topic><topic>Electrochemical analysis</topic><topic>Electrochemical impedance spectroscopy</topic><topic>Sol–gel</topic><topic>TiO2</topic><topic>Titanium</topic><topic>Titanium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Çomaklı, O.</creatorcontrib><creatorcontrib>Yazıcı, M.</creatorcontrib><creatorcontrib>Yetim, T.</creatorcontrib><creatorcontrib>Yetim, A.F.</creatorcontrib><creatorcontrib>Çelik, A.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Surface & coatings technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Çomaklı, O.</au><au>Yazıcı, M.</au><au>Yetim, T.</au><au>Yetim, A.F.</au><au>Çelik, A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The effect of calcination temperatures on structural and electrochemical properties of TiO2 film deposited on commercial pure titanium</atitle><jtitle>Surface & coatings technology</jtitle><date>2016-01-15</date><risdate>2016</risdate><volume>285</volume><spage>298</spage><epage>303</epage><pages>298-303</pages><issn>0257-8972</issn><eissn>1879-3347</eissn><abstract>TiO2 films were deposited on commercial pure titanium (CP-Ti) by sol–gel process, dip coating technique. Coated samples were calcined at various temperatures. The effects of calcination temperature on the structural and electrochemical properties of coated films were investigated. The results showed that the anatase peaks were obtained from the samples calcinated at 500°C. When the calcination temperatures increased from 500°C to 700°C, the intensities of the anatase peaks were increased. As the calcination temperature was 900°C, the anatase phase nearly transformed to the rutile phase. Also, thickness of TiO2 films increased with the increasing calcination temperature. Electrochemical behavior of uncoated and coated samples was mainly investigated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) in simulated body fluid (SBF) solution. According to test results, corrosion resistance values of TiO2 film coated samples were higher than the uncoated CP-Ti values. Furthermore, corrosion resistance increased with increasing calcination temperature and the best result was observed from the sample calcinated at 900°C.
•TiO2 films were coated on commercially pure titanium samples by sol-gel dip method.•The influences of calcinations temperature on corrosion performances of TiO2 films were studied.•Corrosion resistance of untreated commercially pure titanium samples improved with TiO2 film coating.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.surfcoat.2015.11.055</doi><tpages>6</tpages></addata></record> |
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subjects | Anatase Calcination Coating Corrosion resistance Deposition Electrochemical analysis Electrochemical impedance spectroscopy Sol–gel TiO2 Titanium Titanium dioxide |
title | The effect of calcination temperatures on structural and electrochemical properties of TiO2 film deposited on commercial pure titanium |
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