A Comparison Study on Corrosion Resistance of 430 Stainless Steel Surfaces Modified by Alkylsilane and Fluoroalkylsilane SAMs
The self-assembly monolayers （SAMs） of n-dodecyltriethoxysilane （DTES） and 1 H, 1 H, 2H, 2H-perflu- orodecyltriethoxysilane （PFDS） on the surface of the 430 stainless steel （430SS） were prepared and their corrosion protection performance was investigated by potentiodynamic polarization, Fourier tran...
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| Veröffentlicht in: | Journal of iron and steel research, international international, 2013-12, Vol.20 (12), p.75-81 |
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| creator | WANG, Hai-ren XIAO, Zhen QU, Jun-e YANG, Hong-wei CAO, Zhi-yong GUO, Xing-peng |
| description | The self-assembly monolayers （SAMs） of n-dodecyltriethoxysilane （DTES） and 1 H, 1 H, 2H, 2H-perflu- orodecyltriethoxysilane （PFDS） on the surface of the 430 stainless steel （430SS） were prepared and their corrosion protection performance was investigated by potentiodynamic polarization, Fourier transform infrared spectroscopy （FTIR） -attenuated total reflection （ATR）, static contact angle and atomic force microscopy （AFM）. The results showed that the alkali pretreatment and the water added into the self-assembly solution could generate more hydrox- yls on the 430SS surface, and then enhanced the adsorption of the SAMs. A suitable temperature of the self-assem- bly solution is important for the formation of the SAMs. The silane SAMs were chemically adsorbed on the 430SS substrates by Fe-O-Si bonds. In all cases tested, PFDS has a better inhibition effect compared with DTES, and the difference in inhibition effect is most marked at the lowest concentration of 1 mmol/L. |
| doi_str_mv | 10.1016/S1006-706X(13)60219-8 |
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The results showed that the alkali pretreatment and the water added into the self-assembly solution could generate more hydrox- yls on the 430SS surface, and then enhanced the adsorption of the SAMs. A suitable temperature of the self-assem- bly solution is important for the formation of the SAMs. The silane SAMs were chemically adsorbed on the 430SS substrates by Fe-O-Si bonds. In all cases tested, PFDS has a better inhibition effect compared with DTES, and the difference in inhibition effect is most marked at the lowest concentration of 1 mmol/L.</description><identifier>ISSN: 1006-706X</identifier><identifier>EISSN: 2210-3988</identifier><identifier>DOI: 10.1016/S1006-706X(13)60219-8</identifier><language>eng</language><publisher>Singapore: Elsevier Ltd</publisher><subject>430 stainless steel (430SS) ; Applied and Technical Physics ; corrosion protection ; Engineering ; Ferritic stainless steels ; Fourier transforms ; Infrared spectroscopy ; Inhibition ; Iron and steel industry ; Machines ; Manufacturing ; Materials Engineering ; Materials Science ; Metallic Materials ; Physical Chemistry ; Processes ; Self assembly ; self-assembly monolayer (SAM) ; silane ; Stainless steels ; Steels ; Surface chemistry ; 不锈钢表面 ; 傅立叶变换红外光谱 ; 十二烷基 ; 改性 ; 氟硅烷 ; 耐腐蚀性能 ; 腐蚀保护性能 ; 自组装单层</subject><ispartof>Journal of iron and steel research, international, 2013-12, Vol.20 (12), p.75-81</ispartof><rights>2013 Central Iron and Steel Research Institute</rights><rights>China Iron and Steel Research Institute Group 2013</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c514t-8c6e992809e2bde93741732da8fb520565f6adffbad1e02a713011a49d472ace3</citedby><cites>FETCH-LOGICAL-c514t-8c6e992809e2bde93741732da8fb520565f6adffbad1e02a713011a49d472ace3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/86787X/86787X.jpg</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1016/S1006-706X(13)60219-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://dx.doi.org/10.1016/S1006-706X(13)60219-8$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,41488,42557,45995,51319</link.rule.ids></links><search><creatorcontrib>WANG, Hai-ren</creatorcontrib><creatorcontrib>XIAO, Zhen</creatorcontrib><creatorcontrib>QU, Jun-e</creatorcontrib><creatorcontrib>YANG, Hong-wei</creatorcontrib><creatorcontrib>CAO, Zhi-yong</creatorcontrib><creatorcontrib>GUO, Xing-peng</creatorcontrib><title>A Comparison Study on Corrosion Resistance of 430 Stainless Steel Surfaces Modified by Alkylsilane and Fluoroalkylsilane SAMs</title><title>Journal of iron and steel research, international</title><addtitle>J. Iron Steel Res. Int</addtitle><addtitle>Journal of Iron and Steel Research</addtitle><description>The self-assembly monolayers （SAMs） of n-dodecyltriethoxysilane （DTES） and 1 H, 1 H, 2H, 2H-perflu- orodecyltriethoxysilane （PFDS） on the surface of the 430 stainless steel （430SS） were prepared and their corrosion protection performance was investigated by potentiodynamic polarization, Fourier transform infrared spectroscopy （FTIR） -attenuated total reflection （ATR）, static contact angle and atomic force microscopy （AFM）. The results showed that the alkali pretreatment and the water added into the self-assembly solution could generate more hydrox- yls on the 430SS surface, and then enhanced the adsorption of the SAMs. A suitable temperature of the self-assem- bly solution is important for the formation of the SAMs. The silane SAMs were chemically adsorbed on the 430SS substrates by Fe-O-Si bonds. In all cases tested, PFDS has a better inhibition effect compared with DTES, and the difference in inhibition effect is most marked at the lowest concentration of 1 mmol/L.</description><subject>430 stainless steel (430SS)</subject><subject>Applied and Technical Physics</subject><subject>corrosion protection</subject><subject>Engineering</subject><subject>Ferritic stainless steels</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Inhibition</subject><subject>Iron and steel industry</subject><subject>Machines</subject><subject>Manufacturing</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Physical Chemistry</subject><subject>Processes</subject><subject>Self assembly</subject><subject>self-assembly monolayer (SAM)</subject><subject>silane</subject><subject>Stainless steels</subject><subject>Steels</subject><subject>Surface chemistry</subject><subject>不锈钢表面</subject><subject>傅立叶变换红外光谱</subject><subject>十二烷基</subject><subject>改性</subject><subject>氟硅烷</subject><subject>耐腐蚀性能</subject><subject>腐蚀保护性能</subject><subject>自组装单层</subject><issn>1006-706X</issn><issn>2210-3988</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqNkVFrFDEUhYMouNT-BCG-1YfR3CSTSZ5kWawKLYKr4FvITm5q6uxkm8wU9sH_brZbim9rXnIJ3zn3kEPIa2DvgIF6vwbGVNMx9fMCxFvFOJhGPyMLzoE1wmj9nCyekJfkvJRbdjhGCa4X5M-SrtJ253IsaaTrafZ7WodVyjmVWKdvWGKZ3NgjTYFKwSrk4jhgKXVCHOh6zsH1WOh18jFE9HSzp8vh934ocXAjUjd6ejnMKSf3z-t6eV1ekRfBDQXPH-8z8uPy4_fV5-bq66cvq-VV07cgp0b3Co3hmhnkG49GdBI6wb3TYdNy1qo2KOdD2DgPyLjrQDAAJ42XHa_RxBm5OPrucrqbsUx2G0uPwyFImouFTnGontX1JKo6Xc01wGm0lSCF4kz8BwpCaiNFW9H2iPa1gZIx2F2OW5f3Fpg9VG4fKreHPi0I-1C51VWnjrpS-fEGs71Ncx7rt54UfjgKsTZwH6uw9BFr4T5m7CfrUzzp8OYx8q803tzV7U-ZpQEjoRXiL8U8zig</recordid><startdate>20131201</startdate><enddate>20131201</enddate><creator>WANG, Hai-ren</creator><creator>XIAO, Zhen</creator><creator>QU, Jun-e</creator><creator>YANG, Hong-wei</creator><creator>CAO, Zhi-yong</creator><creator>GUO, Xing-peng</creator><general>Elsevier Ltd</general><general>Springer Singapore</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>W92</scope><scope>~WA</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SE</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20131201</creationdate><title>A Comparison Study on Corrosion Resistance of 430 Stainless Steel Surfaces Modified by Alkylsilane and Fluoroalkylsilane SAMs</title><author>WANG, Hai-ren ; XIAO, Zhen ; QU, Jun-e ; YANG, Hong-wei ; CAO, Zhi-yong ; GUO, Xing-peng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c514t-8c6e992809e2bde93741732da8fb520565f6adffbad1e02a713011a49d472ace3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>430 stainless steel (430SS)</topic><topic>Applied and Technical Physics</topic><topic>corrosion protection</topic><topic>Engineering</topic><topic>Ferritic stainless steels</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Inhibition</topic><topic>Iron and steel industry</topic><topic>Machines</topic><topic>Manufacturing</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Physical Chemistry</topic><topic>Processes</topic><topic>Self assembly</topic><topic>self-assembly monolayer (SAM)</topic><topic>silane</topic><topic>Stainless steels</topic><topic>Steels</topic><topic>Surface chemistry</topic><topic>不锈钢表面</topic><topic>傅立叶变换红外光谱</topic><topic>十二烷基</topic><topic>改性</topic><topic>氟硅烷</topic><topic>耐腐蚀性能</topic><topic>腐蚀保护性能</topic><topic>自组装单层</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>WANG, Hai-ren</creatorcontrib><creatorcontrib>XIAO, Zhen</creatorcontrib><creatorcontrib>QU, Jun-e</creatorcontrib><creatorcontrib>YANG, Hong-wei</creatorcontrib><creatorcontrib>CAO, Zhi-yong</creatorcontrib><creatorcontrib>GUO, Xing-peng</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库-工程技术</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>CrossRef</collection><collection>Corrosion Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of iron and steel research, international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>WANG, Hai-ren</au><au>XIAO, Zhen</au><au>QU, Jun-e</au><au>YANG, Hong-wei</au><au>CAO, Zhi-yong</au><au>GUO, Xing-peng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A Comparison Study on Corrosion Resistance of 430 Stainless Steel Surfaces Modified by Alkylsilane and Fluoroalkylsilane SAMs</atitle><jtitle>Journal of iron and steel research, international</jtitle><stitle>J. Iron Steel Res. Int</stitle><addtitle>Journal of Iron and Steel Research</addtitle><date>2013-12-01</date><risdate>2013</risdate><volume>20</volume><issue>12</issue><spage>75</spage><epage>81</epage><pages>75-81</pages><issn>1006-706X</issn><eissn>2210-3988</eissn><abstract>The self-assembly monolayers （SAMs） of n-dodecyltriethoxysilane （DTES） and 1 H, 1 H, 2H, 2H-perflu- orodecyltriethoxysilane （PFDS） on the surface of the 430 stainless steel （430SS） were prepared and their corrosion protection performance was investigated by potentiodynamic polarization, Fourier transform infrared spectroscopy （FTIR） -attenuated total reflection （ATR）, static contact angle and atomic force microscopy （AFM）. The results showed that the alkali pretreatment and the water added into the self-assembly solution could generate more hydrox- yls on the 430SS surface, and then enhanced the adsorption of the SAMs. A suitable temperature of the self-assem- bly solution is important for the formation of the SAMs. The silane SAMs were chemically adsorbed on the 430SS substrates by Fe-O-Si bonds. In all cases tested, PFDS has a better inhibition effect compared with DTES, and the difference in inhibition effect is most marked at the lowest concentration of 1 mmol/L.</abstract><cop>Singapore</cop><pub>Elsevier Ltd</pub><doi>10.1016/S1006-706X(13)60219-8</doi><tpages>7</tpages></addata></record> |
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| subjects | 430 stainless steel (430SS) Applied and Technical Physics corrosion protection Engineering Ferritic stainless steels Fourier transforms Infrared spectroscopy Inhibition Iron and steel industry Machines Manufacturing Materials Engineering Materials Science Metallic Materials Physical Chemistry Processes Self assembly self-assembly monolayer (SAM) silane Stainless steels Steels Surface chemistry 不锈钢表面 傅立叶变换红外光谱 十二烷基 改性 氟硅烷 耐腐蚀性能 腐蚀保护性能 自组装单层 |
| title | A Comparison Study on Corrosion Resistance of 430 Stainless Steel Surfaces Modified by Alkylsilane and Fluoroalkylsilane SAMs |
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