Synthesis and physicochemical study of hexaamminechromium(III) hexamolybdogallate
Hexaamminechromium(III) hexamolybdogallate of composition [Cr(NH 3 ) 6 ][GaMo 6 O 18 (OH) 6 ] · 5H 2 O ( I ) was synthesized and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals I are monoclinic: a = 11.77 Å, b = 10.97 Å, c = 15.49 Å, β = 115.11°, V =...
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| Veröffentlicht in: | Russian journal of inorganic chemistry 2011-11, Vol.56 (11), p.1698-1701 |
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| container_title | Russian journal of inorganic chemistry |
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| creator | Oreshkina, A. V. Kaziev, G. Z. Lobanov, N. N. Shipilova, P. A. |
| description | Hexaamminechromium(III) hexamolybdogallate of composition [Cr(NH
3
)
6
][GaMo
6
O
18
(OH)
6
] · 5H
2
O (
I
) was synthesized and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals
I
are monoclinic:
a
= 11.77 Å,
b
= 10.97 Å,
c
= 15.49 Å, β = 115.11°,
V
= 1811.29 Å
3
, ρ
calc
= 1.17 g/cm
3
,
Z
= 1. The compound obtained was used as a catalyst for soft oxidation of natural gas at 633 K. |
| doi_str_mv | 10.1134/S0036023611110180 |
| format | Article |
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3
)
6
][GaMo
6
O
18
(OH)
6
] · 5H
2
O (
I
) was synthesized and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals
I
are monoclinic:
a
= 11.77 Å,
b
= 10.97 Å,
c
= 15.49 Å, β = 115.11°,
V
= 1811.29 Å
3
, ρ
calc
= 1.17 g/cm
3
,
Z
= 1. The compound obtained was used as a catalyst for soft oxidation of natural gas at 633 K.</description><identifier>ISSN: 0036-0236</identifier><identifier>EISSN: 1531-8613</identifier><identifier>DOI: 10.1134/S0036023611110180</identifier><language>eng</language><publisher>Dordrecht: SP MAIK Nauka/Interperiodica</publisher><subject>Chemistry ; Chemistry and Materials Science ; Crystals ; Diffraction ; Infrared radiation ; Inorganic Chemistry ; Mass spectrometry ; Natural gas ; Synthesis ; Synthesis and Properties of Inorganic Compounds ; Thermogravimetry ; X-rays</subject><ispartof>Russian journal of inorganic chemistry, 2011-11, Vol.56 (11), p.1698-1701</ispartof><rights>Pleiades Publishing, Ltd. 2011</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c306t-278777877a8fa97ec21de968774f183c0174cec724edbef775fddc2c30fc0dd93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036023611110180$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036023611110180$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Oreshkina, A. V.</creatorcontrib><creatorcontrib>Kaziev, G. Z.</creatorcontrib><creatorcontrib>Lobanov, N. N.</creatorcontrib><creatorcontrib>Shipilova, P. A.</creatorcontrib><title>Synthesis and physicochemical study of hexaamminechromium(III) hexamolybdogallate</title><title>Russian journal of inorganic chemistry</title><addtitle>Russ. J. Inorg. Chem</addtitle><description>Hexaamminechromium(III) hexamolybdogallate of composition [Cr(NH
3
)
6
][GaMo
6
O
18
(OH)
6
] · 5H
2
O (
I
) was synthesized and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals
I
are monoclinic:
a
= 11.77 Å,
b
= 10.97 Å,
c
= 15.49 Å, β = 115.11°,
V
= 1811.29 Å
3
, ρ
calc
= 1.17 g/cm
3
,
Z
= 1. The compound obtained was used as a catalyst for soft oxidation of natural gas at 633 K.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crystals</subject><subject>Diffraction</subject><subject>Infrared radiation</subject><subject>Inorganic Chemistry</subject><subject>Mass spectrometry</subject><subject>Natural gas</subject><subject>Synthesis</subject><subject>Synthesis and Properties of Inorganic Compounds</subject><subject>Thermogravimetry</subject><subject>X-rays</subject><issn>0036-0236</issn><issn>1531-8613</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFUN1LwzAQD6LgnP4BvvVxPlRzSdd0jzL8GAxEps8lSy5rR9PMpAX735s63wQ9OA5-X9wdIddAbwF4drehlOeU8RxiUSjoCZnAnENa5MBPyWSk05E_Jxch7CnNMiqKCXndDG1XYahDIludHKoh1MqpCm2tZJOErtdD4kxS4aeU1tYtqso7W_d2tlqtbr5x65phq91ONo3s8JKcGdkEvPqZU_L--PC2fE7XL0-r5f06VZzmXcpEIcTYsjByIVAx0LjII5AZKLiiIDKFSrAM9RaNEHOjtWLRbBTVesGnZHbMPXj30WPoSlsHhXGHFl0fShA5Aw4x8n8pYwDZHHIRpXCUKu9C8GjKg6-t9EMJtBw_Xf76dPSwoydEbbtDX-5d79t4_B-mL7fvgCU</recordid><startdate>20111101</startdate><enddate>20111101</enddate><creator>Oreshkina, A. V.</creator><creator>Kaziev, G. Z.</creator><creator>Lobanov, N. N.</creator><creator>Shipilova, P. A.</creator><general>SP MAIK Nauka/Interperiodica</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20111101</creationdate><title>Synthesis and physicochemical study of hexaamminechromium(III) hexamolybdogallate</title><author>Oreshkina, A. V. ; Kaziev, G. Z. ; Lobanov, N. N. ; Shipilova, P. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c306t-278777877a8fa97ec21de968774f183c0174cec724edbef775fddc2c30fc0dd93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crystals</topic><topic>Diffraction</topic><topic>Infrared radiation</topic><topic>Inorganic Chemistry</topic><topic>Mass spectrometry</topic><topic>Natural gas</topic><topic>Synthesis</topic><topic>Synthesis and Properties of Inorganic Compounds</topic><topic>Thermogravimetry</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Oreshkina, A. V.</creatorcontrib><creatorcontrib>Kaziev, G. Z.</creatorcontrib><creatorcontrib>Lobanov, N. N.</creatorcontrib><creatorcontrib>Shipilova, P. A.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Russian journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Oreshkina, A. V.</au><au>Kaziev, G. Z.</au><au>Lobanov, N. N.</au><au>Shipilova, P. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and physicochemical study of hexaamminechromium(III) hexamolybdogallate</atitle><jtitle>Russian journal of inorganic chemistry</jtitle><stitle>Russ. J. Inorg. Chem</stitle><date>2011-11-01</date><risdate>2011</risdate><volume>56</volume><issue>11</issue><spage>1698</spage><epage>1701</epage><pages>1698-1701</pages><issn>0036-0236</issn><eissn>1531-8613</eissn><abstract>Hexaamminechromium(III) hexamolybdogallate of composition [Cr(NH
3
)
6
][GaMo
6
O
18
(OH)
6
] · 5H
2
O (
I
) was synthesized and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals
I
are monoclinic:
a
= 11.77 Å,
b
= 10.97 Å,
c
= 15.49 Å, β = 115.11°,
V
= 1811.29 Å
3
, ρ
calc
= 1.17 g/cm
3
,
Z
= 1. The compound obtained was used as a catalyst for soft oxidation of natural gas at 633 K.</abstract><cop>Dordrecht</cop><pub>SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S0036023611110180</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0036-0236 |
| ispartof | Russian journal of inorganic chemistry, 2011-11, Vol.56 (11), p.1698-1701 |
| issn | 0036-0236 1531-8613 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1762131968 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Chemistry Chemistry and Materials Science Crystals Diffraction Infrared radiation Inorganic Chemistry Mass spectrometry Natural gas Synthesis Synthesis and Properties of Inorganic Compounds Thermogravimetry X-rays |
| title | Synthesis and physicochemical study of hexaamminechromium(III) hexamolybdogallate |
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