Preparation and study of hydrogen hexamolybdometallates(III) with the hexamminecadmium cation
Hydrogen hexamolybdogallate and hexamolybdoaluminate with the hexamminecadmium cation [Cd(NH₃)₆] · H[GaMo₆O₁₈(OH)₆] · 6H₂O (I) and [Cd(NH₃)₆] · H[AlMo₆O₁₈(OH)₆] · 6H₂O (II) were synthesized and studied by mass spectrometry, thermogravimetric analysis, powder X-ray diffraction, and IR spectroscopy. T...
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| Veröffentlicht in: | Russian journal of inorganic chemistry 2010, Vol.55 (12), p.1863-1866 |
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| container_title | Russian journal of inorganic chemistry |
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| creator | Oreshkina, A. V Kaziev, G. Z Steblevskii, A. V |
| description | Hydrogen hexamolybdogallate and hexamolybdoaluminate with the hexamminecadmium cation [Cd(NH₃)₆] · H[GaMo₆O₁₈(OH)₆] · 6H₂O (I) and [Cd(NH₃)₆] · H[AlMo₆O₁₈(OH)₆] · 6H₂O (II) were synthesized and studied by mass spectrometry, thermogravimetric analysis, powder X-ray diffraction, and IR spectroscopy. The crystals are monoclinic; I: a = 10.82 Å, b = 3.69 Å, c = 11.99 Å, β = 91.06°, V= 469.72 ų, ρcalcd = 2.34 g/cm³, Z = 2; II: a = 10.81 Å, b = 3.67 Å, c =11.98 Å, β = 91.08°, V = 469.78 ų, ρcalcd = 2.38 g/cm³, Z = 2. |
| doi_str_mv | 10.1134/S0036023610120089 |
| format | Article |
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The crystals are monoclinic; I: a = 10.82 Å, b = 3.69 Å, c = 11.99 Å, β = 91.06°, V= 469.72 ų, ρcalcd = 2.34 g/cm³, Z = 2; II: a = 10.81 Å, b = 3.67 Å, c =11.98 Å, β = 91.08°, V = 469.78 ų, ρcalcd = 2.38 g/cm³, Z = 2.</description><identifier>ISSN: 0036-0236</identifier><identifier>EISSN: 1531-8613</identifier><identifier>DOI: 10.1134/S0036023610120089</identifier><language>eng</language><publisher>Dordrecht: Dordrecht : SP MAIK Nauka/Interperiodica</publisher><subject>Cations ; Chemistry ; Chemistry and Materials Science ; Crystals ; Diffraction ; Infrared radiation ; Inorganic Chemistry ; Mass spectrometry ; Spectroscopy ; Synthesis and Properties of Inorganic Compounds ; Thermogravimetric analysis ; X-rays</subject><ispartof>Russian journal of inorganic chemistry, 2010, Vol.55 (12), p.1863-1866</ispartof><rights>Pleiades Publishing, Ltd. 2010</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c330t-a520884a7e38b56b56db51d58611d56232738b02a382a8d8cfc2ca50e6c461033</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036023610120089$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036023610120089$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Oreshkina, A. 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The crystals are monoclinic; I: a = 10.82 Å, b = 3.69 Å, c = 11.99 Å, β = 91.06°, V= 469.72 ų, ρcalcd = 2.34 g/cm³, Z = 2; II: a = 10.81 Å, b = 3.67 Å, c =11.98 Å, β = 91.08°, V = 469.78 ų, ρcalcd = 2.38 g/cm³, Z = 2.</description><subject>Cations</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crystals</subject><subject>Diffraction</subject><subject>Infrared radiation</subject><subject>Inorganic Chemistry</subject><subject>Mass spectrometry</subject><subject>Spectroscopy</subject><subject>Synthesis and Properties of Inorganic Compounds</subject><subject>Thermogravimetric analysis</subject><subject>X-rays</subject><issn>0036-0236</issn><issn>1531-8613</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNqFkF1LwzAUhoMoOKc_wCt7OS-qJ0mbZpcy_CgMFOYuJWRpuna0zUxStP_ezHonKBzOuXif93whdInhBmOa3K4AKANCGQZMAPj8CE1wSnHMGabHaHKQ44N-is6c2wEkCWR8gt5erN5LK31tukh2ReR8XwyRKaNqKKzZ6i6q9KdsTTNsCtNqL5tGeu1meZ5fRx-1ryJf6ZFp604rWbR130bqu-M5Oill4_TFT52i9cP96-IpXj4_5ou7ZawoBR_LlADnicw05ZuUhSg2KS7SsHvIjFCSBQGIpJxIXnBVKqJkCpqpJBxM6RTNxr57a9577bxoa6d0WLXTpncCZ4xgkmQ8-x8lBIe5PGMBxSOqrHHO6lLsbd1KOwgM4vB18evrwUNGjwtst9VW7Exvu3D8n6ar0VRKI-TW1k6sVwQwBTwPBHD6BbCUjCg</recordid><startdate>2010</startdate><enddate>2010</enddate><creator>Oreshkina, A. 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V</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c330t-a520884a7e38b56b56db51d58611d56232738b02a382a8d8cfc2ca50e6c461033</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Cations</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crystals</topic><topic>Diffraction</topic><topic>Infrared radiation</topic><topic>Inorganic Chemistry</topic><topic>Mass spectrometry</topic><topic>Spectroscopy</topic><topic>Synthesis and Properties of Inorganic Compounds</topic><topic>Thermogravimetric analysis</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Oreshkina, A. V</creatorcontrib><creatorcontrib>Kaziev, G. Z</creatorcontrib><creatorcontrib>Steblevskii, A. V</creatorcontrib><collection>AGRIS</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Russian journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Oreshkina, A. V</au><au>Kaziev, G. Z</au><au>Steblevskii, A. V</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and study of hydrogen hexamolybdometallates(III) with the hexamminecadmium cation</atitle><jtitle>Russian journal of inorganic chemistry</jtitle><stitle>Russ. J. Inorg. Chem</stitle><date>2010</date><risdate>2010</risdate><volume>55</volume><issue>12</issue><spage>1863</spage><epage>1866</epage><pages>1863-1866</pages><issn>0036-0236</issn><eissn>1531-8613</eissn><abstract>Hydrogen hexamolybdogallate and hexamolybdoaluminate with the hexamminecadmium cation [Cd(NH₃)₆] · H[GaMo₆O₁₈(OH)₆] · 6H₂O (I) and [Cd(NH₃)₆] · H[AlMo₆O₁₈(OH)₆] · 6H₂O (II) were synthesized and studied by mass spectrometry, thermogravimetric analysis, powder X-ray diffraction, and IR spectroscopy. The crystals are monoclinic; I: a = 10.82 Å, b = 3.69 Å, c = 11.99 Å, β = 91.06°, V= 469.72 ų, ρcalcd = 2.34 g/cm³, Z = 2; II: a = 10.81 Å, b = 3.67 Å, c =11.98 Å, β = 91.08°, V = 469.78 ų, ρcalcd = 2.38 g/cm³, Z = 2.</abstract><cop>Dordrecht</cop><pub>Dordrecht : SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S0036023610120089</doi><tpages>4</tpages></addata></record> |
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| subjects | Cations Chemistry Chemistry and Materials Science Crystals Diffraction Infrared radiation Inorganic Chemistry Mass spectrometry Spectroscopy Synthesis and Properties of Inorganic Compounds Thermogravimetric analysis X-rays |
| title | Preparation and study of hydrogen hexamolybdometallates(III) with the hexamminecadmium cation |
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