Synthesis and X-ray diffraction study of complex oxides of the Zn2 − x(ZraSnb)1 − xFe2xO4 composition
A multicomponent system of complex refractory oxides of the composition Zn 2 − x (Zr a Sn b ) 1 − x Fe 2 x O 4 ( a + b = 1; a : b = 1: 5, 1: 4, 1: 3, 1: 2, 1: 1, 2: 1, 3: 1, 4: 1; x = 0−1.0; Δ x = 0.05) was studied by X-ray diffraction. The samples were prepared from oxides of appropriate metals by...
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| Veröffentlicht in: | Russian journal of inorganic chemistry 2012-02, Vol.57 (2), p.146-151 |
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| creator | Grigoryan, R. A. Grigoryan, L. A. |
| description | A multicomponent system of complex refractory oxides of the composition Zn
2 −
x
(Zr
a
Sn
b
)
1 −
x
Fe
2
x
O
4
(
a + b
= 1;
a
:
b
= 1: 5, 1: 4, 1: 3, 1: 2, 1: 1, 2: 1, 3: 1, 4: 1;
x
= 0−1.0; Δ
x
= 0.05) was studied by X-ray diffraction. The samples were prepared from oxides of appropriate metals by low-temperature plasma synthesis (hydrogen-oxygen flame). Two phases with wide homogeneity ranges were identified: α phase crystallized in the crystal system of inverse cubic spinel and β phase with the structure of tetragonal spinel. The phase boundaries were found. Structural data are presented for about 100 solid solutions. |
| doi_str_mv | 10.1134/S0036023612020106 |
| format | Article |
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2 −
x
(Zr
a
Sn
b
)
1 −
x
Fe
2
x
O
4
(
a + b
= 1;
a
:
b
= 1: 5, 1: 4, 1: 3, 1: 2, 1: 1, 2: 1, 3: 1, 4: 1;
x
= 0−1.0; Δ
x
= 0.05) was studied by X-ray diffraction. The samples were prepared from oxides of appropriate metals by low-temperature plasma synthesis (hydrogen-oxygen flame). Two phases with wide homogeneity ranges were identified: α phase crystallized in the crystal system of inverse cubic spinel and β phase with the structure of tetragonal spinel. The phase boundaries were found. Structural data are presented for about 100 solid solutions.</description><identifier>ISSN: 0036-0236</identifier><identifier>EISSN: 1531-8613</identifier><identifier>DOI: 10.1134/S0036023612020106</identifier><language>eng</language><publisher>Dordrecht: SP MAIK Nauka/Interperiodica</publisher><subject>Chemistry ; Chemistry and Materials Science ; Diffraction ; Homogeneity ; Inorganic Chemistry ; Oxides ; Phase boundaries ; Solid solutions ; Spinel ; Synthesis ; Synthesis and Properties of Inorganic Compounds ; X-rays</subject><ispartof>Russian journal of inorganic chemistry, 2012-02, Vol.57 (2), p.146-151</ispartof><rights>Pleiades Publishing, Ltd. 2012</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036023612020106$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036023612020106$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Grigoryan, R. A.</creatorcontrib><creatorcontrib>Grigoryan, L. A.</creatorcontrib><title>Synthesis and X-ray diffraction study of complex oxides of the Zn2 − x(ZraSnb)1 − xFe2xO4 composition</title><title>Russian journal of inorganic chemistry</title><addtitle>Russ. J. Inorg. Chem</addtitle><description>A multicomponent system of complex refractory oxides of the composition Zn
2 −
x
(Zr
a
Sn
b
)
1 −
x
Fe
2
x
O
4
(
a + b
= 1;
a
:
b
= 1: 5, 1: 4, 1: 3, 1: 2, 1: 1, 2: 1, 3: 1, 4: 1;
x
= 0−1.0; Δ
x
= 0.05) was studied by X-ray diffraction. The samples were prepared from oxides of appropriate metals by low-temperature plasma synthesis (hydrogen-oxygen flame). Two phases with wide homogeneity ranges were identified: α phase crystallized in the crystal system of inverse cubic spinel and β phase with the structure of tetragonal spinel. The phase boundaries were found. Structural data are presented for about 100 solid solutions.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Diffraction</subject><subject>Homogeneity</subject><subject>Inorganic Chemistry</subject><subject>Oxides</subject><subject>Phase boundaries</subject><subject>Solid solutions</subject><subject>Spinel</subject><subject>Synthesis</subject><subject>Synthesis and Properties of Inorganic Compounds</subject><subject>X-rays</subject><issn>0036-0236</issn><issn>1531-8613</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFkbFOwzAQhi0EEqXwAGweyxC4sx3XGVFFAalSh4KEukSuY4OrNAlxIqVvwMwj8iQklI2B6XT3f_8vnX5CLhGuEbm4WQFwCYxLZMAAQR6REcYcIyWRH5PRIEeDfkrOQtgCCAFTNSJ-tS-aNxt8oLrI6EtU6z3NvHO1No0vCxqaNtvT0lFT7qrcdrTsfGbDcOl9dF0w-vXxSbvJutarYnOFh3VuWbcUP6Yy-CHpnJw4nQd78TvH5Hl-9zR7iBbL-8fZ7SKqEBIZaRWDcEpaKRQaxWQsEeUmUQ4zZWwSM82cibUBAWAMs3wqjNtYprLYJQL4mEwOuVVdvrc2NOnOB2PzXBe2bEOKU8mQ8VjE_6PAkSVCJapH2QENVe2LV1un27Kti_6RnkqHCtI_FfBvYM140Q</recordid><startdate>20120201</startdate><enddate>20120201</enddate><creator>Grigoryan, R. A.</creator><creator>Grigoryan, L. A.</creator><general>SP MAIK Nauka/Interperiodica</general><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20120201</creationdate><title>Synthesis and X-ray diffraction study of complex oxides of the Zn2 − x(ZraSnb)1 − xFe2xO4 composition</title><author>Grigoryan, R. A. ; Grigoryan, L. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p1096-a8504f86e6481c82656116b98f1d8ce952a2fc5ac0400cc2e374cfbe28d5f9403</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Diffraction</topic><topic>Homogeneity</topic><topic>Inorganic Chemistry</topic><topic>Oxides</topic><topic>Phase boundaries</topic><topic>Solid solutions</topic><topic>Spinel</topic><topic>Synthesis</topic><topic>Synthesis and Properties of Inorganic Compounds</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Grigoryan, R. A.</creatorcontrib><creatorcontrib>Grigoryan, L. A.</creatorcontrib><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Russian journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Grigoryan, R. A.</au><au>Grigoryan, L. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and X-ray diffraction study of complex oxides of the Zn2 − x(ZraSnb)1 − xFe2xO4 composition</atitle><jtitle>Russian journal of inorganic chemistry</jtitle><stitle>Russ. J. Inorg. Chem</stitle><date>2012-02-01</date><risdate>2012</risdate><volume>57</volume><issue>2</issue><spage>146</spage><epage>151</epage><pages>146-151</pages><issn>0036-0236</issn><eissn>1531-8613</eissn><abstract>A multicomponent system of complex refractory oxides of the composition Zn
2 −
x
(Zr
a
Sn
b
)
1 −
x
Fe
2
x
O
4
(
a + b
= 1;
a
:
b
= 1: 5, 1: 4, 1: 3, 1: 2, 1: 1, 2: 1, 3: 1, 4: 1;
x
= 0−1.0; Δ
x
= 0.05) was studied by X-ray diffraction. The samples were prepared from oxides of appropriate metals by low-temperature plasma synthesis (hydrogen-oxygen flame). Two phases with wide homogeneity ranges were identified: α phase crystallized in the crystal system of inverse cubic spinel and β phase with the structure of tetragonal spinel. The phase boundaries were found. Structural data are presented for about 100 solid solutions.</abstract><cop>Dordrecht</cop><pub>SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S0036023612020106</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0036-0236 |
| ispartof | Russian journal of inorganic chemistry, 2012-02, Vol.57 (2), p.146-151 |
| issn | 0036-0236 1531-8613 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1762123545 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Chemistry Chemistry and Materials Science Diffraction Homogeneity Inorganic Chemistry Oxides Phase boundaries Solid solutions Spinel Synthesis Synthesis and Properties of Inorganic Compounds X-rays |
| title | Synthesis and X-ray diffraction study of complex oxides of the Zn2 − x(ZraSnb)1 − xFe2xO4 composition |
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