A multipurpose ultra-high vacuum-compatible chamber for in situ X-ray surface scattering studies over a wide range of temperature and pressure environment conditions
A low/high temperature (60-1000K) and pressure (10−10−3x103 mbar) "baby chamber", specially adapted to the grazing-incidence X-ray scattering station, has been designed, developed and installed at the Spanish CRG BM25 SpLine beamline at European Synchrotron Radiation Facility. The chamber...
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| Veröffentlicht in: | Journal of physics. Conference series 2013-01, Vol.425 (13), p.132002-6 |
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| creator | Ferrer, P Rubio-Zuazo, J Heyman, C Esteban-Betegón, F Castro, G R |
| description | A low/high temperature (60-1000K) and pressure (10−10−3x103 mbar) "baby chamber", specially adapted to the grazing-incidence X-ray scattering station, has been designed, developed and installed at the Spanish CRG BM25 SpLine beamline at European Synchrotron Radiation Facility. The chamber has a cylindrical form with 100 mm of diameter, built on a 360° beryllium nipple of 150 mm height. The UHV equipment and a turbo pump are located on the upper part of the chamber to leave a wide solid angle for exploring reciprocal space. The chamber features 4 CF16 and 5 CF40 ports for electrical feed through and leak valves, ion gun, etc. The heat exchanger is a customized compact LN2 (or LHe) continuous flow cryostat. The sample is mounted on a Mo support on the heat exchanger, which has in the back side a BORALECTRIC® Heater Elements. Experiments of surfaces/interfaces/ multilayer materials, thin films or single crystals in a huge variety of environments can be performed, also in situ studies of growth or evolution of the samples. Data measurement can be collected with a punctual and a bi-dimensional detector, being possible to simultaneously use them. |
| doi_str_mv | 10.1088/1742-6596/425/13/132002 |
| format | Article |
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The chamber has a cylindrical form with 100 mm of diameter, built on a 360° beryllium nipple of 150 mm height. The UHV equipment and a turbo pump are located on the upper part of the chamber to leave a wide solid angle for exploring reciprocal space. The chamber features 4 CF16 and 5 CF40 ports for electrical feed through and leak valves, ion gun, etc. The heat exchanger is a customized compact LN2 (or LHe) continuous flow cryostat. The sample is mounted on a Mo support on the heat exchanger, which has in the back side a BORALECTRIC® Heater Elements. Experiments of surfaces/interfaces/ multilayer materials, thin films or single crystals in a huge variety of environments can be performed, also in situ studies of growth or evolution of the samples. Data measurement can be collected with a punctual and a bi-dimensional detector, being possible to simultaneously use them.</description><identifier>ISSN: 1742-6588</identifier><identifier>EISSN: 1742-6596</identifier><identifier>DOI: 10.1088/1742-6596/425/13/132002</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Beryllium ; Chambers ; Continuous flow ; Cylindrical chambers ; Detectors ; Diameters ; Heat exchangers ; Heaters ; High temperature ; High vacuum ; Multilayers ; Particle physics ; Physics ; Scattering ; Single crystals ; Synchrotron radiation ; Synchrotrons ; Thin films ; Turbine pumps ; X-ray scattering ; X-rays</subject><ispartof>Journal of physics. 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Conference series</title><description>A low/high temperature (60-1000K) and pressure (10−10−3x103 mbar) "baby chamber", specially adapted to the grazing-incidence X-ray scattering station, has been designed, developed and installed at the Spanish CRG BM25 SpLine beamline at European Synchrotron Radiation Facility. The chamber has a cylindrical form with 100 mm of diameter, built on a 360° beryllium nipple of 150 mm height. The UHV equipment and a turbo pump are located on the upper part of the chamber to leave a wide solid angle for exploring reciprocal space. The chamber features 4 CF16 and 5 CF40 ports for electrical feed through and leak valves, ion gun, etc. The heat exchanger is a customized compact LN2 (or LHe) continuous flow cryostat. The sample is mounted on a Mo support on the heat exchanger, which has in the back side a BORALECTRIC® Heater Elements. Experiments of surfaces/interfaces/ multilayer materials, thin films or single crystals in a huge variety of environments can be performed, also in situ studies of growth or evolution of the samples. Data measurement can be collected with a punctual and a bi-dimensional detector, being possible to simultaneously use them.</description><subject>Beryllium</subject><subject>Chambers</subject><subject>Continuous flow</subject><subject>Cylindrical chambers</subject><subject>Detectors</subject><subject>Diameters</subject><subject>Heat exchangers</subject><subject>Heaters</subject><subject>High temperature</subject><subject>High vacuum</subject><subject>Multilayers</subject><subject>Particle physics</subject><subject>Physics</subject><subject>Scattering</subject><subject>Single crystals</subject><subject>Synchrotron radiation</subject><subject>Synchrotrons</subject><subject>Thin films</subject><subject>Turbine pumps</subject><subject>X-ray scattering</subject><subject>X-rays</subject><issn>1742-6588</issn><issn>1742-6596</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkV-L1DAQwIsoeJ5-Bgd80Ye6SZo27eNyqCcs3IuCb2GaTndztEnNn5X7QH5PW1b24YbATJLfDAm_onjP2WfO2nbHlRRlU3fNTop6x6t1CcbEi-LmevPyWrft6-JNjI-MVWuom-LvHuY8JbvksPhIsNYBy5M9nuCMJue5NH5eMNl-IjAnnHsKMPoA1kG0KcOvMuATxBxGNATRYEoUrDtCTHmwFMGf1w6EP3YgCOiOBH6ERPNCAVMOBOgGWALFuG3InW3wbiaXwHg32GS9i2-LVyNOkd79z7fFz69fftzdl4eHb9_v9ofSSMZTKepmZIbVhpiSRJKpupdcYC9aEmTGqmdKdF2jKmqxZy1rpRxkpxAFSmRjdVt8usw94aSXYGcMT9qj1ff7g97OGK-VUIqd-cp-vLBL8L8zxaRnGw1NEzryOWquGsE579p6RT88Qx99Dm79iRa1UpUUrFYrpS6UCT7GQOP1BZzpTbXeJOpNqF5Va17pi-rqH2c_nsw</recordid><startdate>20130101</startdate><enddate>20130101</enddate><creator>Ferrer, P</creator><creator>Rubio-Zuazo, J</creator><creator>Heyman, C</creator><creator>Esteban-Betegón, F</creator><creator>Castro, G R</creator><general>IOP Publishing</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>H8D</scope><scope>HCIFZ</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7U5</scope><scope>8BQ</scope><scope>JG9</scope><scope>1XC</scope><scope>VOOES</scope></search><sort><creationdate>20130101</creationdate><title>A multipurpose ultra-high vacuum-compatible chamber for in situ X-ray surface scattering studies over a wide range of temperature and pressure environment conditions</title><author>Ferrer, P ; Rubio-Zuazo, J ; Heyman, C ; Esteban-Betegón, F ; Castro, G R</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c401t-256f0c05ce074ee4075b412ab28e2ecf3b07299673e8ab080844d497aa2a4a0f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Beryllium</topic><topic>Chambers</topic><topic>Continuous flow</topic><topic>Cylindrical chambers</topic><topic>Detectors</topic><topic>Diameters</topic><topic>Heat exchangers</topic><topic>Heaters</topic><topic>High temperature</topic><topic>High vacuum</topic><topic>Multilayers</topic><topic>Particle physics</topic><topic>Physics</topic><topic>Scattering</topic><topic>Single crystals</topic><topic>Synchrotron radiation</topic><topic>Synchrotrons</topic><topic>Thin films</topic><topic>Turbine pumps</topic><topic>X-ray scattering</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ferrer, P</creatorcontrib><creatorcontrib>Rubio-Zuazo, J</creatorcontrib><creatorcontrib>Heyman, C</creatorcontrib><creatorcontrib>Esteban-Betegón, F</creatorcontrib><creatorcontrib>Castro, G R</creatorcontrib><collection>CrossRef</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Aerospace Database</collection><collection>SciTech Premium Collection</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Materials Research Database</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Journal of physics. 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| subjects | Beryllium Chambers Continuous flow Cylindrical chambers Detectors Diameters Heat exchangers Heaters High temperature High vacuum Multilayers Particle physics Physics Scattering Single crystals Synchrotron radiation Synchrotrons Thin films Turbine pumps X-ray scattering X-rays |
| title | A multipurpose ultra-high vacuum-compatible chamber for in situ X-ray surface scattering studies over a wide range of temperature and pressure environment conditions |
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