A straightforward synthesis of alkyl 1H-tetrazol-5-yl thioethers via a one-pot reaction of aldehydes and 1H-tetrazole-5-thiols mediated by N-tosylhydrazones

A straightforward synthesis of alkyl 1H-tetrazol-5-yl thioethers via a one-pot reaction of aldehydes and 1H-tetrazole-5-thiols mediated by N-tosylhydrazones

A straightforward approach for the synthesis of alkyl 1 H -tetrazol-5-yl thioethers from aldehydes and 1 H -tetrazole-5-thiol through a one-pot procedure is presented. The aldehydes were first condensed with N -tosylhydrazine to generate the N -tosylhydrazones, which were then reductively coupled in...

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Veröffentlicht in:RSC advances 2015-01, Vol.5 (38), p.29996-30000
Hauptverfasser: Li, Le-Le, Gao, Lian-Xun, Han, Fu-She
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Aldehydes
Condensing
Joining
Synthesis
Synthesis (chemistry)
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Gao, Lian-Xun
Han, Fu-She
description A straightforward approach for the synthesis of alkyl 1 H -tetrazol-5-yl thioethers from aldehydes and 1 H -tetrazole-5-thiol through a one-pot procedure is presented. The aldehydes were first condensed with N -tosylhydrazine to generate the N -tosylhydrazones, which were then reductively coupled in situ with 1 H -tetrazole-5-thiols under metal-free conditions to afford the thioethers in high to excellent yields.
doi_str_mv 10.1039/C5RA04050G
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source Royal Society Of Chemistry Journals 2008-
subjects Aldehydes
Condensing
Joining
Synthesis
Synthesis (chemistry)
title A straightforward synthesis of alkyl 1H-tetrazol-5-yl thioethers via a one-pot reaction of aldehydes and 1H-tetrazole-5-thiols mediated by N-tosylhydrazones
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