Hexanes/acetonitrile: a binary solvent system for the efficient monosilylation of symmetric primary and secondary diols

[Display omitted] Symmetric diols are useful compounds in the synthesis of natural products, their value often dependent on their successful monoprotection. A general and simple method for the monosilylation of symmetrical primary and secondary diols is reported. The method exploits the solubility d...

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Veröffentlicht in:	Tetrahedron letters 2014-04, Vol.55 (16), p.2600-2602
Hauptverfasser:	Wilke, Burkhardt I., Dornan, Mark H., Yeung, Jon, Boddy, Christopher N., Pinto, Atahualpa
Format:	Artikel
Sprache:	eng
Schlagworte:	Acetonitrile Binary solvent system Binary systems (materials) Diols Hexanes Monoprotection Silylation Solubility Solvents Symmetric diol Symmetry Tetrahedrons
Online-Zugang:	Volltext
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