newly developed molecularly imprinted polymer on the surface of TiO2 for selective extraction of triazine herbicides residues in maize, water, and soil
A new surface molecularly imprinted polymer (MIP) based on nano-TiO₂ was developed using propazine (Pro) as a template molecule, ethyleneglycol dimethacrylate (EGDMA) as a crosslinker, methacrylic acid (MAA) as a functional monomer, and 2,2′-azobis (isobutyronitrile) (AIBN) as an initiator. Structur...
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2015-11, Vol.407 (29), p.8803-8812 |
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| creator | Geng, Hao Ran Miao, Shan Shan Jin, She Feng Yang, Hong |
| description | A new surface molecularly imprinted polymer (MIP) based on nano-TiO₂ was developed using propazine (Pro) as a template molecule, ethyleneglycol dimethacrylate (EGDMA) as a crosslinker, methacrylic acid (MAA) as a functional monomer, and 2,2′-azobis (isobutyronitrile) (AIBN) as an initiator. Structures of the newly synthesized surface MIPs were characterized by Fourier transmission infrared spectrometry (FT-IR), scanning electron microscope (SEM), transmission electron microscope (TEM), and X-ray diffraction (XRD). The MIP had a good adsorption capacity and high recognition selectivity to propazine. Meanwhile, it exhibited a cross-selectivity for simazine (Sim) and atrazine (Atr). The MIPs were used as a solid phase extraction (SPE) material. Concomitant extraction, purification, and determination of three pesticides (Pro, Sim, and Atr) residues in water, soil, and maize plant and grain samples were performed by MIP-SPE coupled with high performance liquid chromatography (HPLC). The highly selective separation and enrichment of Pro, Atr, and Sim from the complex environmental media can be achieved. Thus, the newly developed technique provides an analytical platform to quantify the trace amount of Pro, Sim, and Atr residues in multi environmental media and food source. |
| doi_str_mv | 10.1007/s00216-015-9039-x |
| format | Article |
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Structures of the newly synthesized surface MIPs were characterized by Fourier transmission infrared spectrometry (FT-IR), scanning electron microscope (SEM), transmission electron microscope (TEM), and X-ray diffraction (XRD). The MIP had a good adsorption capacity and high recognition selectivity to propazine. Meanwhile, it exhibited a cross-selectivity for simazine (Sim) and atrazine (Atr). The MIPs were used as a solid phase extraction (SPE) material. Concomitant extraction, purification, and determination of three pesticides (Pro, Sim, and Atr) residues in water, soil, and maize plant and grain samples were performed by MIP-SPE coupled with high performance liquid chromatography (HPLC). The highly selective separation and enrichment of Pro, Atr, and Sim from the complex environmental media can be achieved. Thus, the newly developed technique provides an analytical platform to quantify the trace amount of Pro, Sim, and Atr residues in multi environmental media and food source.</description><identifier>ISSN: 1618-2642</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-015-9039-x</identifier><identifier>PMID: 26410737</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>adsorption ; Agriculture ; Analytical Chemistry ; Atrazine ; Biochemistry ; Characterization and Evaluation of Materials ; Chemicals ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Corn ; Crop residues ; Electron microscopes ; Environmental Pollutants - analysis ; Environmental Pollutants - isolation & purification ; ethylene glycol ; Food Analysis - methods ; Food Science ; Fourier transform infrared spectroscopy ; Herbicides ; Herbicides - analysis ; Herbicides - isolation & purification ; high performance liquid chromatography ; Laboratory Medicine ; Limit of Detection ; Liquid chromatography ; Models, Molecular ; molecular imprinting ; Molecular Imprinting - methods ; Monitoring/Environmental Analysis ; Pesticide residues ; Pesticides ; Polymerization ; Polymers ; Polymers - chemistry ; propazine ; Research Paper ; scanning electron microscopes ; scanning electron microscopy ; Simazine ; soil ; Soil - chemistry ; solid phase extraction ; Solid Phase Extraction - methods ; Spectrometry ; Titanium - chemistry ; Titanium dioxide ; transmission electron microscopes ; transmission electron microscopy ; Triazines - analysis ; Triazines - isolation & purification ; Water - analysis ; X-ray diffraction ; Zea mays - chemistry</subject><ispartof>Analytical and bioanalytical chemistry, 2015-11, Vol.407 (29), p.8803-8812</ispartof><rights>Springer-Verlag Berlin Heidelberg 2015</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c503t-78d312ef65ed9448db023efc69658f9240bd9e933e6cb2b447c4b7f077f717bd3</citedby><cites>FETCH-LOGICAL-c503t-78d312ef65ed9448db023efc69658f9240bd9e933e6cb2b447c4b7f077f717bd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00216-015-9039-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00216-015-9039-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27926,27927,41490,42559,51321</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/26410737$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Geng, Hao Ran</creatorcontrib><creatorcontrib>Miao, Shan Shan</creatorcontrib><creatorcontrib>Jin, She Feng</creatorcontrib><creatorcontrib>Yang, Hong</creatorcontrib><title>newly developed molecularly imprinted polymer on the surface of TiO2 for selective extraction of triazine herbicides residues in maize, water, and soil</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>A new surface molecularly imprinted polymer (MIP) based on nano-TiO₂ was developed using propazine (Pro) as a template molecule, ethyleneglycol dimethacrylate (EGDMA) as a crosslinker, methacrylic acid (MAA) as a functional monomer, and 2,2′-azobis (isobutyronitrile) (AIBN) as an initiator. Structures of the newly synthesized surface MIPs were characterized by Fourier transmission infrared spectrometry (FT-IR), scanning electron microscope (SEM), transmission electron microscope (TEM), and X-ray diffraction (XRD). The MIP had a good adsorption capacity and high recognition selectivity to propazine. Meanwhile, it exhibited a cross-selectivity for simazine (Sim) and atrazine (Atr). The MIPs were used as a solid phase extraction (SPE) material. Concomitant extraction, purification, and determination of three pesticides (Pro, Sim, and Atr) residues in water, soil, and maize plant and grain samples were performed by MIP-SPE coupled with high performance liquid chromatography (HPLC). The highly selective separation and enrichment of Pro, Atr, and Sim from the complex environmental media can be achieved. Thus, the newly developed technique provides an analytical platform to quantify the trace amount of Pro, Sim, and Atr residues in multi environmental media and food source.</description><subject>adsorption</subject><subject>Agriculture</subject><subject>Analytical Chemistry</subject><subject>Atrazine</subject><subject>Biochemistry</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemicals</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Corn</subject><subject>Crop residues</subject><subject>Electron microscopes</subject><subject>Environmental Pollutants - analysis</subject><subject>Environmental Pollutants - isolation & purification</subject><subject>ethylene glycol</subject><subject>Food Analysis - methods</subject><subject>Food Science</subject><subject>Fourier transform infrared spectroscopy</subject><subject>Herbicides</subject><subject>Herbicides - analysis</subject><subject>Herbicides - 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analysis</subject><subject>Triazines - isolation & purification</subject><subject>Water - analysis</subject><subject>X-ray diffraction</subject><subject>Zea mays - chemistry</subject><issn>1618-2642</issn><issn>1618-2650</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kUtv1TAQhSMEog_4AWzAEpsuGvAjseMlqnhJlbqgXVuOPW5dJfHFTtp7-0f4u8xVSoVYsPLR6DvHozlV9YbRD4xS9bFQypmsKWtrTYWut8-qQyZZV3PZ0udPuuEH1VEptxTBjsmX1QHOGFVCHVa_JrgfdsTDHQxpA56MaQC3DDbjNI6bHKcZp5s07EbIJE1kvgFSlhysA5ICuYwXnISUSQE0zvEOCGznbFEijMCco32IE5AbyH100UMhGUr0C4o4kdHGBzgl93aGfErs5ElJcXhVvQh2KPD68T2urr58vjz7Vp9ffP1-9um8di0Vc606LxiHIFvwumk631MuIDipZdsFzRvaew1aCJCu533TKNf0KlClgmKq9-K4OllzNzn9xI1mM8biYBjsBGkphikhmBZdIxB9_w96m5Y84XZItY0UulMcKbZSLqdSMgSDNxxt3hlGzb41s7ZmsAyzb81s0fP2MXnpR_BPjj81IcBXoOwLuYb819f_SX23moJNxl7nWMzVD06ZpIhq1XbiN8b8rjg</recordid><startdate>20151101</startdate><enddate>20151101</enddate><creator>Geng, Hao Ran</creator><creator>Miao, Shan Shan</creator><creator>Jin, She Feng</creator><creator>Yang, Hong</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>FBQ</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>7U7</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>H8D</scope><scope>H8G</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>JQ2</scope><scope>K9.</scope><scope>KB.</scope><scope>KR7</scope><scope>L7M</scope><scope>LK8</scope><scope>L~C</scope><scope>L~D</scope><scope>M0S</scope><scope>M1P</scope><scope>M7P</scope><scope>P64</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope></search><sort><creationdate>20151101</creationdate><title>newly developed molecularly imprinted polymer on the surface of TiO2 for selective extraction of triazine herbicides residues in maize, water, and soil</title><author>Geng, Hao Ran ; Miao, Shan Shan ; Jin, She Feng ; Yang, Hong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c503t-78d312ef65ed9448db023efc69658f9240bd9e933e6cb2b447c4b7f077f717bd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>adsorption</topic><topic>Agriculture</topic><topic>Analytical Chemistry</topic><topic>Atrazine</topic><topic>Biochemistry</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemicals</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Corn</topic><topic>Crop residues</topic><topic>Electron microscopes</topic><topic>Environmental Pollutants - 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Academic</collection><jtitle>Analytical and bioanalytical chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Geng, Hao Ran</au><au>Miao, Shan Shan</au><au>Jin, She Feng</au><au>Yang, Hong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>newly developed molecularly imprinted polymer on the surface of TiO2 for selective extraction of triazine herbicides residues in maize, water, and soil</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2015-11-01</date><risdate>2015</risdate><volume>407</volume><issue>29</issue><spage>8803</spage><epage>8812</epage><pages>8803-8812</pages><issn>1618-2642</issn><eissn>1618-2650</eissn><abstract>A new surface molecularly imprinted polymer (MIP) based on nano-TiO₂ was developed using propazine (Pro) as a template molecule, ethyleneglycol dimethacrylate (EGDMA) as a crosslinker, methacrylic acid (MAA) as a functional monomer, and 2,2′-azobis (isobutyronitrile) (AIBN) as an initiator. Structures of the newly synthesized surface MIPs were characterized by Fourier transmission infrared spectrometry (FT-IR), scanning electron microscope (SEM), transmission electron microscope (TEM), and X-ray diffraction (XRD). The MIP had a good adsorption capacity and high recognition selectivity to propazine. Meanwhile, it exhibited a cross-selectivity for simazine (Sim) and atrazine (Atr). The MIPs were used as a solid phase extraction (SPE) material. Concomitant extraction, purification, and determination of three pesticides (Pro, Sim, and Atr) residues in water, soil, and maize plant and grain samples were performed by MIP-SPE coupled with high performance liquid chromatography (HPLC). The highly selective separation and enrichment of Pro, Atr, and Sim from the complex environmental media can be achieved. Thus, the newly developed technique provides an analytical platform to quantify the trace amount of Pro, Sim, and Atr residues in multi environmental media and food source.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>26410737</pmid><doi>10.1007/s00216-015-9039-x</doi><tpages>10</tpages></addata></record> |
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| source | MEDLINE; SpringerNature Journals |
| subjects | adsorption Agriculture Analytical Chemistry Atrazine Biochemistry Characterization and Evaluation of Materials Chemicals Chemistry Chemistry and Materials Science Chromatography Corn Crop residues Electron microscopes Environmental Pollutants - analysis Environmental Pollutants - isolation & purification ethylene glycol Food Analysis - methods Food Science Fourier transform infrared spectroscopy Herbicides Herbicides - analysis Herbicides - isolation & purification high performance liquid chromatography Laboratory Medicine Limit of Detection Liquid chromatography Models, Molecular molecular imprinting Molecular Imprinting - methods Monitoring/Environmental Analysis Pesticide residues Pesticides Polymerization Polymers Polymers - chemistry propazine Research Paper scanning electron microscopes scanning electron microscopy Simazine soil Soil - chemistry solid phase extraction Solid Phase Extraction - methods Spectrometry Titanium - chemistry Titanium dioxide transmission electron microscopes transmission electron microscopy Triazines - analysis Triazines - isolation & purification Water - analysis X-ray diffraction Zea mays - chemistry |
| title | newly developed molecularly imprinted polymer on the surface of TiO2 for selective extraction of triazine herbicides residues in maize, water, and soil |
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