Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology

Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl2 and K2HPO4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120 °C via mi...

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Veröffentlicht in:Chemistry letters 2012-04, Vol.41 (4), p.458-460
Hauptverfasser: Benzigar, Mercy R, Mane, Gurudas P, Talapaneni, Siddulu N, Varghese, Shaji, Anand, Chokkalingam, Aldeyab, Salem S, Balasubramanian, Veerappan V, Vinu, Ajayan
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container_end_page 460
container_issue 4
container_start_page 458
container_title Chemistry letters
container_volume 41
creator Benzigar, Mercy R
Mane, Gurudas P
Talapaneni, Siddulu N
Varghese, Shaji
Anand, Chokkalingam
Aldeyab, Salem S
Balasubramanian, Veerappan V
Vinu, Ajayan
description Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl2 and K2HPO4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120 °C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.
doi_str_mv 10.1246/cl.2012.458
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source Oxford University Press Journals All Titles (1996-Current)
subjects Cetyltrimethylammonium bromide
Crystal structure
Crystallinity
Hydroxyapatite
Microwaves
Morphology
Precursors
Synthesis
title Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology
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