Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology
Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl2 and K2HPO4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120 °C via mi...
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Veröffentlicht in: | Chemistry letters 2012-04, Vol.41 (4), p.458-460 |
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creator | Benzigar, Mercy R Mane, Gurudas P Talapaneni, Siddulu N Varghese, Shaji Anand, Chokkalingam Aldeyab, Salem S Balasubramanian, Veerappan V Vinu, Ajayan |
description | Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl2 and K2HPO4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120 °C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length. |
doi_str_mv | 10.1246/cl.2012.458 |
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The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.</description><subject>Cetyltrimethylammonium bromide</subject><subject>Crystal structure</subject><subject>Crystallinity</subject><subject>Hydroxyapatite</subject><subject>Microwaves</subject><subject>Morphology</subject><subject>Precursors</subject><subject>Synthesis</subject><issn>0366-7022</issn><issn>1348-0715</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFkE1LAzEQhoMoWD9O_oEcBdma76ZHKWoFi-DHOWTTbDcl3axJat1_b6Q9Cp6GGZ55mXkAuMJojAkTt8aPCcJkzLg8AiNMmazQBPNjMEJUiGqCCDkFZymtEUJySskIuIUzMez0l610Si5lu4RvQ5dbWxoYGjh3q9YPcBaHlLX3rrNwYVPoQwzbBOfDMobvQfc6u2zhzuUWavgallVqdV-yFiH2bfBhNVyAk0b7ZC8P9Rx8PNy_z-bV88vj0-zuuTKM0VwJ3jBOhJVMUqk1RVxaUUtas5pM9ZQTI7ARmk0to6RBom40RszwplnqSW0QPQfX-9w-hs-tTVltXDLWe93ZcrLCE4ow4ozK_1EqOMYESVHQmz1abKUUbaP66DY6Dgoj9eteGa9-3avivtDyQLd240x5Nxhn87Auojq1DtvYldmfqz8_h4u7</recordid><startdate>20120405</startdate><enddate>20120405</enddate><creator>Benzigar, Mercy R</creator><creator>Mane, Gurudas P</creator><creator>Talapaneni, Siddulu N</creator><creator>Varghese, Shaji</creator><creator>Anand, Chokkalingam</creator><creator>Aldeyab, Salem S</creator><creator>Balasubramanian, Veerappan V</creator><creator>Vinu, Ajayan</creator><general>The Chemical Society of Japan</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20120405</creationdate><title>Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology</title><author>Benzigar, Mercy R ; Mane, Gurudas P ; Talapaneni, Siddulu N ; Varghese, Shaji ; Anand, Chokkalingam ; Aldeyab, Salem S ; Balasubramanian, Veerappan V ; Vinu, Ajayan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c443t-65f4526e84838aa3058e6b83b4b29a952c61c6a49e432f06bfa104c5ffda7bc03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Cetyltrimethylammonium bromide</topic><topic>Crystal structure</topic><topic>Crystallinity</topic><topic>Hydroxyapatite</topic><topic>Microwaves</topic><topic>Morphology</topic><topic>Precursors</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Benzigar, Mercy R</creatorcontrib><creatorcontrib>Mane, Gurudas P</creatorcontrib><creatorcontrib>Talapaneni, Siddulu N</creatorcontrib><creatorcontrib>Varghese, Shaji</creatorcontrib><creatorcontrib>Anand, Chokkalingam</creatorcontrib><creatorcontrib>Aldeyab, Salem S</creatorcontrib><creatorcontrib>Balasubramanian, Veerappan V</creatorcontrib><creatorcontrib>Vinu, Ajayan</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Chemistry letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Benzigar, Mercy R</au><au>Mane, Gurudas P</au><au>Talapaneni, Siddulu N</au><au>Varghese, Shaji</au><au>Anand, Chokkalingam</au><au>Aldeyab, Salem S</au><au>Balasubramanian, Veerappan V</au><au>Vinu, Ajayan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology</atitle><jtitle>Chemistry letters</jtitle><addtitle>Chemistry Letters</addtitle><date>2012-04-05</date><risdate>2012</risdate><volume>41</volume><issue>4</issue><spage>458</spage><epage>460</epage><pages>458-460</pages><issn>0366-7022</issn><eissn>1348-0715</eissn><abstract>Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl2 and K2HPO4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120 °C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.</abstract><pub>The Chemical Society of Japan</pub><doi>10.1246/cl.2012.458</doi><tpages>3</tpages></addata></record> |
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source | Oxford University Press Journals All Titles (1996-Current) |
subjects | Cetyltrimethylammonium bromide Crystal structure Crystallinity Hydroxyapatite Microwaves Morphology Precursors Synthesis |
title | Microwave-assisted Synthesis of Highly Crystalline Mesoporous Hydroxyapatite with a Rod-shaped Morphology |
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