Ultrasound-driven preparation and pair distribution function-assisted structure solution of a copper-based layered coordination polymer

Ultrasound-driven preparation and pair distribution function-assisted structure solution of a copper-based layered coordination polymer

Nanoparticles of a copper-based layered coordination polymer, STAM-2, have been prepared via an ultrasound mediated transformation from a layered metal-organic framework, STAM-1. The structure of the material was then solved using pair distribution function analysis to identify the structural units...

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Veröffentlicht in:Dalton transactions : an international journal of inorganic chemistry 2014-07, Vol.43 (27), p.10438-10442
Hauptverfasser: Mohideen, M Infas, Allan, Phoebe K, Chapman, Karena W, Hriljac, Joseph A, Morris, Russell E
Format: Artikel
Sprache:eng
Schlagworte:
Coordination polymers
Distribution functions
Mathematical models
Nanoparticles
Transformations
Ultrasound
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Beschreibung
Zusammenfassung:Nanoparticles of a copper-based layered coordination polymer, STAM-2, have been prepared via an ultrasound mediated transformation from a layered metal-organic framework, STAM-1. The structure of the material was then solved using pair distribution function analysis to identify the structural units present and the final structural model refined against the pair distribution function data.
ISSN:1477-9226
1477-9234
DOI:10.1039/c3dt53124d